Method of manufacturing eyeglass lens

Patent metadata

Field	Value
Publication number	US-9651802-B2
Application number	US-201314389207-A
Country	US
Kind code	B2
Filing date	Mar 15, 2013
Priority date	Mar 30, 2012
Publication date	May 16, 2017
Grant date	May 16, 2017

Abstract

An aspect of the present invention relates to a method of manufacturing an eyeglass lens, comprising determining a manufacturing condition by a method of determining a manufacturing condition of an eyeglass lens comprising a vapor-deposited film formed by vapor deposition using a vapor deposition source the main component of which is ZrO 2 , and forming a vapor-deposited film by vapor deposition using a vapor deposition source the main component of which is ZrO 2 under the manufacturing condition that has been determined.

First claim

The invention claimed is:

1. A method of manufacturing an eyeglass lens, which comprises:
determining a manufacturing condition by a method of determining a manufacturing condition of an eyeglass lens comprising a vapor-deposited film formed by vapor deposition using a vapor deposition source the main component of which is ZrO 2 ; and
forming a vapor-deposited film by vapor deposition using a vapor deposition source the main component of which is ZrO 2 under the manufacturing condition that has been determined, wherein
the method of determining a manufacturing condition comprises:
pre-determining a threshold of grain size permitting formation of a ZrO 2 vapor-deposited film with a desired heat resistance;
determining a candidate vapor deposition condition to be employed in vapor deposition of the vapor-deposited film in actual manufacturing;
forming a test vapor-deposited film by conducting vapor deposition under the candidate vapor deposition condition that has been determined;
taking a transmission electron microscope (TEM) image of the test vapor deposited-film;
comparing the grain size in the TEM image with the predetermined threshold of grain size, and
determining the candidate vapor deposition condition as a vapor deposition condition to be employed in a vapor deposition for actual manufacturing of an eyeglass lens when the grain size of the test vapor-deposited film is greater than the predetermined threshold of grain size, or determining a vapor deposition condition, which is determined by adding change(s) so as to increase heat resistance of a ZrO 2 vapor-deposited film or change(s) not affecting heat resistance of a ZrO 2 vapor-deposited film to the candidate vapor deposition condition, as a vapor deposition condition to be employed in a vapor deposition for actual manufacturing of an eyeglass lens when the grain size of the test vapor-deposited film is greater than the predetermined threshold of grain size.

2. The method of manufacturing an eyeglass lens according to claim 1 , wherein the TEM image is a planar TEM image.

3. The method of manufacturing an eyeglass lens according to claim 1 , wherein the grain size to be employed for the determination is an average value of the grain size.

4. The method of manufacturing an eyeglass lens according to claim 1 , wherein the vapor-deposited film is formed as a layer constituting a multi-layered antireflective film.

5. The method of manufacturing an eyeglass lens according to claim 1 , wherein the major or minor diameter of the granular region is adopted as the grain size.

6. The method of manufacturing an eyeglass lens according to claim 1 , wherein the equivalent circle diameter obtained by a circle projection method is adopted as the grain size.

7. The method of manufacturing an eyeglass lens according to claim 1 , wherein the grain size serving as an indicator in determining the manufacturing condition is the maximum size, minimum size, or average value of the grains in a prescribed region of the TEM image.

8. The method of manufacturing an eyeglass lens according to claim 1 , wherein among two or more sets of candidate conditions, the actual manufacturing condition is determined by a relative determination of adopting the condition of the largest grain size in the TEM image as the vapor deposition condition for the ZrO 2 vapor-deposited film in actual manufacturing.

9. The method of manufacturing an eyeglass lens according to claim 1 , wherein preliminary tests are conducted and a database is created of the correlation between the vapor deposition conditions of ZrO 2 vapor-deposited films and their tendency to crack at high temperatures; based on the database, the threshold is pre-determined, and those grain sizes at or above the threshold is determined to be vapor deposition conditions for ZrO 2 vapor-deposited films in actual manufacturing.

10. The method of manufacturing an eyeglass lens according to claim 1 , wherein the change(s) added to the candidate vapor deposition condition include at least one selected from the group consisting of change of current of an ion gun and change of voltage of an ion gun employed in a vapor deposition.

Assignees

• Ogawa Naomi
• Tadokoro Nobuyuki
• Adachi Makoto
• Kamura Hitoshi
• Komine Yuko
• Hoya Corp

Inventors

• Ogawa Naomi
• Tadokoro Nobuyuki
• Adachi Makoto
• Kamura Hitoshi
• Komine Yuko

Classifications

• G02C7/022 Primary

  Ophthalmic lenses having special refractive features achieved by special materials or material structures (G02C7/049 takes precedence) · CPC title

• B29D11/00951

  Measuring, controlling or regulating · CPC title

• C23C14/24 Primary

  Vacuum evaporation · CPC title

• G02B1/115

  Multilayers · CPC title

• C23C14/083

  of refractory metals or yttrium · CPC title