Electrostatic filtration of fine solids from bitumen

Patent metadata

Field	Value
Publication number	US-9752079-B2
Application number	US-201514853018-A
Country	US
Kind code	B2
Filing date	Sep 14, 2015
Priority date	Oct 14, 2014
Publication date	Sep 5, 2017
Grant date	Sep 5, 2017

Abstract

Methods are provided for removing fine particles from crude oils extracted from mined oil sands using a non-aqueous extraction solvent. A bitumen derived from non-aqueous extraction of oil from oil sands can undergo optional physical separation to remove larger particles and then processed using electrostatic filtration to remove particle fines. This can allow for production of a bitumen product from a non-aqueous extraction process that has a sufficiently low particle content to be suitable for pipeline transport.

First claim

What is claimed is:

1. A method for producing a bitumen product from oil sands, comprising:
extracting bitumen from oil sands with a non-aqueous extraction solvent to form a mixture of bitumen and extraction solvent;

performing a physical separation on at least a portion of the mixture of bitumen and extraction solvent to form at least a first filtered mixture of bitumen and extraction solvent;
separating at least a portion of the first filtered mixture of bitumen and extraction solvent to form a filtered bitumen stream and a filtered extraction solvent stream, the filtered bitumen stream containing at least about 0.25 wt % of non-petroleum particles; and
performing an electrostatic separation on at least a portion of the filtered bitumen stream to form a bitumen product containing about 1200 wppm or less of non-petroleum particles.

2. The method of claim 1 , wherein performing an electrostatic separation on at least a portion of the filtered bitumen stream comprises:
passing the at least a portion of the filtered bitumen stream into a separation volume of an electrostatic separator under effective electrostatic separation conditions, the effective electrostatic separation conditions including maintaining a separation voltage across the separation volume;
purging the separation volume with a purge fluid to form a purged portion of the bitumen product; and
washing the separation volume with the extraction solvent, a washing voltage across the separation volume during the washing being less than the separation voltage.

3. The method of claim 2 , wherein the performing of the electrostatic separation comprises a cyclic process, a second passing of at least a portion of the filtered bitumen stream being performed after the washing of the separation volume.

4. The method of claim 2 , the method further comprising removing the extraction solvent from the separation volume after the washing of the separation volume, the removing of the extraction solvent being performed with the purge fluid.

5. The method of claim 2 , wherein the washing voltage is 0, the washing voltage is a voltage produced by stopping power to at least one electrode associated with the separation volume, or a combination thereof.

6. The method of claim 2 , wherein at least a portion of the separation volume contains a solid dielectric material.

7. The method of claim 1 , further comprising diluting the bitumen product with a diluent, the diluent being different from the extraction solvent.

8. The method of claim 1 , further comprising adding water to the mixture of bitumen and extraction solvent prior to the performing of the physical separation.

9. The method of claim 1 , wherein the extraction solvent is cyclohexane.

10. The method of claim 1 , wherein the bitumen product is diluted with a naphtha boiling range stream, a kerosene boiling range stream, or a combination thereof.

11. The method of claim 1 , wherein the filtered bitumen stream contains at least about 0.5 wt % of non-petroleum particles, or at least about 1 wt %.

12. The method of claim 1 , wherein the extracting bitumen with the extraction solvent comprises extracting bitumen with a mixture of the extraction solvent and a recycled portion of the filtered bitumen stream.

13. The method of claim 1 , wherein the extracting bitumen with the extraction solvent comprises extracting bitumen with a mixture of the extraction solvent and a recycled portion of the first filtered mixture of bitumen and extraction solvent.

14. A method for producing a bitumen product from oil sands, comprising:
extracting bitumen from oil sands with a non-aqueous extraction solvent to form a mixture of bitumen and extraction solvent;
performing a physical separation on at least a portion of the mixture of bitumen and extraction solvent to form at least a first filtered mixture of bitumen and extraction solvent, the first filtered mixture of bitumen and extraction solvent containing at least about 0.25 wt % of non-petroleum particles;
performing an electrostatic separation on at least a portion of the first filtered mixture of bitumen and extraction solvent to form a filtered, separated mixture of bitumen and extraction solvent; and
separating at least a portion of the filtered, separated mixture of bitumen and extraction solvent to form a bitumen product and an extraction solvent stream, the bitumen product containing about 1200 wppm or less of non-petroleum particles.

15. The method of claim 14 , wherein performing an electrostatic separation on at least a portion of the first filtered mixture of bitumen and extraction solvent comprises:
passing the at least a portion of the first filtered mixture of bitumen and extraction solvent into a separation volume of an electrostatic separator under effective electrostatic separation conditions, the effective electrostatic separation conditions including maintaining a separation voltage across the separation volume;
purging the separation volume with a purge fluid to form a purged portion of the filtered, separated mixture of bitumen and extraction solvent; and
washing the separation volume with the extraction solvent, a washing voltage across the separation volume during the washing being less than the separation voltage.

16. The method of claim 15 , wherein the performing of the electrostatic separation comprises a cyclic process, a second passing of at least a portion of the first filtered mixture of bitumen and extraction solvent being performed after the washing of the separation volume.

17. The method of claim 15 , the method further comprising removing the extraction solvent from the separation volume after the washing of the separation volume, the removing of the extraction solvent being performed with the purge fluid.

18. The method of claim 15 , wherein the washing voltage is 0, the washing voltage is a voltage produced by stopping power to at least one electrode associated with the separation volume, or a combination thereof.

19. The method of claim 14 , wherein the extracting bitumen with the extraction solvent comprises extracting bitumen with a mixture of the extraction solvent and a recycled portion of the first filtered mixture of bitumen and extraction solvent.

20. The method of claim 14 , further comprising diluting the bitumen product with a diluent, the diluent being different from the extraction solvent.

Assignees

• Cullinane John Timothy
• Minhas Bhupender S
• Exxonmobil Upstream Res Co

Inventors

• Cullinane John Timothy
• Minhas Bhupender S

Classifications

• C10G1/045 Primary

  Separation of insoluble materials · CPC title

• C10G1/04

  by extraction · CPC title

• C10G32/02

  by electric or magnetic means · CPC title

• C10G1/002

  in combination with oil conversion- or refining processes · CPC title

• B03C7/02

  Separators · CPC title