Ultra dense and ultra low power microhotplates using silica aerogel and method of making the same

Patent metadata

Field	Value
Publication number	US-9674896-B2
Application number	US-201414470328-A
Country	US
Kind code	B2
Filing date	Aug 27, 2014
Priority date	Aug 28, 2013
Publication date	Jun 6, 2017
Grant date	Jun 6, 2017

Abstract

An ultra dense and ultra low power microhotplates using silica aerogel and method of making the same, comprising spin coating an aerogel layer followed by SiO 2 as capping interlayer, and Nichrome (Ni 80 /Cr 20 ) for heating element to increase the efficiency of metal oxide gas sensors. There may be multiple thin layers of aerogel separated by interlayers such as of SiO 2 .

First claim

The invention claimed is:

1. A method of making silica aerogel thin and thick films comprising:
a. mixing tetraethyl orthosilicate, ethanol, water and HCl with the molar ratio of approximately 1:4:2:4.3×10 −4 , respectively to form a first solution;
b. stirring said first solution for approximately one hour;
c. adding approximately 0.64 ml. of 0.066 M NH 4 OH to create a second solution;
d. stirring said second solution for approximately 5 minutes to create a sol-gel mixture;
e. aspirating the sol-gel mixture with an aspirator at approximately 15% of gelation time;
f. spraying said the sol-gel mixture onto a column of ethanol to create an impregnated ethanol mixture;
g. aging said impregnated ethanol mixture at room temperature for approximately 24 hours;
h. ultrasounding said impregnated ethanol mixture for approximately 8 minutes;
i. filtering said impregnated ethanol mixture with a 0.2 micrometer filter, resulting in a filtered impregnated ethanol mixture; and
j. spin coating said filtered impregnated ethanol mixture onto the wafer for 40 seconds at approximately 1150 RPM, creating a first aerogel layer.

Assignees

• Univ Louisiana At Lafayette
• The Univ Of Louisiana At Lafayette

Inventors

• Madani Mohammad Reza
• Seyedjalaliaghdam Seyedmohammad

Classifications

• H05B3/10 Primary

  Heating elements characterised by the composition or nature of the materials or by the arrangement of the conductor · CPC title

• B05D1/005

  Spin coating · CPC title

• B05D5/00

  Processes for applying liquids or other fluent materials to surfaces to obtain special surface effects, finishes or structures · CPC title

• B05D3/007

  After-treatment · CPC title

• H05B3/22

  non-flexible · CPC title