Process for producing purified essential oil

Patent metadata

Field	Value
Publication number	US-9580668-B2
Application number	US-201213466370-A
Country	US
Kind code	B2
Filing date	May 8, 2012
Priority date	Nov 11, 2008
Publication date	Feb 28, 2017
Grant date	Feb 28, 2017

Abstract

It is provided a process for producing a purified essential oil excellent in safety and quality with high productivity from an essential oil comprising a harmful contaminant such as an agricultural chemical by simply and smoothly removing the contaminant with high removal rate without causing poor balance of flavor which the essential oil originally has, decrease of flavor strength and the like. It relates to a process for producing a purified essential oil by treating an essential oil comprising a contaminant with an active carbon to remove the contaminant and the removal rate of the contaminant is further improved by using an active carbon activated with a chemical, particularly an active carbon activated with zinc chloride, in the treatment, or by conducting the treatment at a low temperature of room temperature or lower, particularly at −25° C. to 5° C.

First claim

The invention claimed is:

1. A process for producing a purified citrus oil, comprising
a) contacting a citrus oil comprising a contaminant with an active carbon to prepare a suspension;
b) stirring the suspension at a temperature of from −30° C. to 5° C. for 10 minutes to 2 hours; and
c) recovering the purified citrus oil from which the contaminant is removed,
wherein the active carbon is an activated active carbon activated with zinc chloride,
wherein the contaminant is a residual agricultural chemical which is one kind or a mixture of two or more kinds selected from ortho-phenyl phenol, chloroneb, simazine, carbaryl, chlorpyrifos, imazalil, thiabendazole and diphenyl,
wherein the active carbon is added in an amount of 0.5 to 10% by mass, based on the mass of the citrus oil comprising a contaminant, and
wherein flavor and odor components of the citrus oil, selected from the group consisting of nootkatone, octanal, nonanal, decanal, dodecanal and linalool, remain unchanged in the obtained purified citrus oil.

2. The process for producing a purified citrus oil according to claim 1 , wherein the citrus oil is one kind or a mixture of two or more kinds selected from lemon oil, sweet orange oil, bitter orange oil, lime oil, grapefruit oil, bergamot oil, mandarin oil, Yuzu oil (Citrus junos oil) and Sudachi oil (Citrus sudachi oil).

Assignees

• Takeuchi Ryo
• Oshikubo Shigemasa
• Takasago Perfumery Co Ltd

Inventors

• Takeuchi Ryo
• Oshikubo Shigemasa

Classifications

• C11B9/022 Primary

  Refining · CPC title

• B01D15/00

  Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor · CPC title

• A23L27/12

  from fruit, e.g. essential oils · CPC title

• A23L2/56

  Flavouring or bittering agents (sweeteners A23L2/60) · CPC title

• A23V2002/00

  Food compositions, function of food ingredients or processes for food or foodstuffs · CPC title