Method for treating mineral sludge by flocculation in-line then above ground

Patent metadata

Field	Value
Publication number	US-9809482-B2
Application number	US-201314430960-A
Country	US
Kind code	B2
Filing date	Oct 15, 2013
Priority date	Nov 16, 2012
Publication date	Nov 7, 2017
Grant date	Nov 7, 2017

Abstract

The improved process for conditioning sludges by flocculation, according to which:
the sludge to be treated is transported in a pipeline, at least one flocculating agent is inserted in the pipeline that transports the sludge to be treated, the sludge is then mixed with the said flocculating agent. finally, the mixture is transported and then discharged in a natural or an artificial excavation at a distance from the bottom of the said excavation that is less than its depth.

First claim

The invention claimed is:

1. A process for conditioning sludge by flocculation, said process comprising:
transporting the sludge to be treated in a pipeline with an outlet,
inserting at least one flocculating agent in the pipeline that transports the sludge to be treated,
mixing the sludge with the said flocculating agent, thereby forming a sludge-flocculant mixture in the pipeline, and
transporting and then discharging the sludge-flocculant mixture in a natural or an artificial excavation at a distance from the bottom of the natural or artificial excavation lesser than that of its depth, wherein said discharging the sludge-flocculant mixture comprises discharging the sludge-flocculant mixture at a first altitude, and wherein the first altitude is less than the altitude of a level of sludge-flocculant mixture obtained after said discharging, such that as the natural or artificial excavation fills up, the pipeline is gradually immersed, thus forming a boiling crater, where boils at the surface of the boiling crater allow flocs to escape onto a rim of the boiling crater, thereby providing for improved flocculation efficiency.

2. The process according to claim 1 wherein the natural or artificial excavation is located in ground on which no sludge has been spread.

3. The process according to claim 1 , wherein the natural or artificial excavation is located entirely or partially on a sludge layer.

4. The process according to claim 1 , wherein at least a portion of the pipeline in which the sludge is transported and from which the sludge-flocculant mixture is discharged is positioned vertically, wherein the vertical portion of the pipeline comprises the outlet.

5. The process according to claim 1 , wherein the flocculating agent is inserted close to the outlet of the pipeline which is about 10 to 200 times the internal diameter of the pipeline.

6. The process according to claim 1 , comprising, in addition to said inserting at least one flocculating agent in the pipeline, inserting at least one flocculating agent directly into the excavation.

7. The process according to claim 6 , wherein the majority of flocculating agent used during the process is inserted into the pipeline.

8. The process according to claim 1 , wherein the flocculating agent is chosen from the group consisting of acrylic acid, ATBS (2-acrylamido 2-methylpropanesulfonic acid), diallyldimethylammonium chloride (DADMAC), dimethylaminoethyl acrylate (DMAEA) and dialkylaminoethyl methacrylate (MADAME) as well as their acidified or quarternized salts, N-vinylpyrrolidone, ethylene polyoxides and polyethylene amine.

9. The process according to claim 7 , wherein the flocculating agent inserted into the pipeline is inserted at a distance from the outlet of the pipeline which is about 10 to 200 times the internal diameter of the pipeline.

10. The process according to claim 2 , wherein at least a portion of the pipeline in which the sludge is transported and from which the sludge-flocculant mixture is unloaded is positioned vertically, wherein the vertical portion of the pipeline comprises the outlet.

11. The process according to claim 10 , wherein the flocculating agent is chosen from the group consisting of acrylic acid, ATBS (2-acrylamido 2-methylpropanesulfonic acid), diallyldimethylammonium chloride (DADMAC), dimethylaminoethyl acrylate (DMAEA) and dialkylaminoethyl methacrylate (MADAME) as well as their acidified or quarternized salts, N-vinylpyrrolidone, ethylene polyoxides and polyethylene amine.

12. The process according to claim 10 , wherein the flocculating agent is inserted close to the outlet of the pipeline, at a distance from the outlet of the pipeline which is about 10 to 200 times the internal diameter of the pipeline.

13. The process according to claim 3 , wherein at least a portion of the pipeline in which the sludge is transported and from which the sludge-flocculant mixture is discharged is positioned vertically, wherein the vertical portion of the pipeline comprises the outlet.

14. The process according to claim 13 , wherein the flocculating agent is chosen from the group consisting of acrylic acid, ATBS (2-acrylamido 2-methylpropanesulfonic acid), diallyldimethylammonium chloride (DADMAC), dimethylaminoethyl acrylate (DMAEA) and dialkylaminoethyl methacrylate (MADAME) as well as their acidified or quarternized salts, N-vinylpyrrolidone, ethylene polyoxides and polyethylene amine.

15. The process according to claim 13 , wherein the flocculating agent is inserted close to outlet of the pipeline, at a distance from outlet of the pipeline which is about 10 to 200 times the internal diameter of the pipeline.

Assignees

• Spcm Sa

Inventors

• Pich René

Classifications

• B09C1/00

  Reclamation of contaminated soil · CPC title

• E21B43/34

  Arrangements for separating materials produced by the well · CPC title

• E21B21/068

  using chemical treatment · CPC title

• C02F1/52

  by flocculation or precipitation of suspended impurities {(C02F1/463 takes precedence)} · CPC title

• B01D21/01

  using flocculating agents (for purifying water C02F1/52; for liquid radioactive waste G21F9/10) · CPC title