Complex structures in refractory bodies and methods of forming

Patent metadata

Field	Value
Publication number	US-9714729-B2
Application number	US-201214361829-A
Country	US
Kind code	B2
Filing date	Nov 29, 2012
Priority date	Nov 30, 2011
Publication date	Jul 25, 2017
Grant date	Jul 25, 2017

Abstract

A method of forming complex structures in a ceramic-, glass- or glass-ceramic-body microfluidic module is disclosed including the steps of providing at green-state refractory- material structure ( 140 ) comprising least a portion of a body of a microfluidic module, providing a removeable insert ( 120 ) formed of a carbon or of a carbonaceous material having an external surface comprising a negative surface ( 122 ) of a desired surface to be formed in the microfluidic module, machining an opening ( 132 ) in the green-state structure ( 140 ), positioning the insert ( 120 ) in the opening ( 132 ), firing the green-state structure ( 140 ) and the insert ( 120 ) together, and after firing is complete, removing the insert ( 120 ). The insert ( 120 ) is desirably a screw or screw shape, such that interior threads are formed thereby. The insert ( 120 ) desirably comprises graphite, and the structure desirably comprises ceramic, desirably silicon carbide.

First claim

What is claimed is:

1. A method of forming complex structures in a ceramic-, glass-or glass-ceramic-body microfluidic module, the method comprising the steps of:
providing a green-state refractory-material structure comprising least a portion of a body of a microfluidic module;
providing a removable insert formed of a carbon or of a carbonaceous material, an external surface of the insert comprising a negative surface of a desired surface to be formed in the microfluidic module;
machining an opening in the green-state structure;
positioning the insert in the opening, leaving an open volume between the external surface of the insert and an interior surface of the opening;
firing the green-state structure and the insert together;
during firing, closing the open volume; and
after firing is complete, removing the insert.

2. The method according to claim 1 wherein firing comprises firing in an inert atmosphere.

3. The method according to claim 1 , wherein removing comprises pyrolisis of the insert.

4. The method according to claim 1 , wherein removing comprises oxidation of the insert.

5. The method according to claim 1 , wherein the insert is a screw and wherein the complex structure comprises interior screw threads.

6. The method according to claim 5 further comprising removing the insert by unscrewing the insert.

7. The method according to claim 1 , wherein the step of providing a green-state structure comprises providing a structure comprising one or more of glass, glass-ceramic and ceramic.

8. The method according to claim 1 , wherein the step of providing a green-state structure comprises providing a structure comprising a ceramic.

9. The method according to claim 1 , wherein the step of providing a green-state structure comprises providing a structure comprising silicon carbide.

10. A method of forming complex structures in a ceramic-, glass- or glass-ceramic-body microfluidic module, the method comprising the steps of:
providing a green-state refractory-material structure comprising least a portion of a body of a microfluidic module;
providing a removable insert formed of a carbon or of a carbonaceous material, an external surface of the insert comprising a negative surface of a desired surface to be formed in the microfluidic module;
machining an opening in the green-state structure;
positioning the insert in the opening;
firing the green-state structure and the insert together;
after firing is complete, removing the insert, wherein an open volume between the negative surface of the insert and an inside surface of the opening is sufficiently small, and wherein a shrinkage of the green-state structure upon firing is sufficiently large, such that the open volume is closed during the firing process and such that said surface of the opening conforms to the negative surface of the insert.

Assignees

• Corning Inc

Inventors

• Marques Paulo Gaspar Jorge

Classifications

• B01J2219/00831

  Glass · CPC title

• B01J2219/00824

  Ceramic · CPC title

• B01J6/00

  Heat treatments such as} Calcining; Fusing {; Pyrolysis (furnaces F27D) · CPC title

• B01J19/0093 Primary

  Microreactors, e.g. miniaturised or microfabricated reactors (laboratory containers with capillary fluid transport in microfabricated channels or chambers B01L3/5027) · CPC title

• C04B35/64 Primary

  Burning or sintering processes (C04B33/32 takes precedence {; powder metallurgy B22F}) · CPC title