Connector unit and connecting system for connecting capillaries, in particular for high-performance liquid chromatography

Patent metadata

Field	Value
Publication number	US-9804134-B2
Application number	US-201214115143-A
Country	US
Kind code	B2
Filing date	Apr 25, 2012
Priority date	May 2, 2011
Publication date	Oct 31, 2017
Grant date	Oct 31, 2017

Abstract

The invention relates to a connector unit for connecting capillaries, in particular for high-performance liquid chromatography, wherein a sealing element sealing the capillary protrudes at least partially into the interior of the capillary, while a portion of the sealing element that protrudes axially from the capillary can be subjected to a compressive force that is introduced via the capillary to obtain an axial or radial plastic and/or elastic deformation.

First claim

The invention claimed is:

1. A connector unit for connecting capillaries comprising:
a) a connector housing which has an axial bore,
b) a capillary which runs along a capillary axis and which has an inner diameter and which projects through the axial bore of the connector housing,
c) a sealing element,
d) a front end of the capillary is sealed off with an elastic and/or plastic deformation of the sealing element with respect to a pilot bore of a bushing unit which is releasably connected to the connector housing,
e) wherein, in a connected state of the connector unit and the bushing unit, the capillary projects into the pilot bore and is situated with the front end opposite, and substantially in alignment with, a bushing capillary or a bushing capillary opening of the bushing unit,
f) wherein the sealing element has a first sealing section and a second sealing section, wherein, at a foremost section of the capillary, the first sealing section extends into an interior of the capillary, and
g) a section of an insert element is arranged within the first sealing section to support the first sealing section in a radial direction.

2. The connector unit as in claim 1 , in that the first sealing section has a form of a hollow cylinder running concentrically with respect to the capillary axis.

3. The connector unit as in claim 1 , in that, in a non-connected state of the connector unit and the bushing unit, the second sealing section of the sealing element projects facing away from the bushing unit and beyond a front end of the capillary.

4. The connector unit as in claim 1 , in that the first sealing section projects into a recess provided on a face side in the capillary, the recess having
a) an annular chamber within a wall of the capillary, or
b) a cylindrical shape concentric with respect to the capillary axis.

5. The connector unit as in claim 1 , in that the insert element engages behind the first sealing section to exert a forwardly directed thrust force.

6. The connector unit as in claim 1 , in that the insert element extends radially outward as far as the inner diameter of the capillary.

7. The connector unit as in claim 1 , in that the insert element is in a form of a sleeve, a rear end of the sleeve, facing away from the front capillary end, has a flange-like widened portion, the flange-like widened portion exerts a forwardly directed thrust force on the first sealing section.

8. The connector unit as in claim 1 , in that an entire inside of the capillary is lined with a plastic lining.

9. The connector unit as in claim 8 , in that the first sealing section is connected integrally to the plastic lining.

10. The connector unit as in claim 1 , in that the sealing element widens radially from the first sealing section towards the second sealing section, wherein in a non-connected state of the connector unit and bushing unit, an outer diameter of the second sealing section substantially corresponds to an outer diameter of the capillary.

11. The connector unit as in claim 10 , in that a front face wall of the capillary is shaped in a manner complementary to a transition profile of the sealing element from the first sealing section to the second sealing section.

12. The connector unit as in claim 1 , in that in a non-connected state of the connector unit and bushing unit, an outer diameter of the second sealing section substantially corresponds to an inner diameter of the pilot bore.

13. The connector unit as claimed in claim 1 further comprising:
a) a hollow cylindrical thrust piece which engages around the capillary in an axial region facing away from a front face surface of the capillary, and
b) in that the thrust piece has a rear face side which faces away from a front end of the capillary and which, in the connected state of the connector unit and bushing unit, has an axial thrust force exerted thereon by the connector housing,
c) wherein the thrust piece is fixedly connected to the capillary such that an axial thrust force can be transmitted to the capillary without a relative movement between the capillary and the thrust piece.

14. The connector unit as in claim 13 , in that the thrust piece and the first sealing section at least partially overlap in an axial direction.

15. The connector unit as in claim 13 , in that the thrust piece and the capillary are fixedly connected with a frictional lock and/or a positive lock.

16. A connection system for connecting a capillary and a bushing capillary comprising:
a bushing unit; and
a connector unit of claim 1 releasably connected to the bushing unit, wherein the bushing unit has the pilot bore into which the capillary extends when the connector unit and bushing unit are in a connected state, and wherein an inner diameter of the pilot bore substantially corresponds to an outer diameter of the capillary.

17. The connector unit as in claim 1 , in which the sealing element has an annular cross section.

18. The connector unit as in claim 7 , in which the flange-like widened portion has an outer diameter that corresponds to an outer diameter of the first sealing section.

19. The connector unit as in claim 8 , in which the plastic lining extends forward as far as a face side of the capillary.

20. The connector unit as in claim 8 , in which the plastic lining extends forward as far as a face side of the second sealing section.

21. The connector unit as in claim 15 , in which the positive lock comprises a crimped connection.

Assignees

• Bürger Daniel
• Schadl Michael
• Dionex Softron Gmbh

Inventors

• Bürger Daniel
• Schadl Michael

Classifications

• G01N30/6026

  Fluid seals · CPC title

• G01N30/6039

  in series · CPC title

• G01N30/6004 Primary

  end pieces · CPC title

• G01N30/60 Primary

  Construction of the column · CPC title