Resistance analytical furnace

Patent metadata

Field	Value
Publication number	US-9808797-B2
Application number	US-201313920575-A
Country	US
Kind code	B2
Filing date	Jun 18, 2013
Priority date	Jun 19, 2012
Publication date	Nov 7, 2017
Grant date	Nov 7, 2017

Abstract

A resistance furnace provides an improved upper and lower electrode construction with significantly increased coolant flow. The lower electrode has a tip design that significantly lowers the electrode tip temperature during an analysis. The upper and lower electrodes also cooperate with an improved crucible design to significantly reduce the power required to fuse a specimen contained in the crucible. The furnace uniformly heats the floor and lower side walls of a crucible, which lowers the power requirement for specimen fusion and provides higher structural benefits to provide consistent analysis and manufacturing yields. The crucible has a cylindrical body and pedestal base with an annular smoothly curved concave indentation therebetween.

First claim

The invention claimed is:

1. An electrode assembly for a resistance analytical furnace comprising:
a cylindrical upper electrode including a central axially extending aperture configured for admission of a sample into a crucible, an enlarged cylindrical area below said central axially extending aperture, and a funnel-shaped lower end configured to receive a pedestal of a lower electrode;
the lower electrode including said pedestal configured to support the crucible thereon; said pedestal shaped to be raised into sealable engagement within said funnel-shaped lower end of said upper electrode; said lower electrode including a bottom with an upwardly extending truncated conical recess, a cooling water inlet, and a cooling water outlet communicating with said truncated conical recess, wherein said pedestal of said lower electrode includes a center threaded projection which receives a threaded lower electrode tip, said threaded lower electrode tip which is generally cup-shaped with internal threads which threadably mate with said threaded projection on said lower electrode, wherein said threaded lower electrode tip comprises an alloy of tungsten and copper, and wherein said threaded lower electrode tip includes a centered circular upward projection shaped to extend within a circular recess in the bottom of the crucible;
a nozzle positioned in said lower electrode and coupled to said water inlet, said nozzle having an exit end spaced close to an inside surface of said truncated conical recess for projecting cooling water toward said pedestal of said lower electrode; and
further including an upper electrode outer jacket surrounding said upper electrode, wherein said upper electrode includes cooling fins and said jacket surrounds said fins, said outer jacket including a cooling water inlet and a cooling water outlet for receiving water for cooling said upper electrode.

2. A cooling system for the electrodes of a resistance analytical furnace comprising:
upper and lower electrodes configured to hold a graphite crucible between them, said lower electrode including a bottom having a recess formed therein, wherein said lower electrode has a crucible-receiving pedestal and said recess has a truncated conical shape with a thin upper wall;
a water jacket surrounding said lower electrode, said jacket including a water inlet and a water outlet;
a nozzle positioned in said lower electrode and coupled to said water inlet which directs water toward said bottom of said lower electrode; and
further including an upper water jacket surrounding said upper electrode, said upper water jacket including a water inlet and a water outlet, and wherein said upper electrode has a plurality of spiral fins extending radially outwardly into said upper water jacket.

3. The system as defined in claim 2 , wherein said pedestal of said lower electrode includes a center threaded projection for receiving a threaded lower electrode tip.

4. The system as defined in claim 3 , wherein said threaded lower electrode tip is generally cup-shaped with internal threads which threadably mate with said threaded projection on said lower electrode.

Assignees

• Leco Corp

Inventors

• Wetzel Joshua N
• Ford Gordon C

Classifications

• B01L3/04 Primary

  Crucibles · CPC title

• G01N31/12 Primary

  using combustion (G01N25/20 takes precedence) · CPC title