Methods and systems for removing undissolved solids prior to extractive fermentation in the production of butanol

Patent metadata

Field	Value
Publication number	US-9670511-B2
Application number	US-201313874737-A
Country	US
Kind code	B2
Filing date	May 1, 2013
Priority date	Jun 18, 2010
Publication date	Jun 6, 2017
Grant date	Jun 6, 2017

Abstract

A method and system for efficiently producing a fermentative product alcohol such as butanol utilizing in situ product extraction are provided. The efficiency is obtained through separating undissolved solids after liquefying a given feedstock to create a feedstock and prior to fermentation, for example, through centrifugation. Removal of the undissolved solids avoids problems associated with having the undissolved solids present during in situ production extraction, and thereby increases the efficiency of the alcohol production.

First claim

What is claimed is:

1. A system for producing a product alcohol comprising:
a liquefaction vessel configured to liquefy a feedstock to create a feedstock slurry, the liquefaction vessel comprising:
an inlet for receiving the feedstock; and
an outlet for discharging a feedstock slurry, wherein the feedstock slurry comprises sugar, oil, and undissolved solids;

one or more three-phase centrifuges configured to separate the feedstock slurry to form separate streams: (i) an aqueous solution comprising the sugar, (ii) a wet cake comprising the undissolved solids, and (iii) an oil stream, wherein the three-phase centrifuge comprises:
an inlet for receiving the feedstock slurry;
a first outlet for discharging the aqueous solution;
a second outlet for discharging the wet cake; and
a third outlet for discharging the oil stream;

one or more fermentors configured to ferment the aqueous solution to produce the product alcohol, the fermentor comprising:
a first inlet for receiving the aqueous solution; and
a first outlet for discharging fermentation broth; and

a distillation column and a hydrolyzer, wherein the bottoms of the distillation column are added to a feed of the hydrolyzer.

2. The system of claim 1 , further comprising a saccharification vessel configured to saccharify the sugar in the feedstock slurry, the saccharification vessel comprising:
an inlet for receiving the feedstock slurry or aqueous solution; and
an outlet for discharging the feedstock slurry.

3. The system of claim 1 , further comprising a dry mill configured to grind the feedstock, the dry mill comprising:
an inlet for receiving the feedstock; and
an outlet for discharging ground feedstock.

4. The system of claim 1 , wherein the product alcohol is methanol, ethanol, propanol, butanol, pentanol, or isomers thereof.

5. The system of claim 4 , wherein the butanol isomer is 1-butanol, 2-butanol, or isobutanol.

6. The system of claim 1 , further comprising one or more of the following: decanter bowl centrifuge, disk stack centrifuge, filtering centrifuge, decanter centrifuge, filtration, vacuum filtration, beltfilter, pressure filtration, filtration using a screen, screen separation, grating, porous grating, flotation, hydroclone, filter press, screwpress, gravity settler, vortex separator, or combinations thereof.

7. The system of claim 1 , wherein the fermentor further comprises
a second inlet for receiving an extractant; and
a second outlet for discharging the extractant rich with product alcohol.

8. The system of claim 1 , further comprising a rectifier column wherein the rectifier column serves a solvent column.

9. The system of claim 1 , further comprising a multiple effect evaporator.

10. The system of claim 9 , wherein the multiple effect evaporator has a configuration of four bodies by two effects or a configuration of three bodies by three effects.

11. The system of claim 1 , further comprising an extraction vessel.

12. The system of claim 1 , further comprising one or more of the following: preflash column, reboiler, heat exchanger, decanter, mixer, or distillers grain dryer.

13. The system of claim 12 , wherein the preflash column is a retrofit of a beer column.

Assignees

• Butamax Advanced Biofuels Llc

Inventors

• Roesch Brian Michael
• Burlew Keith H
• Hallam John W
• Lowe David J
• Zaher Joseph J

Classifications

• C11B13/00

  Recovery of fats, fatty oils or fatty acids from waste materials · CPC title

• C12M1/00

  Apparatus for enzymology or microbiology · CPC title

• C12P7/6418

  by hydrolysis of fatty acid esters · CPC title

• Y02W30/74

  Recovery of fats, fatty oils, fatty acids or other fatty substances, e.g. lanolin or waxes · CPC title

• C12M45/04

  Phase separators; Separation of non fermentable material; Fractionation · CPC title