Micro-interface enhanced oxidation system and oxidation method for preparing hydrogen peroxide
US-12090458-B2 · Sep 17, 2024 · US
US9732400B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-9732400-B2 |
| Application number | US-201314406492-A |
| Country | US |
| Kind code | B2 |
| Filing date | Jun 10, 2013 |
| Priority date | Jun 19, 2012 |
| Publication date | Aug 15, 2017 |
| Grant date | Aug 15, 2017 |
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In an autoclave apparatus for a high-pressure acid leaching process which advances leaching by stirring heated and pressurized material slurry and sulfuric acid by stirrers in compartments in an autoclave main body of a plurality of compartments, transfers slurry from an upstream side compartment to a downstream one to advance leaching, liquid flow ports for slurry transfer that open and close by doors are provided on the partition walls, the liquid flow ports for slurry transfer are installed at positions where the heights from the lowermost portion the autoclave to the center of gravity are 0.1 to 0.3 times an autoclave diameter and distances from the center lines of the partition walls to the center of gravity are 0.05 to 0.25 times the autoclave diameter, and the liquid flow ports for slurry transfer have shapes which do not reach end portions of the partition walls.
Opening claim text (preview).
The invention claimed is: 1. An autoclave apparatus used during a high-pressure acid leaching process, the autoclave apparatus comprising: a cylindrical main body partitioned into a plurality of compartments by partition walls; stirrers provided in the respective compartments for transferring slurry from an upstream side compartment to a downstream side compartment to sequentially advance leaching; opening portions for a manway provided in bottom portions of each of the respective partition walls such that the opening portions do not reach end portions of the partition walls; and rectangular liquid flow ports for slurry transfer provided on manway doors of the respective opening portions, each liquid flow port having a liquid flow port door for opening or closing the liquid flow port, wherein the liquid flow ports are installed at positions where the heights from the lowermost portion of the autoclave to the center of gravity of the liquid flow port doors are 0.1 times to 0.3 times an autoclave diameter and distances from the longitudinal center lines of the partition walls to the center of gravity of the liquid flow port doors are 0.05 times to 0.25 times the autoclave diameter. 2. The autoclave apparatus according to claim 1 , wherein the liquid flow ports are provided on the manway doors at positions on the downstream side in the stirring direction of the slurry caused by the stirrer in the upstream side compartment. 3. The autoclave apparatus according to claim 1 , wherein the liquid flow ports for slurry transfer are rectangular openings with 30 cm square to 50 cm square.
Operations & Transport · mapped topic
Cross-Sectional Technologies · mapped topic
Stirrers (mixing per se B01F) · CPC title
vertical · CPC title
Baffles · CPC title
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