Method for production of performance enhanced metallic materials

Patent metadata

Field	Value
Publication number	US-9561538-B2
Application number	US-201314102753-A
Country	US
Kind code	B2
Filing date	Dec 11, 2013
Priority date	Dec 11, 2013
Publication date	Feb 7, 2017
Grant date	Feb 7, 2017

Abstract

A method for production of a metallic material from a semifinished metallic billet, the semifinished metallic billet including a nanocrystalline microstructure and/or an ultrafine-grained microstructure, the method including the steps of (1) subjecting the semifinished metallic billet to a rotary incremental forming process to form an intermediate wrought metallic billet, and (2) subjecting the intermediate wrought metallic billet to a high rate forming process to form a metallic product.

First claim

What is claimed is:

1. A method for production of metallic material from a semifinished metallic billet, said semifinished metallic billet comprising at least one of a nanocrystalline microstructure and an ultrafine-grained microstructure, said method comprising:
subjecting said semifinished metallic billet to a rotary incremental forming process to form an intermediate wrought metallic billet; and
subjecting said intermediate wrought metallic billet to a high rate forming process, said high rate forming process being defined by an average equivalent strain rate of at least about 10 s −1 .

2. The method of claim 1 wherein said rotary incremental forming process comprises a rotary swaging process.

3. The method of claim 1 wherein said high rate forming process comprises an extrusion process.

4. The method of claim 1 wherein said rotary incremental forming process comprises a rotary incremental forming process temperature (in degrees Kelvin), said rotary incremental forming process temperature being at most about 90 percent of a melting temperature (in degrees Kelvin) of said semifinished metallic billet.

5. The method of claim 4 wherein said high rate forming process comprises a high rate forming process temperature (in degrees Kelvin), said high rate forming process temperature being at most about 90 percent of said melting temperature (in degrees Kelvin) of said semifinished metallic billet.

6. The method of claim 5 wherein said high rate forming process temperature is less than said rotary incremental forming process temperature.

7. The method of claim 1 further comprising:
providing a metallic material powder;
subjecting said metallic material powder to a cryomilling process to form a cryomilled metallic material powder comprising said microstructure; and
subjecting said cryomilled metallic material powder to a consolidating process to form said semifinished metallic billet comprising said microstructure.

8. The method of claim 7 wherein said consolidating process comprises:
a consolidating temperature, said consolidating temperature ranging from about 30 percent to about 90 percent of a melting temperature (in degrees Kelvin) of said metallic material powder; and
a consolidating pressure, said consolidating pressure being at least 3,000 psi.

9. The method of claim 7 further comprising subjecting said cryomilled metallic material powder to a degassing process before subjecting said cryomilled metallic material powder to said consolidating process.

10. The method of claim 9 wherein said degassing process comprises a degassing temperature, said degassing temperature ranging from about 30 percent to about 90 percent of a melting temperature (in degrees Kelvin) of said metallic material powder.

11. A method for production of a metallic material from a metallic material powder, said method comprising:
subjecting said metallic material powder to a cryomilling process to form a cryomilled metallic material powder comprising at least one of a nanocrystalline microstructure and an ultrafine-grained microstructure;
subjecting said cryomilled metallic material powder to a degassing process to form a degassed metallic material powder;
subjecting said degassed metallic material powder to a consolidating process to form a semifinished metallic billet, said semifinished metallic billet comprising at least one of the nanocrystalline microstructure and the ultrafine-grained microstructure;
subjecting said semifinished metallic billet to a rotary incremental forming process to form an intermediate wrought metallic billet; and
subjecting said intermediate wrought metallic billet to a high rate forming process, said high rate forming process being defined by an average equivalent strain rate of at least about 0.1 s −1 .

12. The method of claim 11 wherein said metallic material powder comprises at least one of aluminum, aluminum alloy, titanium, titanium alloy, iron-based alloy, nickel, nickel alloy, cobalt, cobalt alloy, a refractory metal, a refractory alloy, magnesium, magnesium alloy, copper, copper alloy, a precious metal, a precious metal alloy, zinc, zinc alloy, zirconium, zirconium alloy, hafnium, hafnium alloy, an intermetallic, and a metal matrix material.

13. The method of claim 11 wherein said rotary incremental forming process comprises a rotary incremental forming process temperature, said rotary incremental forming process temperature being at most about 90 percent of a melting temperature (in degrees Kelvin) of said semifinished metallic billet.

14. The method of claim 11 wherein said high rate forming process comprises a high rate forming process temperature, said high rate forming process temperature being at most about 90 percent of a melting temperature (in degrees Kelvin) of said semifinished metallic billet.

15. The method of claim 11 wherein said average equivalent strain rate is at least about 10 s −1 .

16. A method for production of an aluminum alloy from a semifinished aluminum alloy billet, said semifinished aluminum alloy billet comprising at least one of nanocrystalline microstructure and an ultrafine-grained microstructure, said method comprising:
subjecting said semifinished aluminum alloy billet to a rotary swaging process to form an intermediate wrought aluminum alloy billet; and
subjecting said intermediate wrought aluminum alloy billet to a high rate extrusion process, said high rate extrusion process being defined by an average equivalent strain rate of at least about 0.1 s −1 .

17. The method of claim 16 wherein said rotary swaging process comprises a rotary swaging temperature, said rotary swaging temperature being greater than ambient temperature and less than 90 percent of a melting temperature (in degrees Kelvin) of said semifinished aluminum alloy billet.

18. The method of claim 17 wherein said high rate extrusion process is performed at ambient temperature.

19. The method of claim 16 wherein said average equivalent strain rate is at least about 10 s −1 .

Assignees

• Boeing Co

Inventors

• Yousefiani Ali

Classifications

• B22F2999/00

  Aspects linked to processes or compositions used in powder metallurgy · CPC title

• B22F2998/10

  Processes characterised by the sequence of their steps · CPC title

• B22F3/20

  by extruding · CPC title

• B22F9/082

  atomising using a fluid (using centrifugal force B22F9/10) · CPC title

• C21D7/00

  Modifying the physical properties of iron or steel by deformation (apparatus for mechanical working of metal B21, B23, B24) · CPC title