Process for manufacturing an emulsion

Patent metadata

Field	Value
Publication number	US-9622948-B2
Application number	US-201314898563-A
Country	US
Kind code	B2
Filing date	Dec 13, 2013
Priority date	Dec 20, 2012
Publication date	Apr 18, 2017
Grant date	Apr 18, 2017

Abstract

Present invention relates to a process for manufacturing emulsion composition which comprises an oil phase dispersed in a continuous water phase which is stabilized with a surfactant as an emulsifier. The present invention is on a method for producing an emulsion comprising one or more fatty alcohol, one or more oil liquid at 20° C. and one or more surfactant wherein one or more surfactant is added to the dispersion of one or more fatty alcohol and one or more oil liquid at 20° C. in water at a temperature of 50° C. or higher, preferably 60° C. or higher with the condition that the temperature of the dispersion is at least 10° C. higher than the melting point of fatty alcohol having the highest melting point, more preferably between 60 and 85° C. wherein the emulsion thus obtained does not comprise dispersed droplets with a volume size larger than or equal to 10 μm measured directly without dilution of the emulsion at 20° C. measured with a laser particle size analyzer suitable therefore.

First claim

The invention claimed is:

1. A method of producing an emulsion composition, said composition comprising one or more fatty alcohol, one or more oil which is liquid at 20° C., and one or more surfactant, said method comprising:
adding one or more surfactant to a dispersion of the one or more fatty alcohol and the one or more oil liquid at 20° C. in water at a temperature of 50° C. or higher, with the condition that the temperature of the dispersion is at least 10° C. higher than melting point of the one or more fatty alcohol, thus forming an emulsion,
wherein the emulsion does not comprise dispersed droplets with a volume size of larger than or equal to 10 μm measured directly without dilution of the emulsion at 20° C., and measured with a laser particle size analyzer suitable therefore.

2. The method according to claim 1 , wherein the one or more fatty alcohol is selected from fatty alcohols of the general structure
R 1 —OH

wherein R 1 is a saturated or unsaturated, straight or branched alkyl chain having 12 to 30 C atoms which may also be substituted with one or more OH groups.

3. The method according to claim 1 , wherein the one or more oil is selected from synthetic oil and natural oil.

4. The method according to claim 1 , wherein weight ratio of the one or more fatty alcohol to the one or more oil is less than or equal to 1.

5. The method according to claim 1 , wherein the emulsion comprises mineral oil which is liquid at 20° C.

6. The method according to claim 1 , wherein the one or more surfactant is selected from anionic, nonionic and cationic surfactant.

7. The method according to claim 1 , wherein the one or more surfactant is anionic.

8. The method according to claim 1 , wherein the one or more surfactant is selected from cationic surfactants according to general structure

where R 8 is a saturated or unsaturated, branched or non-branched alkyl chain with 8-22 C atoms, or
R 12 CO NH(CH 2 ) n

where R 12 is saturated or unsaturated, branched or non-branched alkyl chain with 7-21 C atoms and n has typical value of 1-4, or
R 13 CO O(CH 2 ) n

where R 13 is saturated or unsaturated, branched or non-branched alkyl chain with 7-21 C atoms and n has typical value of 1-4, and
and R 9 , R 10 and R 11 are independent from each other H or lower alkyl chain with 1 to 4 carbon atoms, and X is an anion.

9. The method according to claim 1 , wherein weight ratio of the one or more surfactant to total of the one or more fatty alcohol and the one or more oil is less than or equal to 0.25.

10. The method according to claim 1 , wherein the emulsion comprises at least one oxidizing agent.

11. The method according to claim 1 , wherein the emulsion comprises one or more of the compounds selected from
a-Cationic polymer,
b-Organic solvent,
c-Ceramide,
d-Phytosterol,
e-Diamide compound according to general structure

wherein R 14 is a linear or branched, saturated or unsaturated alkyl chain with 1 to 12 C atoms which may be substituted with hydroxy and/or alkoxy groups, R 15 is linear or branched alkyl chain with 1 to 5 C atoms, and R 16 linear or branched, saturated or unsaturated alkyl chain with 1 to 22 C atoms, and

f-Ubiqinone according to general structure

where n is a number between 1 and 10.

12. A process for treating hair, comprising:
(a) mixing the composition manufactured according to the method of claim 1 with a second composition, and
(b) applying onto hair a mixture obtained from step (a), and
(c) leaving the mixture obtained from step (a) on hair for a period 1 to 45 min, and
(d) rinsing the mixture obtained from step (a) off from hair.

13. The process according to claim 12 , wherein the second composition comprises at least one hair dye.

14. A kit comprising two or more compositions, wherein one of the two or more compositions is an emulsion manufactured in accordance with the method of claim 1 .

15. The method according to claim 1 , wherein the temperature of the dispersion is 60° C. or higher.

16. The method according to claim 2 , wherein the one or more fatty alcohol is present at a concentration in the range of 1 to 20% by weight calculated to the total of the composition.

17. The method according to claim 2 , wherein the one or more fatty alcohol is solid at 20° C.

18. The method according to claim 3 , wherein the one or more oil is present at a concentration in the range of 1 to 20% by weight calculated to the total of the composition.

19. The method according to claim 6 , wherein the one or more surfactant is present at a total concentration of 0.05 to 10% by weight calculated to the total of the composition.

20. The method according to claim 7 , wherein the one or more surfactant is sodium lauryl sulfate.

Assignees

• Kao Germany Gmbh

Inventors

• Ächtner Anja
• Häckl Carsten
• Wood Jonathan

Classifications

• A61K8/31 Primary

  Hydrocarbons · CPC title

• A61K8/86

  Polyethers · CPC title

• A61K2800/591

  Mixtures of compounds not provided for by any of the codes A61K2800/592 - A61K2800/596 · CPC title

• B01F17/0042

  Operations & Transport · mapped topic

• A61K2800/43

  Pigments; Dyes · CPC title