Sintered body production method
US-2024307956-A1 · Sep 19, 2024 · US
US9643334B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-9643334-B2 |
| Application number | US-201314394752-A |
| Country | US |
| Kind code | B2 |
| Filing date | Apr 17, 2013 |
| Priority date | Apr 20, 2012 |
| Publication date | May 9, 2017 |
| Grant date | May 9, 2017 |
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A method of making a construction comprising a polycrystalline super-hard structure joined to a side surface of an elongate substrate. The method includes: providing a vessel configured for an ultra-high pressure, high temperature furnace, the vessel having an elongate cavity for containing a pre-sinter assembly and defining a longitudinal axis, the cavity having opposite ends connected by a cavity wall. The pre-sinter assembly comprises the substrate, an aggregation comprising a plurality of super-hard grains arranged over at least a part of the side surface of the substrate, and a spacer structure configured for spacing the substrate apart from the cavity wall. The spacer structure comprises material having a Young's modulus of at least 300 GPa. The method further includes inserting the pre-sinter assembly into the cavity, the substrate being substantially longitudinally aligned and the spacer structure arranged between the side surface of the substrate and the cavity wall; applying a force to the pre-sinter assembly and heating it to a temperature, the force being sufficient to generate a pressure within the vessel for sintering the aggregation at the temperature, and providing the construction.
Opening claim text (preview).
The invention claimed is: 1. A method of making a construction comprising a polycrystalline super-hard structure joined to a side surface of an elongate substrate; the method including: providing a vessel configured for an ultra-high pressure of at least 4 GPa, high temperature furnace configured to reach a temperature of at least 1000° C., the vessel having an elongate cavity for containing a pre-sinter assembly and defining a longitudinal axis, the cavity having opposite ends connected by a cavity wall; the pre-sinter assembly comprising the substrate, an aggregation comprising a plurality of super-hard grains arranged over at least a part of the side surface of the substrate, and an annular spacer structure configured for spacing the substrate apart from the cavity wall; the spacer structure comprising material having a Young's modulus of at least 300 GPa; the method further including inserting the pre-sinter assembly into the cavity, the substrate being substantially longitudinally aligned and the spacer structure arranged between the side surface of the substrate and the cavity wall; applying a force to the pre-sinter assembly and heating it to a temperature, the force being sufficient to generate a pressure within the vessel for sintering the aggregation at the temperature, and providing the construction, wherein the spacer and the polycrystalline super-hard structure comprise different materials. 2. A method as claimed in claim 1 , in which the substrate comprises the spacer structure extending laterally from an elongate core structure of the substrate. 3. A method as claimed in claim 1 , in which the spacer structure abuts the substrate. 4. A method as claimed in claim 1 , in which the force is applied longitudinally or tri-axially to the pre-sinter assembly. 5. A method as claimed in claim 1 , in which the substrate comprises an elongate core structure and an end cap defining a proximate end surface of the substrate, the end cap extending laterally beyond the core structure. 6. A method as claimed in claim 1 , in which the spacer structure abuts the cavity wall. 7. A method as claimed in claim 1 , the method including using more than one spacer structure, each arranged at a different respective longitudinal position along the substrate. 8. A method as claimed in claim 1 , in which the substrate is rotationally symmetric about a central longitudinal axis. 9. A method as claimed in claim 1 , in which the spacer structure comprises material having a Young's modulus of at least 300 GPa at a temperature of at least 1,000 degrees centigrade. 10. A method as claimed in claim 1 , in which the spacer structure comprises cemented tungsten carbide. 11. A method as claimed in claim 1 , in which the spacer structure comprises ceramic material. 12. A method as claimed in claim 1 , in which the spacer structure comprises nickel based super-alloy material. 13. A method as claimed in claim 1 , in which the spacer structure comprises super-hard material. 14. A method as claimed in claim 1 , in which the vessel comprises pyrophyllite, mullite, kyonite, kaolinite, salt or ceramic material. 15. A method as claimed in claim 1 , in which the super-hard grains comprise natural or synthetic diamond material, or cubic boron nitride (cBN) material. 16. A method as claimed in claim 1 , in which the polycrystalline super-hard structure comprises polycrystalline diamond (PCD) material, polycrystalline cubic boron nitride (PCBN) material, silicon carbide bonded diamond (SCD) material or cemented carbide material comprising super-hard grains. 17. A method as claimed in claim 1 , in which the construction is for a blank body from which a rotary machine tool cutter element can be manufactured. 18. A method as claimed in claim 1 , in which the aggregation comprises super-hard grains and binder material binding the grains together. 19. A method as claimed in claim 1 , in which the aggregation comprises a plurality of filaments, foils or sheets comprising the super-hard grains. 20. A method as claimed in claim 1 , including providing granules comprising the super-hard grains, and combining and compacting the granules against the substrate. 21. A method as claimed in claim 1 , in which the aggregation comprises an extruded body comprising the super-hard grains. 22. A method as claimed in claim 1 , in which the aggregation is spaced apart from at least one end of the substrate by at least 1 mm. 23. A method as claimed in claim 1 , in which the aggregation is spaced apart from at least one end of the substrate by the spacer structure. 24. A method as claimed in claim 1 , in which the aggregation extends peripherally all the way around at least a part of the substrate. 25. A method as claimed in claim 1 , the method including processing the super-hard structure to provide a cutting edge. 26. A method as claimed in claim 1 , the method including brazing an end of the construction to a tool carrier.
Shank-type cutters, i.e. with an integral shaft · CPC title
simultaneously · CPC title
Burning or sintering processes (C04B33/32 takes precedence {; powder metallurgy B22F}) · CPC title
Alloys containing diamond {or cubic or wurtzitic boron nitride, fullerenes or carbon nanotubes} · CPC title
polycrystalline [PCD] · CPC title
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