Steam stripping apparatus and steam-stripping finishing method using same

Patent metadata

Field	Value
Publication number	US-9616405-B2
Application number	US-201214359603-A
Country	US
Kind code	B2
Filing date	Nov 27, 2012
Priority date	Nov 28, 2011
Publication date	Apr 11, 2017
Grant date	Apr 11, 2017

Abstract

A steam stripping apparatus is provided that prevents adherence of crumbs to an inner wall of a crumbing tank, pipe blockages caused by reaggregated large particle size crumbs, clogging of a screen by small particle size crumbs, and slipping in an extruder, and which can operate over a long period of time. The crumbing tank includes a stir shaft and an impeller, and also has a baffle plate on an inner wall face. The impeller has a knife blade. The baffle plate has an approximately triangular cross-sectional shape having, on a cross section in a cylindrical lateral direction of the crumbing tank, a side face on each of an upstream side and a downstream side with respect to a flow direction of a fluid, and in which the upstream-side side face and the downstream-side side face meet to form an intersection point.

First claim

The invention claimed is:

1. A steam stripping apparatus comprising:
at least one cylindrical upright crumbing tank which recovers a rubbery polymer from a solution containing the rubbery polymer by means of steam;
a stir shaft, inside the crumbing tank, which extends in a cylindrical upright direction, and which rotates in an axial direction;
an impeller that extends from a center of the stir shaft in a direction of an inner wall face of the crumbing tank;
a knife blade mounted on the impeller, wherein the knife blade has a cutting edge with an edge angle between 10 and 60 degrees that faces in a rotational direction of the stir; and
a baffle plate arranged on an inner wall face of the crumbing tank;
wherein the baffle plate has an approximately triangular cross-sectional area having, on a cross section in a cylindrical lateral direction of the crumbing tank, an upstream side and a downstream side with respect to a flow direction of a fluid inside the crumbing tank, and in which the upstream side and the downstream side meet to form an intersection point;
an angle of the baffle plate that is formed by a line segment of the upstream side on the cross section in the cylindrical lateral direction of the crumbing tank and a line segment that connects to the intersection point from the center of the stir shaft is between 30 and 75 degrees;
an angle of the baffle plate formed by a line segment of the downstream side on the cross section in the cylindrical lateral direction of the crumbing tank and the line segment that connects to the intersection point from the center of the stir shaft is between 30 and 75 degrees; and
the crumbing tank includes a steam supply port at a bottom portion thereof to feed the steam into the crumbing tank.

2. The steam stripping apparatus according to claim 1 , wherein the cross-sectional area of the baffle plate is between 1 and 20% relative to a cross-sectional area of the crumbing tank.

3. The steam stripping apparatus according to claim 2 , wherein the cross-sectional area of the crumbing tank is a sum total of cross-sectional areas of the stir shaft, the impeller and the baffle plate.

4. The steam stripping apparatus according to claim 1 , wherein:
the crumbing tank has an inside diameter;
a distance exists between a tip of the cutting edge of the knife blade and a center of a cross section of the stir shaft that is on a same plane as the knife blade;
a ratio of twice the distance to the inside diameter is between 30 and 70%.

5. A steam stripping apparatus comprising:
at least one cylindrical upright crumbing tank which recovers a rubbery polymer from a solution containing the rubbery polymer by means of steam;
a stir shaft, inside the crumbing tank, which extends in a cylindrical upright direction, and which rotates in an axial direction;
an impeller that extends from a center of the stir shaft in a direction of an inner wall face of the crumbing tank; and
a baffle plate arranged on an inner wall face of the crumbing tank; wherein
the baffle plate has an approximately triangular cross-sectional area having, on a cross section in a cylindrical lateral direction of the crumbing tank, an upstream side and a downstream side with respect to a flow direction of a fluid inside the crumbing tank, and in which the upstream side and the downstream side meet to form an intersection point;
an angle of the baffle plate that is formed by a line segment of the upstream side on the cross section in the cylindrical lateral direction of the crumbing tank and a line segment that connects to the intersection point from the center of the stir shaft is between 30 and 75 degrees;
an angle of the baffle plate formed by a line segment of the downstream side on the cross section in the cylindrical lateral direction of the crumbing tank and the line segment that connects to the intersection point from the center of the stir shaft is between 30 and 75 degrees; and
the crumbing tank includes a steam supply port at a bottom portion thereof to feed the steam into the crumbing tank.

6. The steam stripping apparatus according to claim 5 , wherein the cross-sectional area of the baffle plate is between 1 and 20% relative to a cross-sectional area of the crumbing tank.

7. The steam stripping apparatus according to claim 6 , wherein the cross-sectional area of the crumbing tank is a sum total of cross-sectional areas of the stir shaft, the impeller and the baffle plate.

8. A steam stripping apparatus comprising:
at least one cylindrical upright crumbing tank which recovers a rubbery polymer from a slurry containing the rubbery polymer by means of steam;
a stir shaft, inside the crumbing tank, which extends in a cylindrical upright direction, and which rotates in an axial direction;
an impeller that extends from a center of the stir shaft in a direction of an inner wall face of the crumbing tank;
a knife blade mounted on the impeller, wherein the knife blade has a cutting edge with an edge angle between 10 and 60 degrees that faces in a rotational direction of the stir; and
a baffle plate arranged on an inner wall face of the crumbing tank;
wherein the baffle plate has an approximately triangular cross-sectional area having, on a cross section in a cylindrical lateral direction of the crumbing tank, an upstream side and a downstream side with respect to a flow direction of a fluid inside the crumbing tank, and in which the upstream side and the downstream side meet to form an intersection point;
an angle of the baffle plate that is formed by a line segment of the upstream side on the cross section in the cylindrical lateral direction of the crumbing tank and a line segment that connects to the intersection point from the center of the stir shaft is between 30 and 75 degrees;
an angle of the baffle plate formed by a line segment of the downstream side on the cross section in the cylindrical lateral direction of the crumbing tank and the line segment that connects to the intersection point from the center of the stir shaft is between 30 and 75 degrees; and
the crumbing tank includes a steam supply port at a bottom portion thereof to feed the steam into the crumbing tank.

Assignees

• Asahi Kasei Chemicals Corp

Inventors

• Nakahara Tatsuto
• Nakano Hiroshi

Classifications

• B01D19/001

  by bubbling steam through the liquid (B01D19/0042, B01D19/0047 and B01D19/0052 take precedence) · CPC title

• C08F6/10

  Removal of volatile materials, e.g. solvents {(C08F6/001, C08F6/003, C08F6/005, C08F6/006, C08F6/008, C08F6/02, C08F6/04 take precedence)} · CPC title

• C08C2/06 Primary

  Winning of rubber from solutions · CPC title

• B01J2219/1943

  cylindrical · CPC title

• B01J19/006 Primary

  Baffles · CPC title