Method for purifying isopropyl alcohol

Patent metadata

Field	Value
Publication number	US-9758458-B2
Application number	US-201414912835-A
Country	US
Kind code	B2
Filing date	Aug 20, 2014
Priority date	Aug 20, 2013
Publication date	Sep 12, 2017
Grant date	Sep 12, 2017

Abstract

Provided are a method of and a device for purifying isopropyl alcohol. Water may be effectively removed from a feed including water and isopropyl alcohol while consuming a minimum amount of energy, and therefore, a high-purity isopropyl alcohol may be obtained.

First claim

The invention claimed is:

1. A method for purifying isopropyl alcohol, comprising:
removing water by providing a feed including isopropyl alcohol and water to a membrane system to obtain a feed having a water content adjusted to 1,200 ppm or less; and performing purification by providing the feed having the water content adjusted to 1,200 ppm or less to a divided wall column to obtain a discharged product including purified isopropyl alcohol and having a water content of 150 ppm or less,
wherein the divided wall column is divided into a feed inflow region, a top region, a bottom region and a product outflow region, and the product outflow region is divided into an upper product outflow region and a lower product outflow region,
wherein the discharged product including the purified isopropyl alcohol and having a water content of 150 ppm or less is discharged from the lower product outflow region of the divided wall column, and
wherein the discharged product including the purified isopropyl alcohol and having a water content of 150 ppm or less is obtained at a location of 50 to 90% of plates among a number of theoretical plates calculated based on a top of the divided wall column.

2. The method according to claim 1 , wherein the membrane system is a pervaporation system or a vapor permeation system.

3. The method according to claim 1 , wherein the feed provided to the membrane system has a water content of 1,200 to 5,000 ppm.

4. The method according to claim 1 , wherein the temperature of the top region of the divided wall column is adjusted to 40 to 120° C.

5. The method according to claim 1 , wherein the pressure of the top region of the divided wall column is adjusted to 0.1 to 10.0 kg/cm 2 .

6. The method according to claim 4 , wherein the temperature of flow discharged from the lower product outflow region of the divided wall column is 60 to 130° C.

7. The method according to claim 5 , wherein the pressure of the lower product outflow region of the divided wall column is 0.3 to 6.0 kg/cm 2 .

8. The method according to claim 4 , wherein the temperature of the bottom region of the divided wall column is 80 to 160° C.

9. The method according to claim 5 , wherein the pressure of the bottom region of the divided wall column is 0.3 to 6.0 kg/cm 2 .

Assignees

• Lg Chemical Ltd

Inventors

• Park Jong Suh
• Lee Sung Kyu
• Shin Joon Ho
• Lee Jong Ku

Classifications

• B01D2311/2669

  Distillation · CPC title

• B01D61/362

  Pervaporation · CPC title

• C07C29/76 Primary

  by physical treatment · CPC title

• B01D3/145

  One step being separation by permeation · CPC title

• C07C31/10

  containing three carbon atoms · CPC title