Method of manufacturing single crystal

Patent metadata

Field	Value
Publication number	US-9816199-B2
Application number	US-201514965177-A
Country	US
Kind code	B2
Filing date	Dec 10, 2015
Priority date	Dec 24, 2014
Publication date	Nov 14, 2017
Grant date	Nov 14, 2017

Abstract

A manufacturing method of single crystal is provided with a melting process for dissolving raw material in a crucible and a pulling-up process of a single crystal from a melt by the Czochralski method. The pulling-up process includes detecting an edge line of a fusion ring, determining an approximated curve of the edge line by approximating the edge line of the fusion ring by an even function, eliminating constituent pixels of the fusion ring from the image of the fusion ring as noise, the constituent pixels being positioned on the side of the melt relative to the approximated curve and the constituent pixels of the fusion ring and a deviation between the constituent pixels and the approximated curve being a predetermined number of pixels, and calculating the center position of the single crystal from the edge line of the fusion ring from which the noise has been eliminated.

First claim

What is claimed is:

1. A method of manufacturing a single crystal, the method comprising:
a melting process which generates a melt by dissolving raw material in a crucible; and
a pulling-up process which pulls up a single crystal from the melt by the Czochralski method, wherein
the pulling-up process includes a step of calculating a center position of the single crystal from an image of a fusion ring which appears near a solid-liquid interface between the single crystal and the melt,
the step of calculating the center position of the single crystal includes steps of:
detecting an edge line of the fusion ring;
determining an approximated curve of the edge line by approximating the edge line of the fusion ring by an even function;
eliminating constituent pixels of the fusion ring from the image of the fusion ring as noise, the constituent pixels being positioned on the side of the melt relative to the approximated curve and the constituent pixels of the fusion ring and a deviation between the constituent pixels and the approximated curve being at least a predetermined number of pixels; and
calculating the center position of the single crystal from the edge line of the fusion ring from which the noise has been eliminated.

2. The method as claimed in claim 1 , wherein the pulling-up process further includes a step of determining the distance from a surface of the melt to a lower end of the heat shielding body that is disposed above the melt based on the center position of the single crystal.

3. The method as claimed in claim 1 , wherein the pulling-up process further includes a step of determining a diameter of the single crystal based on the center position of the single crystal and the edge line of the fusion ring from which the effect of the noise has been eliminated.

4. The method as claimed in claim 1 , wherein the step of eliminating the noise from the fusion ring is repeated again at a predetermined number of times.

5. The method as claimed in claim 1 , wherein the even function is a quadratic equation and the approximated curve is calculated by means of least-squares method.

6. The method as claimed in claim 5 , wherein the least-squares method has non-linear weights, and the non-linear weight becomes smaller as the deviation between the pixel of the fusion ring and the approximate curve is positive and becomes larger.

7. The method as claimed in claim 1 , wherein the step of detecting the edge line of the fusion ring includes:
setting the luminance arrived at by multiplying the maximum brightness in the captured image that includes the fusion ring with a predetermined coefficient as a reference value; and
detecting pixels closest to the side of the melt out of pixels that have the same brightness as the reference value as the constituent pixels of the edge line.

8. The method as claimed in claim 1 , wherein, the melting process includes steps of:
generating a melt by dissolving initial raw material which has been charged in the crucible; and
additionally depositing new raw material into the melt.

9. The method as claimed in claim 1 , wherein the step of calculating the center position of the single crystal includes steps of:
setting up first and second measuring lines which orthogonally intersect a reference value that passes through the center position of the single crystal and which are separated by first and second distances from the center position;
detecting the two intersections of the first measuring line and the edge line of the fusion ring and calculating the first interval between the two intervals on the first measuring line;
detecting the two intersections of the second measuring line and the edge line of the fusion ring and calculating the second interval between the two intervals on the second measuring line; and
calculating the center position of the single crystal which is positioned on the reference value based on the first interval, the second interval, the first distance and the second distance.

Assignees

• Sumco Corp

Inventors

• Takanashi Keiichi
• Hamada Ken

Classifications

• G06T7/62

  of area, perimeter, diameter or volume · CPC title

• G06T2207/30116

  Casting · CPC title

• G06T7/0004

  Industrial image inspection · CPC title

• G06T7/66

  of image moments or centre of gravity · CPC title

• G06T2207/20192

  Edge enhancement; Edge preservation · CPC title