Method for manufacturing ceramic filter

Patent metadata

Field	Value
Publication number	US-9796632-B2
Application number	US-201514729757-A
Country	US
Kind code	B2
Filing date	Jun 3, 2015
Priority date	Nov 21, 2012
Publication date	Oct 24, 2017
Grant date	Oct 24, 2017

Abstract

A method of manufacturing a ceramic filter for hot gas filtration, and, more particularly, to a method of manufacturing a ceramic filter for hot gas filtration through a drying process. The ceramic filter manufactured by the method is advantageous in that the pore size thereof can be easily adjusted, and the filtering area thereof can be maximized, thus improving the performance thereof. Consequently, the method of manufacturing a ceramic filter can be usefully used in the filter-related industry because a high-performance ceramic filter can be manufactured at a low cost and at low energy.

First claim

What is claimed is:

1. A method of manufacturing a porous ceramic filter, comprising:
filtering a carrier gas including a ceramic-forming composition in the form of a powder on a surface of a polymer filter body having pores of a first size, the ceramic-forming composition containing ceramic precursor particles of a second size and inorganic and/or organic binder, to form a ceramic-forming composition layer on the surface of the polymer filter body (step 1); and
sintering the resultant in step 1, to form a ceramic filter having a pore size of a third size formed by sintering the ceramic precursor particles of the second size, while burning out the polymer filter body (step 2)
wherein the second size is bigger than the first size.

2. The method according to claim 1 , wherein step 1 is repeated at least 2 times using the ceramic precursor particles of the same size.

3. The method according to claim 1 , wherein step 1 is repeated at least 2 times varying the size of ceramic precursor particles and/or the material of ceramic precursor particles.

4. The method according to claim 1 , wherein the ceramic precursor particles are silicon carbide (SiC).

5. The method according to claim 1 , wherein the inorganic and/or organic binder is mullite (3Al 2 O 3 .SiO 2 ), zirconia (ZrO 2 ), calcium carbonate (CaCO 3 ), carboxymethyl cellulose, or a combination thereof.

6. The method according to claim 1 , wherein the ceramic-forming composition comprises silicon carbide (SiC), mullite (3Al 2 O 3 .SiO 2 ), zirconia (ZrO 2 ), calcium carbonate (CaCO 3 ), and carboxymethyl cellulose.

7. The method according to claim 6 , wherein the ceramic-forming composition comprises silicon carbide, mullite, zirconia, calcium carbonate, carboxymethyl cellulose, and water at a weight ratio of 70˜75:3˜4:3˜4:0.5˜1.0:1˜2:10˜20.

8. The method according to claim 1 , wherein the ceramic-forming composition further comprises water.

9. The method according to claim 1 , wherein the size of ceramic precursor particles of the second size ranges from 5 μm to 100 μm.

10. The method according to claim 1 , wherein the polymer filter body is made of polyester, polypropylene, acryl, polyamide, or polyimide.

11. The method according to claim 1 , wherein the filtering step is performed at a rate of from 0.5 m/min to 10 m/min.

12. The method according to claim 1 , wherein ceramic-forming composition layer has a thickness of from 1 mm to 10 mm.

13. The method according to claim 1 , wherein the sintering is performed at a temperature of from 1400° C. to 1500° C.

14. The method according to claim 1 , wherein a heating rate in step 2 of sintering ranges from 3° C./min to 4° C./min.

15. The method according to claim 1 , wherein the sintering is performed for from 1 hour to 5 hours.

Assignees

• Korea Ind Tech Inst

Inventors

• Lee Myong Hwa
• Choi Hyun Jin
• Kim Jeong Uk

Classifications

• C04B2235/6562

  Heating rate · CPC title

• C04B2235/616

  Liquid infiltration of green bodies or pre-forms · CPC title

• C04B35/622

  Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products · CPC title

• C04B2235/3208

  Calcium oxide or oxide-forming salts thereof, e.g. lime · CPC title

• C04B2235/3463

  Alumino-silicates other than clay, e.g. mullite · CPC title