Rapid thickening of aminosilicones to promote emulsion stability and adhesion of UV-curable quantum dot enhancement film emulsions
US-12122948-B2 · Oct 22, 2024 · US
US9650563B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-9650563-B2 |
| Application number | US-201414469816-A |
| Country | US |
| Kind code | B2 |
| Filing date | Aug 27, 2014 |
| Priority date | Aug 29, 2013 |
| Publication date | May 16, 2017 |
| Grant date | May 16, 2017 |
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The present invention provides a method for producing a fluoride fluorescent material, comprising: contacting a fluoride particles represented by the following general formula (I): K 2 [M 1-a Mn 4+ a F 6 ] (I) wherein M is at least one member selected from the group consisting of elements belonging to Groups 4 and 14 of the Periodic Table, and a satisfies the relationship: 0<a<0.2; with a solution containing alkaline earth metal ions in the presence of a reducing agent to form an alkaline earth metal fluoride on the surface of the fluoride particles.
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The invention claimed is: 1. A method for producing a fluoride fluorescent material, the method consisting of: contacting fluoride particles represented by the following general formula (I): K 2 [M 1-a Mn 4+ a F 6 ] (I) wherein M is at least one element selected from the group consisting of elements belonging to Groups 4 and 14 of the Periodic Table, and a satisfies the relationship: 0<a<0.2; with a solution containing calcium ions in the presence of a reducing agent to form calcium fluoride on the surface of the fluoride particles. 2. The method according to claim 1 , wherein M is at least one element selected from the group consisting of titanium (Ti), zirconium (Zr), hafnium (Hf), silicon (Si), germanium (Ge), and tin (Sn). 3. The method according to claim 1 , wherein the solution containing calcium ions is a solution of at least one compound selected from the group consisting of Ca(NO 3 ) 2 , Ca(CH 3 CO 2 ) 2 , CaCl 2 , Cal 2 , and CaBr 2 .
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