Method and apparatus for testing gel-based lost circulation materials

Patent metadata

Field	Value
Publication number	US-9739694-B2
Application number	US-201514837741-A
Country	US
Kind code	B2
Filing date	Aug 27, 2015
Priority date	Aug 28, 2014
Publication date	Aug 22, 2017
Grant date	Aug 22, 2017

Abstract

A compression test rig apparatus for determining a mechanical characterization of a gel-based LCM test sample comprising an LCM test cell configured to contain the gel-based LCM test sample, the LCM test cell comprising a cylinder wall defining a cell space volume configured to hold the gel-based LCM test sample, and a floor defining an extrusion hole configured to extrude the gel-based LCM test sample to create an extruded gel; an extruded gel collector configured to receive the extruded gel from the extrusion hole as an extruded gel volume; a perforated disc comprising perforations, wherein the perforated disc is configured to allow the gel-based LCM test sample to pass through the perforations; and a flat foot disc piston in flush contact with the cylinder wall, the flat foot disc piston configured to compress the gel-based LCM test sample at a displacement speed to produce compression data.

First claim

What is claimed is:

1. A method for determining a mechanical characterization of a gel-based LCM using a compression test rig, the method comprising the steps of:
placing a gel-based LCM sample volume in a cell space volume of a LCM test cell of the compression test rig, the compression test rig comprising:
an LCM test cell, the LCM test cell configured to contain the gel-based LCM test sample, the LCM test cell comprising:
a cylinder wall, the cylinder wall defining the cell space volume, wherein the cell space volume is configured to contain the gel-based LCM test sample, and
a floor, the floor physically connected to the cylinder wall, the floor defining an extrusion hole, the extrusion hole having an extrusion hole diameter, the extrusion hole configured to extrude the gel-based LCM test sample to create an extruded gel,
wherein the gel-based LCM sample volume fills the cell space volume to a fill level;

an extruded gel collector, the extruded gel collector proximate to the floor of the LCM test cell, the extruded gel collector configured to receive the extruded gel from the extrusion hole as an extruded gel volume;
a perforated disc, the perforated disc in contact with the floor of the LCM test cell and flush with the cylinder wall, the perforated disc comprising perforations,
wherein the perforated disc is configured to allow the gel-based LCM test sample to pass through the perforations; and

a flat foot disc piston, the flat foot disc piston in flush contact with the cylinder wall of the LCM test cell, the flat foot disc piston configured to compress the gel-based LCM test sample contained in the cell space volume at a displacement speed to produce compression data;

placing the flat foot disc piston at the fill level in contact with the gel-based sample volume;
applying a load to the flat foot disc piston to move the flat foot disc toward the floor of the LCM test cell at a displacement speed,
wherein the flat foot disc compresses the gel-based LCM test sample contained in the cell space volume,
wherein the gel-based LCM test sample is compressed to a compressed level,
wherein a measured reactive force is produced in response to being compressed by the flat foot disc piston; and

measuring compression data with an acquisition system, the acquisition system in electronic communication with the LCM test cell, the acquisition system configured to record the compression data, the acquisition system further configured to display the compression data.

2. The method of claim 1 , further comprising the steps of:
generating the load in a normal stress applicator, the normal stress applicator mechanically connected to a load cell carrier arm, the normal stress applicator configured to generate the load, wherein the load is operable to be variable in order to maintain a constant displacement speed;
moving the load cell carrier arm, the load cell carrier arm mechanically connected to a piston rod, the load cell carrier arm configured to apply the load to the piston rod, the load cell carrier arm comprising a load cell, the load cell mechanically connected to the load carrier arm cell, the load cell configured to measure a measured reactive force of the gel-based LCM test sample, the load cell further configured to convert the measured reactive force into an electrical signal, wherein the electrical signal is recorded by the acquisition system, wherein the measured reactive force is produced in response to being compressed by the flat foot disc piston; and
moving the piston rod, the piston road mechanically connected to the flat foot disc piston, the piston rod is configured to move the flat foot disc piston between the fill level and the compressed level.

3. The method of claim 1 , the perforations comprising:
a central perforation, the central perforation in the center of the perforated disc, the central perforation having a central perforation diameter; and
a plurality of peripheral perforations, the plurality of peripheral perforations arranged in a ring around the central perforation to form a perforation ring, the perforation ring having a perforation ring diameter, the plurality of peripheral perforations having a peripheral perforation diameter.

4. The method of claim 1 , wherein the extrusion hole diameter is 3.3 cm.

5. The method of claim 1 , wherein the central perforation diameter is 3 mm.

6. The method of claim 1 , wherein the peripheral perforation diameter is 3 mm.

7. The method of claim 1 , wherein the perforation ring diameter is 2.6 cm.

8. The method of claim 1 , wherein the mechanical characterization is selected from the group consisting of yield strength, gel stiffness modulus, and combinations thereof.

9. The method of claim 1 , wherein the displacement speed is 1 mm/sec.

10. The method of claim 1 , wherein the compression data is selected from the group consisting of time, the extruded gel volume, the load, the measured reactive force, the fill level, the compressed level, and combinations thereof.

11. A compression test rig apparatus for determining a mechanical characterization of a gel-based LCM test sample, the compression test rig apparatus comprising:
an LCM test cell, the LCM test cell configured to contain the gel-based LCM test sample, the LCM test cell comprising:
a cylinder wall, the cylinder wall defining a cell space volume, wherein the cell space volume is configured to hold the gel-based LCM test sample, and
a floor, the floor being physically connected to the cylinder wall, the floor defining an extrusion hole, the extrusion hole having an extrusion hole diameter, the extrusion hole configured to extrude the gel-based LCM test sample to create an extruded gel;

an extruded gel collector, the extruded gel collector being proximate to the floor of the LCM test cell, the extruded gel collector configured to receive the extruded gel from the extrusion hole as an extruded gel volume;
a perforated disc, the perforated disc being in contact with the floor of the LCM test cell and flush with the cylinder wall, the perforated disc comprising perforations,
wherein the perforated disc is configured to allow the gel-based LCM test sample to pass through the perforations; and

a flat foot disc piston, the flat foot disc piston in flush contact with the cylinder wall of the LCM test cell, the flat foot disc piston configured to compress the gel-based LCM test sample contained in the cell space volume at a displacement speed to produce compression data.

12. The compression test rig apparatus of claim 11 further comprising:
an acquisition system, the acquisition system in electronic communication with the LCM test cell, the acquisition system configured to record the compression data, the acquisition system further configured to display the compression data.

13. The compression test rig apparatus of claim 11 further comprising:
a piston rod mechanically connected to the flat foot disc piston, configured to move the flat foot disc piston between a fill level and a compressed level;
a load cell carrier arm mechanically connected to the piston rod, the load cell carrier arm configured to apply a load to the piston rod, wherein the load is operable to be variable in order to maintain a constant displacement speed;
a load cell, the load cell mechanically connected to the load carrier arm, the load cell configured to measure a measured reactive force of the gel-based LCM test sample, the load cell further configured to convert the measured reactive force into an electrical signal, wherein the electrical signal is recorded by the acquisition system, wherein the measured reactive force is produced in response

Assignees

• Saudi Arabian Oil Co

Inventors

• Amanullah Md
• Alsubaie Turki Thuwaini Mohammed

Classifications

• G01N3/08 Primary

  by applying steady tensile or compressive forces (G01N3/28 takes precedence) · CPC title

• G01N3/12

  Pressure testing · CPC title

• G01N11/04

  through a restricted passage, e.g. tube, aperture · CPC title

• E21B21/003 Primary

  Means for stopping loss of drilling fluid (plastering the borehole wall E21B33/138) · CPC title

• C09K8/03

  Specific additives for general use in well-drilling compositions · CPC title