Apparatus and method for measuring phase behavior

Patent metadata

Field	Value
Publication number	US-9752430-B2
Application number	US-201214346965-A
Country	US
Kind code	B2
Filing date	Jul 3, 2012
Priority date	Nov 8, 2011
Publication date	Sep 5, 2017
Grant date	Sep 5, 2017

Abstract

An apparatus for measuring phase behavior of a reservoir fluid comprises a first sample container and a second sample container in fluid communication with a microfluidic device defining a microchannel. A first pump and a second pump are operably associated with the sample containers and the microfluidic device to fill the microchannel with a reservoir fluid and to maintain a predetermined pressure of reservoir fluid within the microchannel.

First claim

What is claimed is:

1. An apparatus for measuring phase behavior of a reservoir fluid, comprising:
a microfluidic device defining an entrance passageway, an exit passageway, and a microchannel in fluid communication with the entrance passageway and the exit passageway;
a first sample container;
a first pump operably associated with the first sample container;
a second sample container;
a second pump operably associated with the second sample container;
an outlet valve fluidly coupled between the exit passageway of the microfluidic device and the second sample container;
a bypass line in fluid communication with the second sample container; and
an input switching valve fluidly coupled to the first sample container, the bypass line and the entrance passageway of the microfluidic device, wherein the input switching valve has a first configuration where reservoir fluid disposed in the first sample container is introduced from the first sample container into the entrance passageway of the microfluidic device while inhibiting the flow of the reservoir fluid through the bypass line, and wherein the input switching valve has a second configuration where reservoir fluid flows through the bypass line to the entrance passageway of the microfluidic device while reservoir fluid disposed in the first sample container does not flow into the entrance passageway of the microfluidic device;
wherein the first pump and the first configuration of the input switching valve are used to urge reservoir fluid disposed in the first sample container into the entrance passageway of the microfluidic device; and
wherein the second pump and the second configuration of the input switching valve are used to maintain a desired pressure within the microchannel of the microfluidic device.

2. The apparatus of claim 1 , wherein the microfluidic device comprises:
a first substrate defining the microchannel, an entrance well, and an exit well, the microchannel extending between and in fluid communication with the entrance well and the exit well; and
a second substrate attached to the first substrate to form the microfluidic device, the second substrate defining the entrance passageway in fluid communication with the entrance well and the exit passageway in fluid communication with the exit well.

3. The apparatus of claim 1 , further comprising:
an inlet pressure sensor configured to measure a pressure of the reservoir fluid urged into the entrance passageway of the microfluidic device; and
an outlet pressure sensor configured to measure a pressure of the reservoir fluid in the exit passageway of the microfluidic device.

4. The apparatus of claim 1 , further comprising a computer for operating the first pump and the second pump based at least upon a pressure of the reservoir fluid urged into the entrance passageway of the microfluidic device and a pressure of the reservoir fluid urged into the exit passageway of the microfluidic device.

5. The apparatus of claim 1 , further comprising a camera operably associated with the microfluidic device.

6. The apparatus of claim 1 , wherein:
the bypass line is fluidly coupled between the outlet valve and the input switching valve.

7. The apparatus of claim 1 , further comprising:
an inlet pressure sensor operably associated with the entrance passageway of the microfluidic device;
an outlet pressure sensor operably associated with the exit passageway of the microfluidic device;
a camera operably associated with the microfluidic device; and
a computer operably associated with the first pump, the inlet pressure sensor, the second pump, and the outlet pressure sensor for operating the first pump and the second pump to provide a desired pressure drop across the microchannel of the microfluidic device.

8. The apparatus of claim 7 , wherein the computer is operably associated with the camera for analyzing images of the microfluidic device.

9. The apparatus of claim 7 , further comprising a light source for illuminating the microfluidic device.

10. The apparatus of claim 7 , wherein:
the first pump and the first configuration of the input switching valve are used to inject a reservoir fluid into a microchannel of a microfluidic device at a pressure resulting in a substantially single phase in the reservoir fluid;
the second pump and the second configuration of the input switching valve are used to lower the pressure of the reservoir fluid in the microchannel until a second phase forms in the reservoir fluid; and
the camera and the computer are used to determine a distribution of the phases of the reservoir fluid in the microchannel.

11. The apparatus of claim 10 , wherein both the first pump and the second pump are operated to inject the reservoir fluid into the microchannel of the microfluidic device.

12. The apparatus of claim 11 , wherein the operations of the first pump and the second pump are controlled by a computer.

13. The apparatus of claim 11 , wherein the operations of the first pump and the second pump are controlled by using the inlet pressure sensor to monitor pressure of the reservoir fluid proximate the entrance passageway of the microfluidic device and by using the outlet pressure sensor to monitor pressure of the reservoir fluid proximate the exit passageway of the microfluidic device.

14. The apparatus of claim 10 , wherein the camera is configured to produce an image of the reservoir fluid in the microchannel.

15. The apparatus of claim 14 , wherein the computer is configured to analyze the image of the reservoir fluid in order to determine distribution of the phases of the reservoir fluid in the microchannel.

16. The apparatus of claim 14 , further comprising a light source that illuminates the microfluidic device.

17. The apparatus of claim 10 , wherein:
the second pump and the second configuration of the input switching valve are used to iteratively lower pressure of the reservoir fluid in the microchannel in predetermined steps; and
the camera and the computer are used to determine distribution of the phases of the reservoir fluid in the microchannel for each iteration.

18. The apparatus of claim 10 , wherein:
with the input switching valve in its second configuration, pressure of the reservoir fluid in the microfluidic device is controlled by operation of the second pump.

19. The apparatus of claim 10 , wherein:
the reservoir fluid is an oil, and the second phase is a gaseous phase.

20. The apparatus of claim 10 , wherein:
the reservoir fluid is a gas condensate, and the second phase is a liquid phase.

Assignees

• Mostowfi Farshid
• Molla Shahnawaz Hossain
• Schlumberger Technology Corp

Inventors

• Mostowfi Farshid
• Molla Shahnawaz Hossain

Classifications

• B81B2207/03

  Electronic circuits for micromechanical devices which are not application specific, e.g. for controlling, power supplying, testing, protecting · CPC title

• G01N35/1097

  characterised by the valves (valves in general F16K) · CPC title

• B01L2200/0673

  Handling of plugs of fluid surrounded by immiscible fluid · CPC title

• B01L2300/0816

  Cards, e.g. flat sample carriers usually with flow in two horizontal directions · CPC title

• B01L2400/0406

  capillary forces · CPC title