Personal care compositions and methods

Patent metadata

Field	Value
Publication number	US-9687425-B2
Application number	US-201514755507-A
Country	US
Kind code	B2
Filing date	Jun 30, 2015
Priority date	Jun 30, 2014
Publication date	Jun 27, 2017
Grant date	Jun 27, 2017

Abstract

Methods of making personal care compositions including microcapsules and methods of enhancing the efficacy of the microcapsules in said personal care compositions.

First claim

What is claimed is:

1. A method of manufacturing an anhydrous antiperspirant composition, the method comprising:
combining a first process stream at a first temperature and a second process stream at a second temperature, wherein the first process stream comprises a structurant, a solvent, or combinations thereof; and the second process stream comprises an antiperspirant active and a plurality of microcapsules; wherein the second temperature does not exceed 80° C.

2. The method of claim 1 , wherein the second temperature is less than about 75° C.

3. The method of claim 1 , wherein the second temperature is less than about 70° C., less than about 60° C., or less than about 50° C.; but greater than 0° C.

4. The method of claim 1 , wherein the second temperature is from about 20° C. to about 40 ° C.

5. The method of claim 4 , wherein the second process stream further comprises a material selected from the group consisting of a fragrance, an anhydrous liquid carrier, and combinations thereof.

6. The method of claim 5 , wherein the second process stream further comprises a volatile silicone.

7. The method of claim 6 , wherein the microcapsules are spray-dried before inclusion into the second process stream.

8. The method of claim 6 , wherein the second process stream further comprises a malodor reducing agent, a moisture-triggered fragrance technology, or combinations thereof.

9. The method of claim 6 , wherein the second process stream further comprises a moisture-triggered fragrance technology selected from the group consisting of cyclic oligosaccharides, starches, polysaccharide-based encapsulation systems, and combinations thereof.

10. The method of claim 1 , wherein the second process stream further comprises a malodor reducing agent selected from the group consisting of pantothenic acid, petrolatum, menthyl acetate, uncomplexed cyclodextrin, complexed cyclodextrin, talc, silica, and combinations thereof.

11. The method of claim 5 , wherein the microcapsules comprise a core material and a shell; wherein the core material comprises a fragrance.

12. The method of claim 11 , wherein the core material further comprises an oil soluble material selected from the group consisting of mono, di- and tri-esters of C 4 -C 24 fatty acids and glycerine; butyl oleate; hydrogenated castor oil; castor oil; mineral oil; capryllic triglyceride; vegetable oil; geranyl palmitate; silicone oil; isopropryl myristate; soybean oil; hexadecanoic acid; methyl ester; isododecane; and combinations thereof.

13. The method of claim 11 , the shell comprises a material selected from the group consisting of polyacrylates; polyethylenes; polyamides; polystyrenes; polyisoprenes; polyc arbonates; polyesters; polyureas; polyurethanes; polyolefins; polysaccharides; epoxy resins; vinyl polymers; urea cross-linked with formaldehyde or gluteraldehyde; melamine cross-linked with formaldehyde; gelatin-polyphosphate coacervates optionally cross-linked with gluteraldehyde; gelatin-gum Arabic coacervates; cross-linked silicone fluids; polyamine reacted with polyisocyanates; acrylate monomers polymerized via free radical polymerization; silk; wool; gelatin; cellulose; proteins; and combinations thereof.

14. The method of claim 11 , wherein the shell comprises a reaction product of a first mixture in the presence of a second mixture comprising an emulsifier, the first mixture comprising a reaction product of i) an oil soluble or dispersible amine with ii) a multifunctional acrylate or methacrylate monomer or oligomer, an oil soluble acid and an initiator, the emulsifier comprising a water soluble or water dispersible acrylic acid alkyl acid copolymer, an alkali or alkali salt, and optionally a water phase initiator.

15. The method of claim 14 , wherein the amine comprises aminoalkyl acrylate or aminoalkyl methacrylate.

16. The method of claim 14 , wherein said amine is a diethylaminoethyl methacrylate, dimethylaminoethyl methacrylate, or tertiarybutyl aminoethyl methacrylate.

17. The method of claim 1 , wherein the anhydrous personal care composition is selected from the group consisting of a soft-solid antiperspirant, and an invisible solid antiperspirant.

18. The method of claim 1 , the method further comprises mixing the microcapsules with at least one of an anhydrous liquid carrier and gelling agent prior to incorporation into the second process stream.

19. The method of claim 1 , wherein the microcapsules are in the form of a powder with a water content of less than 15% by weight of the powder when the microcapsules are added to the second process stream.

Assignees

• Procter & Gamble

Inventors

• Cetti Jonathan Robert
• Dihora Jiten Odhavji
• Witt Steven Edward
• Henley Eric Shane

Classifications

• A61K2800/592

  Mixtures of compounds complementing their respective functions · CPC title

• A61K2800/805

  Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95 · CPC title

• A61K8/37

  Esters of carboxylic acids · CPC title

• A61K2800/412

  Microsized, i.e. having sizes between 0.1 and 100 microns · CPC title

• A61K8/8152

  Homopolymers or copolymers of esters, e.g. (meth)acrylic acid esters; Compositions of derivatives of such polymers · CPC title