Method for producing a thermally insulating mixture

Patent metadata

Field	Value
Publication number	US-9784402-B2
Application number	US-201314421594-A
Country	US
Kind code	B2
Filing date	Oct 15, 2013
Priority date	Oct 26, 2012
Publication date	Oct 10, 2017
Grant date	Oct 10, 2017

Abstract

A method for continuous production of a thermally insulating mixture comprising silica particles and opacifier particles, in which a premixed stream comprising a carrier gas, silica particles and opacifier particles is introduced into a fine impact mill, ground and mixed therein, after which the solid is separated from the gas stream, wherein the fine impact mill is an air-stream mill comprising grinding tracks arranged one above the other on a rotatable shaft.

First claim

The invention claimed is:

1. A method for continuous production of a thermally insulating mixture comprising silica particles and opacifier particles,
the method comprising
introducing a premixed stream comprising a carrier gas, silica particles and opacifier particles into a fine impact mill, ground and mixed therein, and then
separating solid from the gas stream,
wherein the fine impact mill is an air-stream mill comprising grinding tracks arranged one above the other on a rotatable shaft.

2. The method as claimed in claim 1 , wherein the peripheral speed of the air-stream mill amounts to up to 200 ms −1 .

3. The method as claimed in claim 1 , wherein the mean residence time of the silica particles and opacifier particles in the air-stream mill amounts to less than 10 seconds.

4. The method as claimed in claim 1 , wherein the carrier gas is preheated to 100° C. to 450° C.

5. The method as claimed in claim 1 , wherein the premixed stream is obtained by bringing together silica particles and opacifier particles in each case into a carrier gas stream in each case via a metering unit.

6. The method as claimed in claim 1 , wherein the particulate fractions of the mixture conveyed to the fine impact mill comprise 30 to 95 wt. % silica particles and 5 to 70 wt. % particulate opacifier, relative to the total of the particulate fractions.

7. The method as claimed in claim 1 , wherein loading of the carrier gas amounts to 0.2 to 2 kg solids/Nm 3 carrier gas.

8. The method as claimed in claim 1 , wherein fibers are introduced into the particle-containing stream above the final grinding track, but still inside an air-stream mill.

9. The method as claimed in claim 8 , wherein the fibers are selected from the group consisting of glass wool, rock wool, ceramic fibers, silicon dioxide fibers, cellulose fibers, textile fibers and plastics fibers.

10. The method as claimed in claim 1 , wherein a throughput of silica particles, opacifier particles and optionally fibers amounts in total to at least 200 kg/h.

11. The method as claimed in claim 1 , wherein pyrogenically produced silica particles are employed.

12. The method as claimed in claim 1 , wherein the opacifier particles are selected from the group consisting of carbon blacks, titanium oxides, silicon carbides, zirconium oxides, ilmenites, iron titanates, iron oxides, zirconium silicates, and manganese oxides.

Assignees

• Menzel Frank
• Banert Tobias
• Mueller Hubert
• Geisler Matthias
• Schultz Thorsten
• Evonik Degussa Gmbh

Inventors

• Menzel Frank
• Banert Tobias
• Mueller Hubert
• Geisler Matthias
• Schultz Thorsten

Classifications

• C04B14/062

  Microsilica, e.g. colloïdal silica (preparing microsilica slurries or suspensions C04B18/148) · CPC title

• B02C23/24 Primary

  Passing gas through crushing or disintegrating zone ({B02C15/001}, B02C23/38, B02C23/40 take precedence) · CPC title

• C04B14/064

  Silica aerogel · CPC title

• C04B2103/56

  Opacifiers · CPC title

• C04B30/02

  containing fibrous materials · CPC title