Distributor device for a multiple-bed downflow reactor

Patent metadata

Field	Value
Publication number	US-9630159-B2
Application number	US-201214366722-A
Country	US
Kind code	B2
Filing date	Dec 20, 2012
Priority date	Dec 22, 2011
Publication date	Apr 25, 2017
Grant date	Apr 25, 2017

Abstract

The invention relates to a device and method for distributing a liquid and gas in a multiple-bed downflow reactor, such as a hydrocarbon processing reactor, like a hydrocracker. The device comprises respectively the method uses a distributor device comprising a substantially horizontal collecting tray provided with a central gas passage. Gas passing in downward direction through the central gas passage is forced into a swirling motion by a swirler. This swirling motion has a swirl direction around a vertical swirl axis so that the gas leaves the central gas passage as a swirl. At a location above the collecting tray, a quench fluid is ejected into gas in an ejection direction, which is, viewed in a horizontal plane, at least partly opposite to the swirl direction.

First claim

That which is claimed is:

1. A process, comprising: providing distributor device for distributing liquid and gas in a multiple-bed downflow reactor; wherein the distributor device comprises:
a substantially horizontal collecting tray provided with:
a central gas passage and
liquid passages around the central gas passage;
a swirler, which swirler:
is located above the collecting tray around the central gas passage, and
is provided with vanes defining a swirl direction and being arranged to impart a swirling motion to gas passing through the central gas passage so that the gas leaves the central gas passage as a swirl swirling in said swirl direction around a vertical swirl axis;
one or more ejection nozzles located above the collecting tray and arranged for ejecting, in an ejecting direction, a quench fluid into the gas before said gas enters the swirler;
wherein the ejection direction is represented in an orthogonal set of three ejection vectors comprised of a radial ejection vector extending perpendicular to the swirl axis, an axial ejection vector (A) extending parallel to the swirl axis and a tangential ejection vector extending tangentially with respect to the swirl axis;

introducing the quench fluid through the one or more injection nozzle; and passing the gas through the swirler;
characterized, in that the ejection nozzle is directed such that the tangential ejection vector,

T) of the ejection direction of the ejected quench fluid is directed opposite to the swirl direction.

2. A process according to claim 1 , further comprising using the distribution device in hydrocarbon processing, such as hydrocracking, such as in hydrotreating and/or hydrocracking process.

3. A distributing method for distributing a liquid and gas in a multiple-bed downflow reactor, such as a hydrocarbon processing reactor, like a hydrocracker;
wherein a distributor device is used, which distributor device comprises a substantially horizontal collecting tray provided with a central gas passage;
wherein gas passing in downward direction through a swirler surrounding the central gas passage is forced into a swirling motion having a swirl direction around a vertical swirl axis so that the gas leaves the central gas passage as a swirl;
wherein liquid is collected on the collecting tray;
wherein, at a location above the collecting tray and before the gas enters the swirler, a quench fluid, like a gaseous quench fluid, is ejected into said gas in an ejection direction, which is, viewed in a horizontal plane, at least partly opposite to the swirl direction.

4. The distributing method according to claim 3 , wherein the ejection direction is represented in an orthogonal set of three ejection vectors comprised of a radial ejection vector extending perpendicular to the swirl axis, an axial ejection vector (A) extending parallel to the swirl axis and a tangential ejection vector extending tangentially with respect to the swirl axis; and wherein the ejection nozzle is directed such that the tangential ejection vector is directed opposite to the swirl direction.

5. The distributing method according to claim 4 , wherein the radial ejection vector is directed to the swirl axis.

6. The distributing method according to claim 4 , wherein the ejection direction and associated radial ejection vector define, viewed in a horizontal plane, an angle (α) in the range of from 5° to 35°.

7. The process according to claim 1 , wherein the ejection nozzle is directed such that the radial ejection vector of the ejection direction of the quench fluid is directed to the swirl axis.

8. The process according to claim 1 , wherein the ejection direction and associated radial ejection vector of a said nozzle define an angle of more than 5°.

9. The process according to claim 1 , wherein the ejection direction and associated radial ejection vector of a said ejection nozzle define an angle of at least 10°.

10. The process according to claim 1 , wherein the ejection direction and associated radial ejection vector of a said ejection nozzle define an angle of at most 35°.

11. The process according to claim 1 , wherein the ejection direction and associated radial ejection vector of a said ejection nozzle define an angle of at most 30°.

12. The process according to claim 1 , wherein the ejection direction and associated radial ejection vector of a said ejection nozzle define an angle in the range of from 5° to 35°.

13. The process according to claim 1 , wherein:
the distributor device further comprises a mixing chamber defined between the collecting tray and the distribution tray;
the central gas passage is surrounded by a weir;
the distributor device further comprises a cover located above the central gas passage and covering the entire central gas passage;
and/or
the distributor device further comprises a substantially horizontal pre-distribution tray arranged below the central gas passage, above the distribution tray and, in case present, lower than the optional injection nozzles of the optional one or more guide conduits, which pre-distribution tray is provided with an overflow weir at its perimeter and a plurality of openings near the perimeter;
and/or
one or more guide conduits arranged below the collecting tray ( 20 ), wherein the guide conduits have: first ends communicating with the liquid passages ( 40 ) of the collecting tray for receiving liquid; and
second ends provided with an injection nozzle arranged to inject, in an injection direction, liquid received by the first ends into said swirl; wherein optionally
the one or more guide conduits comprise at least eight guide conduits distributed around the central gas passage; and/or
the injection nozzles of the one or more guide conduits are arranged to lie within the same horizontal plane; and/or
the distributor device further comprises a substantially horizontal distribution tray located below the collecting tray, which distribution tray is provided with a plurality of downcomers for downward flow of liquid and gas; each downcomer optionally comprising an upstanding, open ended tube having an aperture at its side for entry of liquid into the tube; and/or
the one or more ejection nozzles comprise a plurality of ejection nozzles arranged around the swirl axis to lie within the same horizontal plane.

Assignees

• Shell Int Research
• Shell Oil Co

Inventors

• Degaleesan Sujatha
• Ouwerkerk Charles Eduard Dammis
• Witkamp Benoit
• Worthen Rachel Anna

Classifications

• C10G45/00

  Refining of hydrocarbon oils using hydrogen or hydrogen-generating compounds · CPC title

• C10G47/00 Primary

  Cracking of hydrocarbon oils, in the presence of hydrogen or hydrogen- generating compounds, to obtain lower boiling fractions (C10G15/00 takes precedence; destructive hydrogenation of non-melting solid carbonaceous or similar materials C10G1/06) · CPC title

• B01J8/0492 Primary

  Feeding reactive fluids (for solid material, see B01J8/0015) · CPC title

• B01J2208/027

  Beds · CPC title