Method for preparing titanium nitride-titanium diboride-cubic boron nitride composite material

US9714198B2 · US · B2

Patent metadata
FieldValue
Publication numberUS-9714198-B2
Application numberUS-201415100857-A
CountryUS
Kind codeB2
Filing dateJun 27, 2014
Priority dateJun 9, 2014
Publication dateJul 25, 2017
Grant dateJul 25, 2017

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  1. Title

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  2. Abstract

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  4. Key dates

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  5. First independent claim

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Abstract

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A method for preparing a titanium nitride-titanium diboride-cubic boron nitride composite material is disclosed. Titanium powder and cubic boron nitride raw powders are mixed by a planetary ball milling method, and then the titanium nitride-titanium diboride-cubic boron nitride composite material is prepared through the steps of wet mixing, drying, sieving, pre-sintering through a high-temperature vacuum furnace, cold isostatic press molding and high-temperature sintering.

First claim

Opening claim text (preview).

The invention claimed is: 1. A method for preparing a titanium nitride-titanium diboride-cubic boron nitride composite material having a desired volume content of cubic boron nitride, cBN product, and using an in-situ reaction represented by the following formula (I): ( 1 - x ) ⁢ Ti + 2 + x 3 ⁢ c ⁢ BN → 2 ⁢ ( 1 - x ) 3 ⁢ Ti ⁢ N + ( 1 - x ) 3 ⁢ Ti ⁢ B 2 + x ⁢ c ⁢ BN , ( I ) wherein x is a mole fraction of cBN product in the composite material, the method comprising: (1) calculating weights of titanium, Ti powder and cBN powder to be used as raw materials in the reaction of formula (I) based on a desired volume content of cBN product in the composite material, and based on a desired total weight of Ti powder and cBN powder to be used as the raw materials in the reaction of formula (I), and according to the following formulas (II)-(V): V TiN = ( 1 - V cBN ) × ( 2 × M TiN ρ TiN 2 × M TiN ρ TiN + M TiB ⁢ ⁢ 2 ρ TiB ⁢ ⁢ 2 ) , ( II ) ; V TiB ⁢ ⁢ 2 = ( 1 - V cBN )

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Classifications

  • of calcined, sintered clinker or ceramics · CPC title

  • Treatment time · CPC title

  • Drying, e.g. freeze-drying, spray-drying, microwave or supercritical drying · CPC title

  • based on cubic boron nitrides {or Wurtzitic boron nitrides, including crystal structure transformation of powder} · CPC title

  • micrometer sized, i.e. from 1 to 100 micron · CPC title

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What does patent US9714198B2 cover?
A method for preparing a titanium nitride-titanium diboride-cubic boron nitride composite material is disclosed. Titanium powder and cubic boron nitride raw powders are mixed by a planetary ball milling method, and then the titanium nitride-titanium diboride-cubic boron nitride composite material is prepared through the steps of wet mixing, drying, sieving, pre-sintering through a high-temperat…
Who is the assignee on this patent?
Univ Hohai
What technology area does this patent fall under?
Primary CPC classification C04B35/5831. Mapped technology areas include Chemistry & Metallurgy.
When was this patent published?
Publication date Tue Jul 25 2017 00:00:00 GMT+0000 (Coordinated Universal Time) (B2). Legal status and post-grant events are not shown on this page.
What related patents are in patentsdb?
We list 1 related publication on this page (citations in our corpus or others sharing the same primary CPC).