Method for producing capacitor

Patent metadata

Field	Value
Publication number	US-9607770-B2
Application number	US-201314409906-A
Country	US
Kind code	B2
Filing date	Apr 9, 2013
Priority date	Jun 22, 2012
Publication date	Mar 28, 2017
Grant date	Mar 28, 2017

Abstract

A capacitor having at least an anode body composed of a tungsten sintered compact and having less leakage current under high-voltage conditions and less variation in leakage current values, obtained by a production method including the steps of: compacting a tungsten powder to obtain a compression body; firing the compression body to obtain an anode body; applying voltage to the anode body, which is used as an positive electrode, in an alkaline fluid; chemically converting the surface layer of the anode body into a dielectric; optionally removing water from the anode body; and heat-treating the anode body, whose surface has been chemically converted into a dielectric, at a temperature of 100° C. or more and 260° C. or less.

First claim

The invention claimed is:

1. A method for producing a capacitor, in which the method comprises the steps of:
(1) applying voltage to a tungsten anode body, which is used as a positive electrode, in an alkaline fluid;
(2) chemically converting the surface of the anode body treated in the step (1) into a dielectric layer; and
(3) heat-treating the anode body treated in the step (2) at a temperature of 100° C. or more and 260° C. or less.

2. The production method according to claim 1 , wherein the tungsten anode body is composed of a sintered compact obtained by compacting a tungsten powder to obtain a compression body, and firing the compression body.

3. The production method according to claim 2 , wherein the voltage application in the step (1) is performed at a current of 0.1 to 20 mA per anode body.

4. The production method according to claim 2 , wherein the voltage application in the step (1) is performed at a voltage of 0.1 to 20 V.

5. The production method according to claim 2 , wherein the alkaline fluid is an aqueous solution containing at least one selected from the group consisting of alkali metal hydroxides, ammonia, and quaternary amines.

6. The production method according to claim 2 , wherein water is removed from the anode body after the step (2) and before the step (3).

7. The production method according to claim 1 , wherein the voltage application in the step (1) is performed at a current of 0.1 to 20 mA per anode body.

8. The production method according to claim 1 , wherein the voltage application in the step (1) is performed at a voltage of 0.1 to 20 V.

9. The production method according to claim 1 , wherein the alkaline fluid is an aqueous solution containing at least one selected from the group consisting of alkali metal hydroxides, ammonia, and quaternary amines.

10. The production method according to claim 1 , wherein water is removed from the anode body after the step (2) and before the step (3).

Assignees

• Showa Denko Kk
• Show A Denko K K

Inventors

• Naito Kazumi
• Tamura Katsutoshi

Classifications

• H01G9/0032 Primary

  formation of the dielectric layer · CPC title

• H01G9/0525

  Powder therefor · CPC title

• H01G9/15

  Solid electrolytic capacitors (H01G11/00 takes precedence) · CPC title

• H01G9/052

  Sintered electrodes · CPC title

• C25D11/26

  of refractory metals or alloys based thereon · CPC title