Compositions of diamond particles having organic compounds attached thereto

Patent metadata

Field	Value
Publication number	US-9701877-B2
Application number	US-201514599213-A
Country	US
Kind code	B2
Filing date	Jan 16, 2015
Priority date	Apr 14, 2010
Publication date	Jul 11, 2017
Grant date	Jul 11, 2017

Abstract

A substance includes diamond particles having a maximum linear dimension of less than about 1 μm and an organic compound attached to surfaces of the diamond particles. The organic compound may include a surfactant or a polymer. A method of forming a substance includes exposing diamond particles to an organic compound, and exposing the diamond particles in the presence of the organic compound to ultrasonic energy. The diamond particles may have a maximum linear dimension of less than about 1 μm. A composition includes a liquid, a plurality of diamond nanoparticles dispersed within the liquid, and an organic compound attached to surfaces of the diamond nanoparticles. A method includes mixing a plurality of diamond particles with a solution comprising a liquid solvent and an organic compound, and exposing the mixture including the plurality of diamond nanoparticles and the solution to ultrasonic energy.

First claim

The invention claimed is:

1. A substance, comprising:
diamond particles comprising at least one functional group and having a maximum linear dimension of less than about 1 μm; and
an organic compound attached to surfaces of the functionalized diamond particles, the organic compound comprising at least one of a surfactant and a polymer, wherein the organic compound is selected from the group consisting of sodium laurel sulfate, 4-dodecylbenzenesulfonic acid, sodium dodecylbenzenesulfonate, sodium dodecylsulfonate, sodium alkyl allyl sulfosuccinate, polystyrene sulfonate, dodecyltrimethylammonium bromide, cetyltrimethylammonium bromide, polyoxyethylene (20) stearyl ether, polyethylene glycol 4400 octadecyl ether, sodium dodecyl sulfate, polyethylene glycol sorbitan monooleate, polyoxyethylenesorbitan trioleate, polyethylene glycol sorbitan monolaurate, 4-(1,1,3,3-tetramethylbutyl)phenyl-polyethylene glycol, polyethylene glycol tert-octylphenyl ether, poly(vinylpyrrolidone)-1300, a block copolymer based on ethylene oxide and 1,2-butylene oxide, and a block copolymer based on ethylene oxide and propylene oxide.

2. The substance of claim 1 , wherein the organic compound substantially covers outer surfaces of the functionalized diamond particles.

3. The substance of claim 1 , wherein the functionalized diamond particles comprise a non-diamond carbon-based outer shell.

4. The substance of claim 1 , wherein the functionalized diamond particles comprise agglomerates of diamond nanoparticles, the organic compound attached to surfaces of the agglomerates of functionalized diamond nanoparticles.

5. The substance of claim 1 , wherein the functionalized diamond nanoparticles have an average maximum linear dimension of less than about 200 nm.

6. The substance of claim 1 , wherein a ratio of an average maximum linear dimension of the functionalized diamond particles to an average minimum linear dimension of the functionalized diamond particles is greater than about 100.

7. A composition, comprising:
a liquid;
a plurality of diamond nanoparticles comprising at least one functional group dispersed within the liquid; and
an organic compound, the organic compound comprising at least one of a surfactant and a polymer attached to surfaces of the functionalized diamond nanoparticles, wherein the organic compound is selected from the group consisting of sodium laurel sulfate, 4-dodecylbenzenesulfonic acid, sodium dodecylbenzenesulfonate, sodium dodecylsulfonate, sodium alkyl allyl sulfosuccinate, polystyrene sulfonate, dodecyltrimethylammonium bromide, cetyltrimethylammonium bromide, polyoxyethylene (20) stearyl ether, polyethylene glycol 4400 octadecyl ether, sodium dodecyl sulfate, polyethylene glycol sorbitan monooleate, polyoxyethylenesorbitan trioleate, polyethylene glycol sorbitan monolaurate, 4-(1,1,3,3-tetramethylbutyl)phenyl-polyethylene glycol, polyethylene glycol tert-octylphenyl ether, poly(vinylpyrrolidone)-1300, a block copolymer based on ethylene oxide and 1,2-butylene oxide, and a block copolymer based on ethylene oxide and propylene oxide.

8. The composition of claim 7 , wherein the liquid comprises a solution including a solvent and the organic compound, the solvent selected from the group consisting of water, an oil, an alcohol, a glycol, an acid, an aldehyde, a ketone, an amide, an amine, and combinations thereof.

9. The composition of claim 8 , wherein the solvent comprises a solvent selected from the group consisting of methylethylketone, methyletherketone, tetrahydrofuran, dimethylformamide, and sulfuric acid.

10. The composition of claim 8 , wherein from about 0.1 wt % to about 40 wt % of the solution is comprised by the organic compound.

11. The composition of claim 8 , wherein the solvent comprises water.

12. The composition of claim 7 , wherein the plurality of functionalized diamond nanoparticles and the liquid form a suspension.

13. The composition of claim 7 , wherein the plurality of functionalized diamond nanoparticles and the liquid form a slurry.

14. The composition of claim 7 , wherein the functionalized diamond nanoparticles of the plurality have an average maximum linear dimension of less than about 200 nm.

15. The composition of claim 7 , wherein the functionalized diamond nanoparticles of the plurality comprise a plurality of agglomerates of functionalized diamond nanoparticles, the organic compound attached to surfaces of the agglomerates of functionalized diamond nanoparticles.

16. The substance of claim 4 , wherein the agglomerates of functionalized diamond nanoparticles comprise functionalized diamond nanoparticles having a maximum linear dimension in a range extending from about 4 nm to about 6 nm.

17. The substance of claim 16 , wherein the agglomerates have maximum linear dimensions in a range extending from about 10 nm to about 400 nm.

Assignees

• Baker Hughes Inc

Inventors

• Chakraborty Soma
• Agrawal Gaurav
• Digiovanni Anthony A

Classifications

• B24D99/005

  Segments of abrasive wheels · CPC title

• B01J2203/0655

  Diamond · CPC title

• B01J2203/0685

  Crystal sintering · CPC title

• B82Y30/00

  Nanotechnology for materials or surface science, e.g. nanocomposites · CPC title

• B01J2203/062

  Diamond · CPC title