Installation and method with improved performance for forming a compact film of particles on the surface of a carrier fluid

Patent metadata

Field	Value
Publication number	US-9802217-B2
Application number	US-201415027173-A
Country	US
Kind code	B2
Filing date	Oct 9, 2014
Priority date	Oct 11, 2013
Publication date	Oct 31, 2017
Grant date	Oct 31, 2017

Abstract

An installation for forming a compact film of particles on a surface of a carrier fluid, including: a zone acting as a reservoir of carrier fluid; an inclined ramp; a particle storage and transfer zone situated extending from the inclined ramp; a mechanism moving the fluid; a mechanism dispensing the particles in solution, configured to dispense the particles at the surface of the carrier on the surface of the carrier fluid in the zone acting as a reservoir; and a mechanism raising a level of the carrier fluid by capillary effect, arranged at a junction between the zone acting as a reservoir and the inclined ramp.

First claim

The invention claimed is:

1. An installation for forming a compact film of particles on a surface of a carrier fluid, the installation comprising:
a zone acting as a carrier fluid reservoir;
an inclined ramp situated extending from the zone acting as a reservoir and whereon the particles can circulate gravitationally;
a particle storage and transfer zone situated extending from the inclined ramp;
moving means for moving the carrier fluid to make the carrier fluid circulate from the zone, acting as a reservoir, to the particle storage and transfer zone, via the inclined ramp;
dispensing means for dispensing the particles in solution, the dispensing means dispensing the particles on the surface of the carrier fluid in the zone acting as a reservoir; and
raising means for raising a level of the carrier fluid by capillary effect, the raising means arranged at a junction between the zone acting as a reservoir and the inclined ramp.

2. The installation according to claim 1 , wherein the means for raising the level of carrier fluid by capillary effect includes a barrier of contacts spaced out from one another.

3. The installation according to claim 2 , wherein the contacts are fitted with an interval of approximately 2 to 4 mm.

4. The installation according to claim 2 , wherein the contacts have an overall conical, pyramidal, or tubular shape.

5. The installation according to claim 2 , wherein the contacts are made of a hydrophobic material.

6. The installation according to claim 2 , wherein the contacts have a ratio between height in mm and maximum width in mm thereof between 1:1 and 1:30.

7. The installation according to claim 2 , wherein the contacts have a base approximately 2 mm in width and between 2 and 3 mm air height.

8. The installation according to claim 1 , wherein the means for raising the level of the carrier fluid by capillary effect extends along a transverse direction of the installation parallel with the surface of the carrier fluid and orthogonal to a main flow direction of the carrier fluid from the zone acting as a reservoir to the particle storage and transfer zone.

9. The installation according to claim 1 , further comprising a substrate for depositing the compact film of particles, the substrate facing an outlet of particles from the storage and transfer zone.

10. The installation according to claim 9 , configured to carry out deposition of the compact film of particles on a conveyed substrate, the substrate being flexible or rigid.

11. The installation according to claim 1 , further comprising a structure for deflecting particles that pass through the surface of the carrier fluid into the zone acting as a reservoir, the structure arranged downstream from the means for dispensing particles along the main flow direction of the carrier fluid from the zone acting as a reservoir to the particle storage and transfer zone, the structure configured to favour, along the transverse direction of the installation parallel with the surface of the carrier fluid and orthogonal to a main flow direction, spreading of the particles at the outlet of the zone acting as a reservoir, the structure for deflecting particles being permeable to the carrier fluid.

12. A method for forming a compact film of particles on the surface of a carrier fluid, comprising:
providing an installation according to claim 1 ; and
moving the carrier fluid to make the carrier fluid circulate from the zone acting as a reservoir to the particle storage and transfer zone, via the inclined ramp, and dispensing the particles in solution on the surface of the moving carrier fluid, in the zone acting as a reservoir, the moving the carrier fluid being carried out to generate, by capillary effect at the raising means, a bulge of carrier fluid.

13. The method according to claim 12 , used for forming a compact film of particles having a size between 1 nm and 500 μm.

14. The method according to claim 12 , wherein the carrier fluid is deionised water, and the particles are found in solution in a solvent having a surface tension less than that of deionised water, the solvent being n-butanol, methanol, chloroform, or a mixture of at least two thereof.

15. The method according to claim 14 , wherein the solvent is n-butanol, methanol, chloroform, or a mixture of at least two thereof.

Assignees

• Commissariat Energie Atomique
• Commissariat L Energie Atomique Et Aux Energies Alternatives

Inventors

• Dellea Olivier
• Fugier Pascal

Classifications

• B05D2518/10

  Silicon-containing polymers · CPC title

• B05D1/204 Primary

  LB techniques · CPC title

• B05C19/008

  Accessories or implements for use in connection with applying particulate materials to surfaces; not provided elsewhere in B05C19/00 · CPC title

• B05D1/20 Primary

  substances to be applied floating on a fluid · CPC title

• B05D5/08

  to obtain an anti-friction or anti-adhesive surface (rendering particulate materials free-flowing in general, e.g. making them hydrophobic B01J2/30) · CPC title