Ceramic pressure measuring cell and method for its manufacture

Patent metadata

Field	Value
Publication number	US-9816887-B2
Application number	US-201214004228-A
Country	US
Kind code	B2
Filing date	Feb 10, 2012
Priority date	Mar 16, 2011
Publication date	Nov 14, 2017
Grant date	Nov 14, 2017

Abstract

A method for manufacturing a pressure measuring cell, which has a ceramic platform and a ceramic measuring membrane, wherein the measuring membrane is joined with the platform pressure tightly by an active hard solder, or braze, wherein the method includes: providing the platform, the measuring membrane and the active hard solder, or braze, positioning the active hard solder, or braze, between the platform and the measuring membrane; melting the active hard solder, or braze, by irradiating the active hard solder, or braze, by a laser, wherein the irradiating of the active hard solder, or braze, occurs through the measuring membrane; and letting the active hard solder, or braze, solidify by cooling.

First claim

The invention claimed is:

1. A method for manufacturing a pressure measuring cell, which has a ceramic platform and a ceramic measuring membrane, wherein the measuring membrane is joined with the platform pressure tightly by an active hard solder, or braze, the method comprising:
providing the platform, the measuring membrane and the active hard solder, or braze;
positioning the active hard solder, or braze, between the platform and the measuring membrane;
melting the active hard solder, or braze, by irradiating the active hard solder, or braze, by a laser, wherein the irradiating of the active hard solder, or braze, occurs through the measuring membrane; and
letting the active hard solder, or braze, solidify by cooling.

2. The method as claimed in claim 1 , wherein:
said melted of the active hard solder, or braze, is held at or above the liquidus temperature not more than 1 minute, especially not more than30seconds, preferably not more than 15 seconds.

3. The method as claimed in claim 1 , wherein:
said letting of the active hard solder, or braze, solidify by cooling occurs down to the solidus temperature with an average cooling rate of not less than 20 K/minute, especially not less than 40 K/minute, preferably not less than 1 K/second, and especially preferably not less than 2 K/second.

4. The method as claimed in claim 3 , wherein:
the further cooling occurs down to a temperature of 100K below the solidus temperature, preferably 200K below the solidus temperature, with an average rate of not less than 20 K/minute, especially not less than 40 K/minute, preferably not less than 1 K/second and especially preferably not less than 2 K/second.

5. The method as claimed in claim 1 , wherein:
said cooling is supported by providing the pressure sensor with a noble gas, especially argon.

6. The method as claimed in claim 1 , wherein:
said irradiating of the active solder occurs by means of a laser at a wavelength, at which the ceramic material of the measuring membrane does not absorb or, at most, negligibly absorbs, wherein the wavelength especially lies in the visible region.

7. The method as claimed in claim 1 , wherein:
the platform and the measuring membrane are heated at least locally in the region of the joint to a temperature, which lies not more than 200 K, especially not more than 100 K and preferably not more than 50 K below the solidus temperature of the active hard solder, or braze.

8. The method as claimed in claim 7 , wherein:
the preheating occurs by a laser in a wavelength range, in which the ceramic material of the platform, or the measuring membrane, absorbs, especially by means of a Nd-YAG laser or a CO 2 laser.

9. The method as claimed in claim 7 , wherein:
the preheating occurs by an oven, in which the components are arranged.

10. The method as claimed in claim 1 , wherein:
the melting of the active hard solder, or braze, and the letting of the active hard solder, or braze, solidify occur at least at times under vacuum and/or protective-gas, especially argon.

11. The method as claimed in claim 1 , wherein:
the ceramic material of the platform and the measuring membrane comprise corundum.

12. The method as claimed in claim 1 , wherein:
the ceramic material of the measuring membrane is essentially transparent.

13. A pressure measuring cell, comprising:
a ceramic platform; and
a ceramic measuring membrane, wherein:
said measuring membrane is connected with a surface of said platform by a peripheral joint to form a measuring chamber between the surface of said platform and said measuring membrane;
said joint comprises an active hard solder, or braze, wherein, to the extent that the joint contains any segregated, especially granularly segregated, phases of the active hard solder, or braze, these segregated phases have a maximum extent in a direction perpendicular to the surface of said platform of not more than 4 μm, especially not more than 2 μm and preferably not more than 1 μm.

14. The pressure measuring cell as claimed in claim 13 , wherein:
said ceramic measuring membrane and said ceramic platform comprise corundum; and
said active hard solder, or braze, comprises a Zr—Ni—Ti active hard solder, or braze, or a Cu—Ti—Zr—Ni active hard solder, or braze.

Assignees

• Berlinger Andrea
• Drewes Ulfert
• Rossberg Andreas
• Schmidt Elke
• Uehlin Thomas
• Endress Hauser Gmbh Co Kg

Inventors

• Berlinger Andrea
• Drewes Ulfert
• Rossberg Andreas
• Schmidt Elke
• Uehlin Thomas

Classifications

• B23K2203/172

  Operations & Transport · mapped topic

• G01L9/0048 Primary

  Details about the mounting of the diaphragm to its support or about the diaphragm edges, e.g. notches, round shapes for stress relief · CPC title

• C04B2237/708

  of one or more of the interlayers · CPC title

• B23K1/0016

  Soldering of electronic components · CPC title

• C22C30/02

  containing copper · CPC title