Environmentally benign production of graphene materials
US-2016244333-A1 · Aug 25, 2016 · US
US9556033B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-9556033-B2 |
| Application number | US-201113879223-A |
| Country | US |
| Kind code | B2 |
| Filing date | Oct 17, 2011 |
| Priority date | Oct 20, 2010 |
| Publication date | Jan 31, 2017 |
| Grant date | Jan 31, 2017 |
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An expanded graphite sheet is provided that can remarkably improve the quality and yield rate by preventing chipping and cracks in the surface in molding the sheet into a desired shape by inhibiting degradation in the flexibility while reducing the ash content to a certain degree. An expanded graphite sheet ( 3 ) has a flexibility of 25 times or greater, as determined in a flexibility test in which the flexibility is defined as the number of times the expanded graphite sheet ( 3 ) can be bent using a flexibility testing device having a rotator ( 2 ) to which one end of a plate-shaped expanded graphite sheet ( 3 ) is fixed, a weight ( 7 ) fixed to the other end of the expanded graphite sheet ( 3 ), and a bending position determining member ( 5 ) for determining a bending position of the expanded graphite sheet ( 3 ) when the rotator ( 2 ) is rotated.
Opening claim text (preview).
The invention claimed is: 1. An expanded graphite sheet characterized by having a flexibility of 25 times or greater and an ash content of 500 ppm or lower, the flexibility being determined by a flexibility test in which the flexibility is defined as the number of times the expanded graphite sheet can be bent using a flexibility testing device comprising a rotator to which one end of a plate-shaped expanded graphite sheet is fixed, a weight fixed to the other end of the expanded graphite sheet, and a bending position determining member for determining a bending position of the expanded graphite sheet when the rotator is rotated, wherein the expanded graphite sheet is set to have a width of 10 mm, a thickness of 0.42 mm, and a length of a drooping portion thereof from the rotator of 90 mm, the weight is set at 50 g, the swing angles of the rotator in lateral directions are set at 30 degrees with respect to a vertical direction, and an arrangement position of the bending position determining member is set at 20 mm from a lower end of the expanded graphite sheet and; wherein the content of sulfur is 500 ppm or higher. 2. The expanded graphite sheet according to claim 1 , wherein the content of ash is 300 ppm or lower and the content of sulfur is 1000 ppm or higher.
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