Method and system for impregnating fibers to form a prepreg

Patent metadata

Field	Value
Publication number	US-9782930-B2
Application number	US-201414537977-A
Country	US
Kind code	B2
Filing date	Nov 11, 2014
Priority date	Nov 22, 2013
Publication date	Oct 10, 2017
Grant date	Oct 10, 2017

Abstract

A method for impregnating a fibrous material with a curable resin to form a prepreg is disclosed. The method includes conveying a web material through at least one moving pressure nip formed between a moving pressure roller and a moving supporting surface, wherein the moving pressure roller and the moving supporting surface travel at different velocities relative to each other resulting in a relative velocity between the web material and the pressure nip. The at least one moving pressure nip travels in the same direction as the web material while applying sufficient pressure to compress the web material and to affect impregnation of the fibrous material with the curable resin. Also disclosed is a system for implementing the disclosed impregnation method.

First claim

What is claimed is:

1. A method of impregnating a fibrous material with a curable resin to form a prepreg comprising:
forming a continuous web material comprising a layer of fibrous material between two films of curable resin;
conveying the web material along a travel path and through at least one moving pressure nip formed between a moving pressure roller and a moving supporting surface,
wherein the moving pressure roller and the moving supporting surface travel at different velocities relative to each other resulting in a relative velocity V rel between the web material and the pressure nip, and
wherein the at least one moving pressure nip travels in the same direction as the web material while applying sufficient pressure to compress the web material and to affect impregnation of the fibrous material with the curable resin.

2. The method of claim 1 , wherein the at least one moving pressure nip applies a pressure-at-time of up to 10 MPa·s to affect full impregnation, and
pressure-at-time is defined as P/V rel , where P is the linear force applied to the web material.

3. The method of claim 2 , wherein the web material is conveyed through a plurality of moving pressures nips configured to establish a pressure-at-time of up to 10 MPa·s during impregnation.

4. The method of claim 2 , wherein pressure-at-time is up to 7 MPa·s during impregnation.

5. The method according to claim 1 , wherein the web material is traveling at a velocity of 15 m/min or greater.

6. The method according to claim 1 , wherein the web material is traveling at a velocity of 100 m/min or greater.

7. The method according to claim 1 , wherein
the moving support surface is provided by a rotating drum having an outer circumferential surface, the web material wraps around a portion of the drum's outer circumferential surface as the drum rotates during impregnation, and
the at least one moving pressure nip is a plurality of moving pressure nips, which are created by an endless roller chain of linking idler rollers revolving in a direction opposite to the rotational direction of the rotating drum while some idler rollers in the roller chain are pressed against a portion of the drum's circumferential surface and against the web material passing there between.

8. The method according to claim 1 , wherein,
prior to being conveyed through at least one moving pressure nip, the web material is heated to lower the viscosity of the curable resin, and
after impregnation, the web material is cooled to increase the viscosity of the resin therein.

9. The method of claim 8 , wherein heating of the web material is provided by a pre-heating roll located upstream from the rotating drum, along the travel path of the web material, and cooling of the web material is provided by a chill roll located downstream from the rotating drum.

10. The method according to claim 1 , wherein the curable resin comprises at least one thermoset resin as a major component.

11. The method according to claim 1 , wherein the layer of fibrous material comprises continuous, unidirectional fibers arranged parallel to each other.

12. The method according to claim 1 , wherein the layer of fibrous material is in the form of a continuous, self-supporting fabric.

13. The method according to claim 1 , wherein the layer of fibrous material comprises fibers selected from the group consisting of: glass fibers, carbon fibers, graphite fibers, aramid fibers, polyamide fibers, high-modulus polyethylene (PE) fibers, polyester fibers, poly-p-phenylene-benzoxazole (PBO) fibers, boron fibers, quartz fibers, basalt fibers, ceramic fibers, and combinations thereof.

Assignees

• Cytec Ind Inc

Inventors

• Junker Shawn
• Reynolds Larry

Classifications

• B29C66/82

  Pressure application arrangements, e.g. transmission or actuating mechanisms for joining tools or clamps · CPC title

• B29C35/02

  Heating or curing, e.g. crosslinking or vulcanizing {during moulding, e.g. in a mould}(cold vulcanisation B29C35/18 {; vulcanising tyres, presses therefor B29D30/0601}) · CPC title

• B29L2009/00

  Layered products · CPC title

• B29B15/12 Primary

  of reinforcements of indefinite length · CPC title

• B29C66/45 Primary

  Joining of substantially the whole surface of the articles (methods or apparatus for laminating B32B37/00) · CPC title