Apparatus for producing aligned carbon nanotube aggregates

Patent metadata

Field	Value
Publication number	US-9598285-B2
Application number	US-201013148619-A
Country	US
Kind code	B2
Filing date	Feb 8, 2010
Priority date	Feb 10, 2009
Publication date	Mar 21, 2017
Grant date	Mar 21, 2017

Abstract

An apparatus of the present invention for producing aligned carbon nanotube aggregates is an apparatus for producing aligned carbon nanotube aggregates, the apparatus being configured to grow the aligned carbon nanotube aggregate by: causing a catalyst formed on a surface of a substrate to be surrounded by a reducing gas environment constituted by a reducing gas; heating at least either the catalyst or the reducing gas; causing the catalyst to be surrounded by a raw material gas environment constituted by a raw material gas; and heating at least either the catalyst or the raw material gas, at least either an apparatus component exposed to the reducing gas or an apparatus component exposed to the raw material gas being made from a heat-resistant alloy, and having a surface plated with molten aluminum.

First claim

The invention claimed is:

1. An apparatus for producing aligned carbon nanotube aggregates,
the apparatus being configured to grow the aligned carbon nanotube aggregate by:
causing a catalyst formed on a surface of a substrate to be surrounded by a reducing gas environment constituted by a reducing gas;
heating at least either the catalyst or the reducing gas;
causing the catalyst to be surrounded by a raw material gas environment constituted by a raw material gas; and
heating at least either the catalyst or the raw material gas,
at least either an apparatus component exposed to the reducing gas or an apparatus component exposed to the raw material gas being made from a heat-resistant alloy, and having a surface plated with molten aluminum so as to have, between a base material, which is the heat-resistant alloy, and aluminum, an alloy layer of the heat-resistant alloy and aluminum,
the apparatus comprising:
a formation unit for causing the catalyst to be surrounded by the reducing gas environment constituted by the reducing gas, and heating at least either the catalyst or the reducing gas;
a growth unit for growing the aligned carbon nanotube aggregate by causing the catalyst to be surrounded by the raw material gas environment constituted by the raw material gas, and heating at least either the catalyst or the raw material gas; and
a transfer unit for transferring the substrate at least from the formation unit to the growth unit,
the formation unit including a formation furnace in which the reducing gas is retained, a reducing gas ejection section for ejecting the reducing gas, and a heater for heating at least either the catalyst or the reducing gas,
the growth unit including a growth furnace in which the raw material gas is retained, a raw material gas ejection section for ejecting the raw material gas, and a heater for heating at least either the catalyst or the raw material gas,
the transfer unit including a mesh belt and a belt driven section,
one of the apparatus components which have been plated with molten aluminum being the growth furnace, in which an environment of high-carbon concentration is retained, the environment of high-carbon concentration being an environment in which a proportion of the raw material gas to a total flow is approximately 2% to 20%,
wherein the base material, which is the heat-resistant alloy, includes at least one selected from the group consisting of a heat-resistant steel, stainless steel, and a nickel-based alloy, and wherein the apparatus component is not the substrate.

Assignees

• Shibuya Akiyoshi
• Kawata Keiichi
• Hata Kenji
• Yumura Motoo
• Zeon Corp
• Nat Inst Advanced Ind Science & Tech

Inventors

• Shibuya Akiyoshi
• Kawata Keiichi
• Hata Kenji
• Yumura Motoo

Classifications

• B01J19/22

  in the form of endless belts · CPC title

• B01J2219/0894

  Processes carried out in the presence of a plasma · CPC title

• B01J2219/00159

  controlling multiple zones along the direction of flow, e.g. pre-heating and after-cooling · CPC title

• B82Y40/00

  Manufacture or treatment of nanostructures · CPC title

• C01B32/158 Primary

  Carbon nanotubes · CPC title