Method for manufacturing an electrochemical component comprising a lithium metal anode and an ion-conductive inorganic material layer
US-2024234676-A9 · Jul 11, 2024 · US
US9657387B1 · US · B1
| Field | Value |
|---|---|
| Publication number | US-9657387-B1 |
| Application number | US-201615140822-A |
| Country | US |
| Kind code | B1 |
| Filing date | Apr 28, 2016 |
| Priority date | Apr 28, 2016 |
| Publication date | May 23, 2017 |
| Grant date | May 23, 2017 |
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Methods are provided for forming a thermal barrier coating system on a surface of a component. The method can include introducing the component into a coating chamber, where a first ceramic source material and a second ceramic source material are positioned within the coating chamber of a physical vapor deposition apparatus. An energy source is directed onto the first ceramic source material to vaporize the first ceramic source material to deposit a first layer on the component. The energy source is alternated between the first ceramic source material and the second ceramic source material to form a blended layer on the first layer.
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What is claimed is: 1. A method of forming a thermal barrier coating system on a surface of a component, the thermal barrier coating system comprising a thermal barrier coating that has columnar grains, the method comprising: introducing the component into a coating chamber, wherein a first ceramic source material and a second ceramic source material are positioned within the coating chamber of a physical vapor deposition apparatus; directing an energy source onto the first ceramic source material to vaporize the first ceramic source material to deposit a first layer on the component; alternating the energy source between the first ceramic source material and the second ceramic source material to form a blended layer on the first layer, wherein the blended layer is formed from vapors from the first ceramic source material and the second ceramic source material; and after alternating the energy source between the first ceramic source material and the second ceramic source material, directing the energy source onto the second ceramic source material to vaporize the second ceramic source material to deposit a second layer on the blended layer such that the blended layer is positioned between the first layer and the second layer. 2. The method of claim 1 , wherein the blended layer forms a granular interface between the first layer and the second layer. 3. The method of claim 1 , wherein the blended layer has a graded composition extending from the first layer to the second layer. 4. The method of claim 1 , wherein the first layer and the second layer forms a thermal barrier coating having columnar grains, and wherein the blended layer of the thermal barrier coating is a mixture of the first and second ceramic compositions. 5. The method of claim 1 , wherein the blended layer has a graded composition extending from the first layer to the second layer. 6. The method of claim 5 , wherein the blended layer has a higher concentration of the first ceramic source material than the second ceramic source material at its interface with the first layer and a higher concentration of the second ceramic source material than the first ceramic source material at its interface with the second layer. 7. The method of claim 1 , wherein the blended layer has a stepped composition extending from the first layer to the second layer. 8. The method of claim 7 , wherein the blended layer is formed from at least two layers. 9. The method of claim 7 , wherein the blended layer is formed from a plurality of sub-layers, and wherein each of the sublayers have a composition that increases in concentration of the second ceramic source material as it extends away from the first layer. 10. The method of claim 7 , further comprising: after directing the energy source onto the first ceramic source material, alternating the energy source between the first ceramic source material and the second ceramic source material at a first alternating rate to form a first blended layer between the first layer and the second layer; and thereafter, alternating the energy source between the first ceramic source material and the second ceramic source material at a second alternating rate to form a second blended layer between the first layer and the second layer, wherein the second blended layer has a greater concentration of the second ceramic source material than the first blended layer. 11. The method of claim 7 , further comprising: after directing the energy source onto the first ceramic source material, alternating the energy source between the first ceramic source material and the second ceramic source material at a first alternating rate to form a first blended layer between the first layer and the second layer; thereafter, alternating the energy source between the first ceramic source material and the second ceramic source material at a second alternating rate to form a second blended layer between the first layer and the second layer, wherein the second blended layer has a greater concentration of the second ceramic source material than the first blended layer; and thereafter, alternating the energy source between the first ceramic source material and the second ceramic source material at a third alternating rate to form a third blended layer between the first layer and the second layer, wherein the third blended layer has a greater concentration of the second ceramic source material than the second blended layer.
Metallic sublayers · CPC title
Ion beam deposition (C23C14/46, C23C14/48 take precedence) · CPC title
by wave energy or particle radiation (C23C14/32 - C23C14/48 take precedence) · CPC title
of refractory metals or yttrium · CPC title
with at least one metal alloy layer · CPC title
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