Process for producing purified tea extract

Patent metadata

Field	Value
Publication number	US-9808023-B2
Application number	US-28140207-A
Country	US
Kind code	B2
Filing date	Mar 1, 2007
Priority date	Mar 2, 2006
Publication date	Nov 7, 2017
Grant date	Nov 7, 2017

Abstract

Provided is a process for producing a tea extract having a high recovery rate of non-polymer catechins, a low caffeine content and an improved taste and color tone. As one embodiment of this invention provides, there is provided a process for producing a purified tea extract by adsorbing a tea extract on a synthetic adsorbent, bringing an aqueous solution of an organic solvent or a basic aqueous solution into contact with the synthetic adsorbent to elute non-polymer catechins, and then bringing the eluate into contact with activated carbon in an aqueous solution of an organic solvent.

First claim

The invention claimed is:

1. A process for producing a purified tea extract, comprising adsorbing a tea extract on a synthetic adsorbent, washing the synthetic adsorbent with a basic aqueous solution or ethanol at a solvent concentration of from 0 to 5 wt %, contacting the synthetic adsorbent with ethanol at a solvent concentration of from 10 to 80 wt % to elute non-polymer catechins, and then bringing the eluate into contact with activated carbon in ethanol, wherein the synthetic adsorbent is an acrylic resin, methacrylic resin, polyvinyl resin or styrene resin.

2. A process for producing a purified tea extract, comprising adsorbing a tea extract on a synthetic adsorbent, eluting said tea extract with a basic aqueous solution by contacting the synthetic adsorbent with said basic aqueous solution to elute non-polymer catechins, adjusting the pH of the eluate to 7 or lower, concentrating the eluate, and then subjecting the eluate to solid-liquid separation to remove precipitated and suspended matters, wherein the synthetic adsorbent is an acrylic resin, methacrylic resin, polyvinyl resin or styrene resin.

3. A process for producing a purified tea extract, comprising adsorbing a tea extract on a synthetic adsorbent, washing the synthetic adsorbent with ethanol at a solvent concentration of from 0 to 5 wt %, and then contacting the synthetic adsorbent with a basic aqueous solution or ethanol at a solvent concentration of from 10 to 80 wt % to fractionate a tea extract having a percentage of non-gallates as non-polymer catechins in a range of from 55 to 100 wt % and a caffeine/non-polymer catechins of from 0 to 0.15, wherein the synthetic adsorbent is an acrylic resin, methacrylic resin, polyvinyl resin or styrene resin.

4. The process according to claim 1 , wherein the tea extract undergoes a hydrolysis treatment.

5. The process according to claim 1 , wherein subsequent to completion of the adsorption step, the synthetic adsorbent is washed, and the basic aqueous solution or ethanol is then brought into contact with the synthetic adsorbent.

6. The process according to claim 1 , wherein the synthetic adsorbent is contacted with ethanol.

7. The process according to claim 1 , wherein the resulting purified tea extract comprises from 25 to 90 wt % of non-polymer catechins based on its solid content.

8. The process according to claim 1 , wherein the resulting purified tea extract comprises from 25 to 90 wt % of non-polymer catechins based on its solid content, and has a ratio of caffeine to non-polymer catechins in a range of from 0 to 0.15.

9. The process according to claim 1 , wherein the resulting purified tea extract comprises from 25 to 90 wt % of non-polymer catechins based on its solid content, a ratio of caffeine to said non-polymer catechins is from 0 to 0.15, a percentage of gallates in said non-polymer catechins is from 0 to 70 wt %, and a ratio of gallic acid to the non-polymer catechins is from 0 to 0.1.

10. The process according to claim 4 , wherein the hydrolysis treatment is treatment with an enzyme, cells or culture having tannase activity.

11. The process according to claim 2 , wherein the tea extract undergoes a hydrolysis treatment.

12. The process according to claim 11 , wherein the hydrolysis treatment is treatment with an enzyme, cells or culture having tannase activity.

Assignees

• Maruyama Eizo
• Sugiyama Yukiteru
• Shikata Kenichi
• Shibata Keiji
• Ueoka Hideaki
• Kao Corp

Inventors

• Maruyama Eizo
• Sugiyama Yukiteru
• Shikata Kenichi
• Shibata Keiji
• Ueoka Hideaki

Classifications

• A23F3/20 Primary

  Removing unwanted substances ({A23F3/166 takes precedence; } reducing or removing alkaloid content A23F3/38) · CPC title

• A23F3/205

  Using flocculating or adsorbing agents · CPC title

• A23F3/00

  Tea; Tea substitutes; Preparations thereof (preservation of tea, tea substitutes or herbal tea A23B85/00) · CPC title

• A23F3/16 Primary

  Tea extraction; Tea extracts; Treating tea extract; Making instant tea · CPC title

• A23F3/18

  Extraction of water soluble tea constituents ({A23F3/166 takes precedence; } isolation of tea flavour or tea oil A23F3/42) · CPC title