High-throughput sorting of small objects via oil and/or moisture content using low-field nuclear magnetic resonance

Patent metadata

Field	Value
Publication number	US-9658176-B2
Application number	US-201414206238-A
Country	US
Kind code	B2
Filing date	Mar 12, 2014
Priority date	Mar 15, 2013
Publication date	May 23, 2017
Grant date	May 23, 2017

Abstract

The current disclosure describes an automated high-throughput small object sorting system for separating small object via oil and/or moisture content using novel nuclear magnetic resonance (NMR) systems and methods. The disclosed systems and methods for measuring the oil and/or moisture content of a single small object in a low-field time domain NMR instrument are superior in sample throughput and signal-to-noise ratio to conventional NMR systems and methods (free induction decay or spin echo) for single small object oil/moisture measurement.

First claim

What is claimed is:

1. A high throughput dynamic small object sorting system, said system comprising:
a conveyor assembly including a small object conveyor belt having a plurality of small object cups attached thereto, the conveyor assembly structured and operable to continuously move the conveyor belt at a selected constant rate of speed during operation of the system;
a small object feeder assembly structured and operable to singulate small objects from a plurality of small objects and deposit each singulated small object into a respective one of the small object cups as the conveyor belt continuously moves at the selected constant rate of speed;
a nuclear magnetic resonance (NMR) assembly having the conveyor belt operably extending therethrough, the NMR assembly structure and operable to generate at least one of oil and moisture mass data for each small object as each small object moves through the NMR assembly at the selected constant rate of speed;
a microwave resonance cavity structured and operable to receive and have pass therethrough, without pause, each small object after each respective small object has been conveyed through the NMR assembly and to obtain total small object mass data for each respective small object; and
a computer based central control system structured and operable to:
receive the at least one of oil and moisture mass data from the NMR assembly for each small object,
receive the total small object mass from the microwave resonance cavity for each small object, and
execute oil/moisture content software to:
store the at least one of oil and moisture mass data for each small object and associate the at least one of oil and moisture mass data received for each small object with the respective small object,
store the total small object mass data for each small object and associate the total small object mass data for each small object with the respective small object; and
based on the at least one of oil and moisture mass and total mass data for each small object, compute an oil/moisture content value for each respective small object within a time period dictated by the selected constant rate of speed of the conveyor belt.

2. The system of claim 1 , further comprising a diverter assembly structured and operable to receive the small objects from the microwave resonance cavity and, via commands from the central control system, separate the small objects based on the computed oil/moisture content of each respective small object.

3. The system of claim 1 , wherein the selected rate of speed is approximately one meter per second.

4. The system of claim 1 , wherein the NMR assembly comprises:
an NMR rexlameter structured and operable to exert a magnetic force on each small object passing through the NMR assembly; and
a radio frequency (RF) probe structured and operable to generate a plurality of pulses and receive an echo from each pulse from which the at least one of oil and moisture mass data is generated.

5. The system of claim 4 , wherein the number of pulses generated each millisecond is such that noise generated by each pulse cancels the noise of subsequent pulses, thereby increasing the signal-to-noise ratio of NMR measurement during determination of the at least one of oil and moisture mass data.

6. The system of claim 5 , wherein the number of pulses generated each millisecond is approximately five pulses per millisecond.

7. The system of claim 1 further comprising a stray small object removal assembly structured and operable to remove stray small object that are not retained within a small object cup from the conveyor belt.

8. The system of claim 1 , wherein each small object cup comprises a reservoir into which each respective small object is deposited by the small object feeder assembly and a plurality of serrations through a body of small object cup, the reservoir and serrations structured and operable to center and reduce vibration of each small object within the respective small object cup and retain each small object in a stable orientation within the respective small object cup as each small object is conveyed through the NMR assembly.

9. The system of claim 1 , where each small object comprises a seed.

10. A method for high throughput dynamic small object sorting, said method comprising:
continuously moving a conveyor belt having a plurality of small object cups attached thereto at a selected constant rate of speed, the conveyor belt included in a conveyor assembly of high throughput dynamic small object sorting system;
singulating small objects from a plurality of small objects and depositing each singulated small object into a respective one of the small object cups as the conveyor belt continuously moves at the selected constant rate of speed, utilizing a small object feeder assembly of the high throughput dynamic small object sorting system;
generating at least one of oil and moisture mass data for each small object as each small object moves through a nuclear magnetic resonance (NMR) assembly at the selected constant rate of speed, the NMR assembly included in the high throughput dynamic small object sorting system and having the conveyor belt operably extending therethrough;
obtaining total small object mass data for each respective small object by passing each small object through a microwave resonance cavity, without pause, after each small object has been conveyed through the NMR assembly, the microwave resonance cavity included in the high throughput dynamic small object sorting system; and
executing oil/moisture content software, utilizing a computer based central control system of the high throughput dynamic small object sorting system, to:
store at least one of oil mass and moisture data received from the NMR assembly for each small object and associate the at least one of oil and moisture mass data received for each small object with the respective small object,
store total small object mass data received from the microwave resonance cavity for each small object and associate the total small object mass data for each small object with the respective small object; and
based on the at least one of oil and moisture mass, and the total mass data for each small object, compute an at least one of oil and moisture content value for each respective small object within a time period dictated by the selected constant rate of speed of the conveyor belt.

11. The method of claim 10 , further comprising:
receiving the small objects from the microwave resonance cavity in a diverter assembly of the high throughput dynamic small object sorting system; and
via commands from the central control system, separating the small objects based on the computed at least one of oil and moisture content of each respective small object via the divert assembly.

12. The method of claim 10 , wherein generating the at least one of oil and moisture mass data for each small object as each small object moves through the NMR assembly at the selected constant rate of speed comprises generating the at least one of oil and moisture mass data for each small object as each small object moves through the NMR assembly at approximately one meter per second.

13. The method of claim 10 , generating the at least one of oil and moisture mass data for each small object as each small object moves through the NMR assembly at the selected constant rate of speed comprises:
exerting a magnetic force on each small object passing through the NMR assembly utilizing an NMR rexlameter of the NMR assembly; and
generating a plurality of radio frequency (RF) pulses utilizing an RF probe of the NMR assembly;
receiving an echo from each pulse uti

Assignees

• Monsanto Technology Llc

Inventors

• Dai Bin
• Macisaac Susan
• Deppermann Kevin L
• Ehrhardt Mark
• White Brad
• Brown Wayne
• Krasucki Paul
• Mcdonald Jemmi C

Classifications

• G01N24/08 Primary

  by using nuclear magnetic resonance (G01N24/12 takes precedence) · CPC title

• G01R33/448

  Relaxometry, i.e. quantification of relaxation times or spin density (G01R33/50 takes precedence) · CPC title

• G01R33/307

  specially adapted for moving the sample relative to the MR system, e.g. spinning mechanisms, flow cells or means for positioning the sample inside a spectrometer · CPC title

• G01R33/445

  MR involving a non-standard magnetic field B0, e.g. of low magnitude as in the earth's magnetic field or in nanoTesla spectroscopy, comprising a polarizing magnetic field for pre-polarisation, B0 with a temporal variation of its magnitude or direction such as field cycling of B0 or rotation of the direction of B0, or spatially inhomogeneous B0 like in fringe-field MR or in stray-field imaging · CPC title

• G01R33/561

  by reduction of the scanning time, i.e. fast acquiring systems, e.g. using echo-planar pulse sequences · CPC title