Setting accelerator for a dry mortar blend, process for producing such a setting accelerator, a dry mortar blend and a mortar paste

Patent metadata

Field	Value
Publication number	US-9611176-B2
Application number	US-201415033956-A
Country	US
Kind code	B2
Filing date	Nov 4, 2014
Priority date	Nov 5, 2013
Publication date	Apr 4, 2017
Grant date	Apr 4, 2017

Abstract

The invention relates to a setting accelerator for a dry mortar blend, the setting accelerator being in the form of a powder comprising calcium nitrate and having a water content between 0.1% and 20%. The invention furthermore relates to a process for producing such a setting accelerator, wherein either prills and/or granules comprising calcium nitrate and a different nitrate salt are processed forming a powder comprising calcium nitrate and the different nitrate salt and having a water content of higher than 5% and lower than 20%, either an aqueous solution at least comprising dissolved calcium nitrate is spray dried at a temperature between 150° C. and 250° C., forming a powder comprising at least calcium nitrate and having a water content between 0.1% and 20%, the powder serving as the setting accelerator. The invention also relates to a dry mortar blend comprising at least a cement, sand and a setting accelerator according to the invention and to a mortar paste comprising the dry mortar blend according to the invention which is mixed with water.

First claim

The invention claimed is:

1. A method for reducing the setting time of a mortar paste comprising the step of introducing a setting accelerator in a dry mortar blend, wherein the setting accelerator is in the form of a powder comprising calcium nitrate, wherein the powder has a water content between 0.1% by weight and 20% by weight and a particle size of 0.1 mm to 1 mm; and wherein upon mixing the dry mortar blend comprising the setting accelerator with water to make the mortar paste the setting time of the mortar paste is reduced.

2. The method according to claim 1 , wherein the powder is an anhydrous calcium nitrate powder having a water content between 0.1% by weight and 5% by weight.

3. The method according to claim 1 , wherein the powder comprises calcium nitrate and at least a different nitrate salt, the powder having a water content higher than 5% by weight and lower than 20% by weight.

4. The method according to claim 3 , wherein the different nitrate salt is potassium nitrate.

5. The method according to claim 3 , wherein the powder comprises 75 weight % to 80 weight % of calcium nitrate and 7 weight % to 11 weight % of potassium nitrate.

6. The method according to claim 3 , wherein the powder comprises a complex salt of calcium nitrate, potassium nitrate and water.

7. The method according to claim 1 , wherein the dry mortar blend comprising the setting accelerator does not clog nor cake and wherein the calcium nitrate in the dry mortar blend, upon mixing with water, does not precipitate.

8. Process for producing a setting accelerator for a dry mortar blend, the setting accelerator in the form of a powder comprising calcium nitrate, wherein the process comprises the step of cutting or grinding prills and/or granules comprising calcium nitrate and at least a different nitrate salt into a powder, wherein said powder serves as the setting accelerator and has a water content higher than 5% by weight and lower than 20% by weight and a particle size of 0.1 mm to 1 mm.

9. Process according to claim 8 , wherein the prills and/or granules are cut or grinded at a temperature between 10° C. and 40° C.

10. Process according to claim 8 , wherein the prills and/or granules are cut or grinded at a relative humidity of between 1% and 45%.

11. Process according to claim 8 , wherein the prills and/or granules are cut using rotating blades.

12. Process for producing a setting accelerator for a dry mortar blend, the setting accelerator in the form of a powder comprising calcium nitrate, wherein the process comprises the step of spray drying an aqueous solution at least comprising dissolved calcium nitrate, at a temperature between 150° C. and 250° C., into a powder, wherein said powder serves as the setting accelerator and has a water content between 0.1% by weight and 20% by weight and a particle size of 0.1 mm to 1 mm.

13. Process according to claim 12 , wherein the setting accelerator in the form of a powder comprising calcium nitrate has a water content between 0.1% by weight and 5% by weight.

14. Process according to claim 12 , wherein the aqueous solution comprises dissolved calcium nitrate and at least a different dissolved nitrate salt, and the setting accelerator in the form of a powder comprising calcium nitrate having a water content higher than 5% by weight and lower than 20% by weight.

15. Process according to claim 12 , wherein the aqueous solution comprises 50% by weight of dissolved calcium nitrate.

16. Dry mortar blend comprising at least a binder, an aggregate and a setting accelerator, wherein the setting accelerator is a powder comprising calcium nitrate and having a water content between 0.1% by weight and 20% by weight and a particle size of 0.1 mm to 1 mm.

17. Dry mortar blend according to claim 16 , wherein the dry mortar blend comprises a weight ratio of powder to binder of 0.005 to 0.05.

18. Dry mortar blend according to claim 16 , wherein the dry mortar blend comprises a weight ratio of aggregate to binder of between 2 and 4.

19. Dry mortar blend according to claim 16 , wherein, the dry mortar blend comprising the setting accelerator does not clog nor cake and wherein, upon mixing the dry mortar blend with water, the calcium nitrate does not precipitate.

Assignees

• Yara Int Asa

Inventors

• Franke Wolfram
• Langholm Anne Mette
• Thommesen Hilde Brekke Dahl
• Engesveen Bjørn Helge

Classifications

• C01F11/36

  Nitrates · CPC title

• C04B28/04

  Portland cements · CPC title

• C04B40/0042

  Powdery mixtures · CPC title

• C04B22/085 Primary

  containing nitrogen in the anion, e.g. nitrites · CPC title

• C04B28/02

  containing hydraulic cements other than calcium sulfates · CPC title