Porous ceramic material, manufacturing method and use thereof

Patent metadata

Field	Value
Publication number	US-9648909-B2
Application number	US-201514814093-A
Country	US
Kind code	B2
Filing date	Jul 30, 2015
Priority date	Apr 30, 2015
Publication date	May 16, 2017
Grant date	May 16, 2017

Abstract

The present invention relates to a manufacturing method of a porous ceramic material, which includes the following steps: mixing a silicate material and a porogen to obtain a premix, wherein the silicate material includes sodium silicate and other compounds being at least one selected from the group consisting of oxides, nitrides, and carbides; drying the premix to obtain a silicate aggregate; mixing the silicate aggregate and an adhesive to obtain an injection molding material, wherein in a weight percentage, the silicate aggregate is in the range of from 50% to 60%, the adhesive is in the range of from 40% to 50%; injection molding the injection molding material to obtain a green body; and degumming and calcinating the green body successively to obtain the porous ceramic material. In the aforementioned manufacturing method of the porous ceramic material, the space-holder method is combined with the injection molding method, such that the obtained porous ceramic material has a high porosity, controllable pore sizes and good mechanical properties. In addition, compared with the dry pressing process, the use of the injection molding process can significantly improve the production efficiency, and is suitable for large-scale production.

First claim

What is claimed is:

1. A method of manufacturing a porous ceramic material, comprising the following steps:
mixing a silicate material and a porogen to obtain a premix, wherein the silicate material comprises sodium silicate and other compounds being at least one selected from the group consisting of oxides, nitrides, and carbides; wherein in a weight percentage, the sodium silicate is in the range of from 20% to 40%, the other compounds are in the range of from 45% to 75%, the porogen is in the range of from 3% to 20%;
drying the premix to obtain a silicate aggregate;
mixing the silicate aggregate and an adhesive to obtain an injection molding material, wherein in a weight percentage, the silicate aggregate is in the range of from 50% to 60%, the adhesive is in the range of from 40% to 50%;
injection molding the injection molding material to obtain a green body; and
degumming and calcinating the green body successively to obtain the porous ceramic material.

2. The method of manufacturing the porous ceramic material according to claim 1 , wherein the porogen is at least one selected from the group consisting of sawdust, starch, and graphite.

3. The method of manufacturing the porous ceramic material according to claim 1 , wherein the premix is dried at a temperature of 70° C. to 110° C. for 200 min to 400 min.

4. The method of manufacturing the porous ceramic material according to claim 1 , wherein in a weight percentage, the adhesive comprises 60% to 80% of paraffin wax, 5% to 15% of polypropylene, 5% to 15% of stearic acid, and 5% to 15% of dibutyl phthalate.

5. The method of manufacturing the porous ceramic material according to claim 1 , wherein the silicate aggregate and the adhesive are mixed at a temperature of 180° C. to 220° C. for 3 h to 5 h.

6. The method of manufacturing the porous ceramic material according to claim 1 , wherein injection molding conditions for the injection molding material are: injection temperature of 100° C. to 160° C.; injection pressure of 50 MPa to 140 MPa; holding pressure of 10 MPa to 30 MPa.

7. The method of manufacturing the porous ceramic material according to claim 1 , wherein the green body is degummed at a temperature of 200° C. to 800° C. for 3 h to 10 h.

8. The method of manufacturing the porous ceramic material according to claim 1 , wherein the green body is calcinated at a temperature of 800° C. to 1600° C. for 1 h to 4 h.

9. The method of manufacturing the porous ceramic material according to claim 1 , comprising forming the porous ceramic material into an atomizer of an electronic cigarette.

Assignees

• Shenzhen Smoore Technology Ltd
• Zhou Hongming
• Li Jian
• Shenzhen Smoore Technology Ltd

Inventors

• Zhou Hongming
• Xia Qinglu
• Xiao Kaiwen
• Li Jian
• Liu Pingkun

Classifications

• B28B11/243

  Setting, e.g. drying, dehydrating or firing ceramic articles (B28B11/242 takes precedence) · CPC title

• C03C11/00

  Multi-cellular glass {; Porous or hollow glass or glass particles} · CPC title

• B05B17/00

  Apparatus for spraying or atomising liquids or other fluent materials, not covered by the preceding groups (dropping or releasing powdered, liquid or gaseous matter in flight B64D1/16) · CPC title

• A24F47/008 Primary

  Human Necessities · mapped topic

• B28B1/24 Primary

  by injection moulding {(injection moulding of ceramic slips B28B1/265; of tubular articles B28B21/38)} · CPC title