Dry cellulose filaments and the method of making the same

Patent metadata

Field	Value
Publication number	US-9803320-B2
Application number	US-201314440930-A
Country	US
Kind code	B2
Filing date	Nov 7, 2013
Priority date	Nov 7, 2012
Publication date	Oct 31, 2017
Grant date	Oct 31, 2017

Abstract

The present invention relates to dry cellulose filaments and particularly those that are re-dispersible in water. Dry cellulose filaments comprise at least 50% by weight of the filaments having a filament length up to 350 μm; and a diameter of between 100 and 500 nm, wherein the filaments are re-dispersible in water. Also described here is a film of dry cellulose filaments comprising the filaments described, wherein the film is dispersible in water. A method of making a dry film of cellulose filaments is also described that includes providing a liquid suspension of the cellulose filaments described; and retaining the filaments on the forming section of a paper or tissue making machine or on a modified paper or tissue making machine. The film can be optionally converted to powders or flakes for shipment, storage or subsequent uses. The filaments, the film, the powders or flakes and the method are in a preferred embodiment free of additives and the derivatization of the filaments.

First claim

The invention claimed is:

1. A film of dry cellulose filaments, the film comprising
a basis weight of 5 to 120 g cellulose filaments/m 2 of film,
at least 50% by weight of the filaments having:
a filament length up to 350 μm and a diameter of between 100 and 500 nm,
wherein the filaments are fibrillated and free of additives and derivatization,
wherein the film comprising a solids content of 75% to 95% by weight solids, and
wherein the film is produced from a liquid suspension on a paper making machine and is re-dispersible in water.

2. The film according to claim 1 , wherein the film has a range of thickness from 10 to 300 μm.

3. The film according to claim 1 , wherein the filaments lengths are between 300 and 350 μm.

4. The film according to claim 1 , wherein the basis weight is 10 to 100 g of cellulose filaments/m 2 of film.

5. The film according to claim 1 , wherein the basis weight is 10 to 80 g of cellulose filaments/m 2 of film.

6. The film according to claim 1 , wherein the solids content is 80% to 95% by weight solids.

7. A method of making a dry film of fibrillated cellulose filaments comprising:
providing a liquid suspension of the cellulose filaments wherein at least 50% by weight of the filaments comprise a filament length up to 350 μm; and a filament diameter between 100 and 500 nm, wherein the filaments are fibrillated and free of additives and derivatization, and
retaining over 90% of the filaments on a forming section of a paper making machine,
wherein the film produced is re-dispersible in water, and
the film comprising a basis weight of 5 to 120 g cellulose filaments/m 2 of film, a solids content of 75% to 95% by weight solids.

8. The method according to claims 7 , wherein the paper making machine is a Sheet Machine with a 150- to 400-mesh screen.

9. The method according to claim 7 , further comprising pressing the film in a press section of the machine to produce a pressed film.

10. The method according to claim 9 , further comprising drying the pressed film in at least one dryer section of the machine to produce the dry film.

11. The method according to claim 7 , wherein the film produced has a range of thickness from 200-300 μm or less.

12. The method according to claim 7 , wherein the filaments lengths are between 300 and 350 μm.

13. The method according to claim 7 , wherein the paper making machine operates at a speed of 500-1500 m/min.

14. The method according to claim 7 , wherein the basis weight is 10 to 100 g of cellulose filaments/m 2 of film.

15. The method according to claim 7 , wherein the basis weight is 10 to 80 g of cellulose filaments/m 2 of film.

16. The method according to claim 7 , wherein the solids content is 80% to 95% by weight solids.

Assignees

• Fpinnovations

Inventors

• Dorris Gilles Marcel
• Ben Yuxia
• Hu Thomas-Qiuxiong
• Neault Patrick

Classifications

• D21H11/04

  Kraft or sulfate pulp · CPC title

• D21H27/002

  Tissue paper; Absorbent paper (D21H21/22, D21H27/02, D21H27/20 take precedence; toilet paper A47K10/00; absorbent pads for physiological fluids A61L15/16; making on paper-making machines D21F11/00) · CPC title

• D21H11/20 Primary

  Chemically or biochemically modified fibres · CPC title

• D21H21/18

  Reinforcing agents · CPC title

• D21H11/16 Primary

  modified by a particular after-treatment · CPC title