System and method for increasing the bulk density of metal powder

Patent metadata

Field	Value
Publication number	US-9555473-B2
Application number	US-201113269587-A
Country	US
Kind code	B2
Filing date	Oct 8, 2011
Priority date	Oct 8, 2011
Publication date	Jan 31, 2017
Grant date	Jan 31, 2017

Abstract

An apparatus for increasing the bulk density of metal powder may include a sealed chamber, a nozzle, and a target. The sealed chamber may include an inert environment. The nozzle may be coupled to an inert gas source and may be configured to introduce raw metal powder into a flow of the inert gas for discharge as a cold spray mixture of the raw metal powder and the inert gas into the chamber. The target may be housed within the sealed chamber and may be configured to receive an impact of the cold spray mixture. The nozzle and the target may be configured to flatten the raw metal particles into flattened metal particles in response to the cold spray mixture impacting the target.

First claim

What is claimed is:

1. A method of increasing a bulk density of metal powder formed of a metal material, comprising the steps of:
introducing raw metal powder containing raw metal particles into a flow of inert gas to form a cold spray mixture;
directing the cold spray mixture toward a target housed within a sealed chamber;
impacting the cold spray mixture against the target;
densifying the raw metal powder by plastically deforming the raw metal particles into flattened metal particles in loose form to produce a flattened metal powder consisting of the flattened metal particles prior to compaction of the flattened metal powder, wherein densifying the raw metal powder produces the flattened metal powder having a bulk density higher than that of the raw metal powder to an extent that the flattened metal powder has the bulk density of at least approximately 10 percent of a theoretical density of the metal material;
receiving the flattened metal powder in an elastomeric bag having flexible walls and sealed to the sealed chamber during the densifying step;
placing the elastomeric bag containing the flattened metal powder within a chamber;
injecting fluid between the elastomeric bag and chamber walls; and
hydrostatically pressurizing the elastomeric bag in the chamber using fluid pressure to cause the compaction of the flattened metal powder and form a green structure using a cold isostatic process.

2. The method of claim 1 wherein the step of deforming the raw metal particles comprises:
deforming the raw metal particles into flattened metal particles having a bulk density of at least approximately 50 percent of the theoretical density.

3. The method of claim 1 further comprising the step of:
maintaining the sealed chamber at a sub-atmospheric pressure.

4. The method of claim 1 further comprising the step of:
recirculating the inert gas from the chamber to a nozzle.

5. The method of claim 1 further comprising the step of:
maintaining a temperature of the metal powder below a melting point thereof.

6. The method of claim 5 further comprising one of the following steps:
cooling the target to prevent bonding of the metal particles to the target;
heating the target to promote softening of the metal particles and plastic deformation thereof during impaction of the metal particles against the target.

7. The method of claim 1 further comprising the step of:
preventing exposure of the flattened metal particles to an external atmosphere when the flattened metal particles are received within the elastomeric bag.

8. The method of claim 1 wherein the inert gas comprises hydrogen, the hydrogen gas being contained within the green structure, the method further comprising the step of:
removing the hydrogen gas from the green structure by sintering the green structure in a vacuum.

9. The method of claim 1 wherein the metal powder comprises at least one of the following materials:
titanium, titanium alloy, aluminum, aluminum alloy, iron, iron alloy, steel, steel alloy, nickel-based alloy, copper-based alloy, beryllium, beryllium-based alloy, cobalt, cobalt-based alloy, molybdenum, molybdenum-based alloy, tungsten, and tungsten-based alloy.

Assignees

• Slattery Kevin Thomas
• Boeing Co

Inventors

• Slattery Kevin Thomas

Classifications

• B22F9/026

  Spray drying of solutions or suspensions · CPC title

• C23C24/06

  Compressing powdered coating material, e.g. by milling · CPC title

• B22F3/16

  in successive or repeated steps · CPC title

• B22F3/003

  Apparatus, e.g. furnaces (in general F27B) · CPC title

• B22F2201/20

  Use of vacuum · CPC title