Gas diffusion system and method for introducing a gas stream in an apparatus, in particular a passivating gas stream in a urea plant

Patent metadata

Field	Value
Publication number	US-9694334-B2
Application number	US-201414902814-A
Country	US
Kind code	B2
Filing date	Jul 4, 2014
Priority date	Jul 5, 2013
Publication date	Jul 4, 2017
Grant date	Jul 4, 2017

Abstract

A gas diffusion system configured to feed a gas stream, in particular a passivating gas stream, into an apparatus, in particular a decomposer, of a urea plant; the system extends along an axis and has a gas feed conduit having an outlet from which the gas flows substantially parallel to the axis, and a diffuser assembly configured to diffuse the gas supply from the conduit; the diffuser assembly is shaped so as to intercept the gas stream flowing axially from the outlet, and divert the gas stream substantially radially with respect to the axis and uniformly about the axis.

First claim

The invention claimed is:

1. A urea plant decomposer with a gas diffusion system configured to feed a passivating gas stream into the urea plant decomposer extending along an axis, said urea plant decomposer comprising:
a bottom holder which defines a chamber, said bottom holder including:
a bottom portion of a casing,
a bottom catch portion closed at a bottom end by a bottom wall, and having a substantially cylindrical lateral wall around the axis, and
a funnel-shaped top diffusion portion which flares upwards, tapers towards the bottom catch portion and is bounded by a truncated-cone-shaped lateral wall around the axis;

a gas feed conduit including:
a base pipe transverse to the substantially cylindrical lateral wall and the axis, and
a fitting which terminates with an opening defining an outlet which is transverse to the axis and from which the passivating gas stream flows substantially parallel to the axis, said outlet being located centrally inside the bottom holder and the defined chamber substantially about the axis, wherein said gas feed conduit projects inside the chamber from an inlet hole formed through the substantially cylindrical lateral wall of the bottom catch portion and said gas feed conduit terminates with said outlet; and

a diffuser assembly including a central diffuser and a peripheral shield which are spaced axially apart along the axis and offset radially with respect to each other, wherein the peripheral shield includes an annular member positioned about the axis and defining a plurality of through peripheral openings, angularly spaced apart from one another and uniformly distributed around the axis, and the diffuser assembly is configured to diffuse the passivating gas stream from the gas feed conduit inside the chamber, said diffuser assembly being shaped to:
intercept the passivating gas stream flowing axially from the outlet, and
divert the passivating gas stream substantially radially with respect to the axis and about the axis.

2. The urea plant decomposer of claim 1 , wherein the diffuser assembly defines a plurality of gas outlet openings arranged about the axis.

3. The urea plant decomposer of claim 2 , wherein at least two of the plurality of gas outlet openings are at different distances from the axis.

4. The urea plant decomposer of claim 2 , wherein the gas outlet openings define slots elongated longitudinally in a first direction.

5. The urea plant decomposer of claim 1 , wherein the annular member has a radially inner peripheral edge and a radially outer peripheral edge which define a plurality of peripheral slots spaced angularly apart and defining the peripheral openings.

6. The urea plant decomposer of claim 1 , wherein the annular member tapers upwards from the radially outer peripheral edge to the radially inner peripheral edge.

7. The urea plant decomposer of claim 1 , wherein the fitting projects perpendicularly from the base pipe.

8. The urea plant decomposer of claim 7 , wherein the gas feed conduit is substantially T-shaped.

9. The urea plant decomposer of claim 1 , wherein the base pipe includes at least two portions of at least one of: different cross sections to one another and eccentric with respect to one another.

10. The urea plant decomposer of claim 1 , wherein the diffuser assembly defines at least one drain hole formed in one or more bottom end portions of the diffuser assembly to drain off any liquid penetrating the diffuser assembly.

11. The urea plant decomposer of claim 1 , wherein the diffuser assembly includes at least one support which axially supports and angularly locks the diffuser assembly, said support including a bracket which defines a seat which receives a bottom end portion of the diffuser assembly resting axially on the bracket, inside the seat, the diffuser assembly having at least one fastener having two downward-facing lateral shoulders which cooperate with respective lateral edges of the seat.

12. The urea plant decomposer of claim 11 , wherein the seat defines at least one drain hole formed through the bracket at the bottom of the seat to drain off any liquid collecting inside the seat.

13. The urea plant decomposer of claim 1 , wherein the base pipe is perpendicular to the substantially cylindrical lateral wall and the axis.

14. The urea plant decomposer of claim 1 , wherein the outlet is perpendicular to the axis.

15. The urea plant decomposer of claim 1 , wherein said diffuser assembly is shaped to divert the passivating gas stream uniformly about the axis.

16. A urea plant decomposer with a gas diffusion system configured to feed a passivating gas stream into the urea plant decomposer extending along an axis, said urea plant decomposer comprising:
a bottom holder which defines a chamber, said bottom holder including:
a bottom portion of a casing, a bottom catch portion closed at a bottom end by a bottom wall, and
having a substantially cylindrical lateral wall around the axis, and
a funnel-shaped top diffusion portion which flares upwards, tapers towards the bottom catch portion and is bounded by a truncated-cone-shaped lateral wall around the axis;
a gas feed conduit including:
a base pipe transverse to the substantially cylindrical lateral wall and the axis, and
a fitting which terminates with an opening defining an outlet which is transverse to the axis and from which the passivating gas stream flows substantially parallel to the axis, said outlet being located centrally inside the bottom holder and the defined chamber substantially about the axis, wherein said gas feed conduit projects inside the chamber from an inlet hole formed through the substantially cylindrical lateral wall of the bottom catch portion and said gas feed conduit terminates with said outlet; and
a diffuser assembly including a central diffuser located over the outlet of the gas feed conduit, said central diffuser being aligned with the outlet along the axis and defining a plurality of radial gas outlet openings uniformly spaced about the axis, wherein the diffuser assembly is configured to diffuse the passivating gas stream from the gas feed conduit inside the chamber, said diffuser assembly being shaped to:
intercept the passivating gas stream flowing axially from the outlet, and divert the passivating gas stream substantially radially with respect to the axis and about the axis, wherein the central diffuser is associated with a distributor connected to the gas feed conduit to receive the passivating gas stream from the outlet of the gas feed conduit, said distributor being shaped to distribute at least part of the oncoming passivating gas stream radially to the central diffuser.

17. The urea plant decomposer of claim 16 , wherein the central diffuser is positioned crosswise to the axis to obstruct the outlet from above and stop the passage of the passivating gas stream exiting from the outlet along the axis.

18. The urea plant decomposer of claim 16 , wherein the central diffuser includes a dome-shaped hood having a peripheral edge spaced axially apart from the outlet and radially outwards with respect to the outlet.

19. The urea plant decomposer of claim 16 , wherein the distributor is an axial distributor extending along or parallel to the axis, said axial distributor receives the passivating gas stream from the gas feed conduit along the axis.

20. The urea plant decomposer of claim 19 , wherein the axial distributor includes a tubular member extending along the axis and defining a plurality of longitudinal slits formed through a lateral wal

Assignees

• Saipem Spa

Inventors

• Minola Paolo

Classifications

• C07C273/02

  of urea, its salts, complexes or addition compounds · CPC title

• B01F2003/04304

  Operations & Transport · mapped topic

• B01J2219/24

  Stationary reactors without moving elements inside · CPC title

• B01J4/002 Primary

  Nozzle-type elements (nozzle-type reactors B01J19/26) · CPC title

• B01J19/24

  Stationary reactors without moving elements inside (B01J19/08, B01J19/26 take precedence; with stationary particles B01J8/02) · CPC title