Apparatus for producing mixed solution and method for preparing mixed solution

Patent metadata

Field	Value
Publication number	US-9561479-B2
Application number	US-201213980220-A
Country	US
Kind code	B2
Filing date	Jan 31, 2012
Priority date	Jan 31, 2011
Publication date	Feb 7, 2017
Grant date	Feb 7, 2017

Abstract

An apparatus for producing a mixed solution, comprising a mixing vessel for preparing an aqueous mixed solution containing a dicarboxylic acid and a Nb compound and a filter for the aqueous mixed solution connected to the mixing vessel via a pipe, the mixing vessel being anticorrosive and equipped with a stirring unit, a heating unit and a cooling unit for the aqueous mixed solution, wherein the aqueous mixed solution prepared in the mixing vessel is fed to the filter via the pipe and filtered in the filter under increased pressure.

First claim

What is claimed is:

1. An apparatus for producing a mixed solution, comprising:
a mixing vessel containing an aqueous solution containing a dicarboxylic acid and a niobium compound and having a stirring unit to mix the aqueous solution to obtain an aqueous mixed solution and a heating or cooling unit to heat or cool the aqueous solution, wherein the mixing vessel is anticorrosive;
a filter for the aqueous mixed solution connected to the mixing vessel via a pipe; and
a container for storing a filtrate comprising a filtered said aqueous mixed solution, wherein
the mixing vessel is configured to apply a temperature induced pressure, which is induced by the heating or cooling unit, to the filter via the pipe such that the aqueous mixed solution prepared in the mixing vessel, which has been fed to the filter via the pipe, is filtered in the filter under an increased pressure,
wherein the container for storing the filtrate is connected to the filter and is equipped with a concentration measuring unit configured to measure the concentration of the filtrate and a concentration adjusting unit configured to adjust the concentration of the filtrate, and
wherein the mixing vessel is further equipped with a pressure adjusting unit configured to apply a pressure to or release a pressure from the mixing vessel, so that a pressure in the mixing vessel is adjusted by the pressure adjusting unit.

2. The apparatus for producing the mixed solution according to claim 1 , wherein the filter has a jacket and a heating medium and/or a cooling medium is fed into the jacket to adjust a temperature of the filter.

3. The apparatus for producing the mixed solution according to claim 1 or 2 , wherein the mixing vessel has a jacket as the heating or cooling unit, so that the jacket serves as a heating unit by feeding a heating medium into the jacket and the jacket serves as a cooling unit by feeding a cooling medium into the jacket.

4. The apparatus for producing the mixed solution according to claim 1 or 2 , wherein the mixing vessel is made of a glass and/or a fluoro-based resin or has an inner surface coated with a glass and/or a fluoro-based resin.

5. The apparatus for producing the mixed solution according to claim 1 , wherein
the concentration adjusting unit comprises a pot for containing a dicarboxylic acid and/or a niobium,
the container for storing the filtrate and the pot is connected by a pipe via a pump, so that the filtrate i) is introduced from the container to the pot through the pipe, ii) contacts with dicarboxylic acid and/or niobium to dissolve the dicarboxylic acid and/or niobium in the pot, and ii) returns to the container through the pipe, whereby the mixed solution is adjusted to an intended dicarboxylic acid concentration and/or niobium concentration, when the dicarboxylic acid concentration and/or niobium concentration of the mixed solution, as determined by the concentration measuring unit, is lower than the intended dicarboxylic acid concentration and/or niobium concentration.

Assignees

• Ishii Yusuke
• Kato Takaaki
• Asahi Kasei Chemicals Corp

Inventors

• Ishii Yusuke
• Kato Takaaki

Classifications

• B01J2523/00

  Constitutive chemical elements of heterogeneous catalysts · CPC title

• B01F1/0016

  Operations & Transport · mapped topic

• C07C51/412

  by conversion of the acids, their salts, esters or anhydrides with the same carboxylic acid part · CPC title

• B01J2523/68

  Molybdenum · CPC title

• B01J2523/53

  Antimony · CPC title