Method and device for coating a series of support bodies

Patent metadata

Field	Value
Publication number	US-9551253-B2
Application number	US-66559105-A
Country	US
Kind code	B2
Filing date	Oct 14, 2005
Priority date	Oct 19, 2004
Publication date	Jan 24, 2017
Grant date	Jan 24, 2017

Abstract

The accuracy of the coating concentration when applying a catalytically active coating to suitable carrier bodies can be increased if, following raw coating with a relatively wide fluctuation range in the coating concentration, excessive or insufficient coating applied is if appropriate corrected iteratively. Excessive coating suspension applied is removed, for example by subsequent suction, while the coating is still in the wet state, whereas insufficient coating suspension applied is topped up, for example by spraying on additional coating suspension.

First claim

What is claimed is:

1. A method for coating a series of open-pored bodies with at least one coating suspension for producing coated bodies having a predetermined catalytic activity, comprising
a) performing a raw coating process comprising introducing to the bodies a first quantity of the coating suspension that is greater than a target coating quantity and removing a second quantity of the coating suspension that is designed to yield on the bodies a raw coating of the coating suspension that is made to be below the target coating quantity, the target coating quantity being the minimum quantity of coating suspension that is required, in the wet state, for achieving the predetermined catalytic activity;
b) determining the raw coating quantity produced on the bodies; and
c) correcting the raw coating quantity by introducing a third quantity of coating suspension to the raw coating quantity while the raw coating is still wet, so that a final coating quantity is made to be equal to or greater than the target coating quantity,
wherein the raw coating process of step a) has a predetermined fluctuation range that defines a minimum quantity of raw coating that the process is predetermined to apply to a body and a maximum quantity of raw coating that the process is predetermined to apply to a body, and
wherein any difference between the target coating quantity and the final coating quantity applied in step c) is less than half the difference between the predetermined minimum and maximum quantities of raw coating defined by the fluctuation range of the raw coating process of step a).

2. The method according to claim 1 , in which the raw coating quantity is determined by weighing the bodies before and after the coating operation in step a).

3. The method according to claim 1 , in which the bodies to be coated in step a) are oriented vertically and are filled with the first quantity of coating suspension via a lower end face.

4. The method according to claim 1 , in which the second quantity of coating suspension is removed from the bodies in step a) by pumping, sucking, blowing or a combination of these actions.

5. The method according to claim 1 , in which the coating of the carrier bodies is dried and calcined after step c).

6. The method according to claim 1 , wherein the third quantity of coating suspension is introduced via an upper end face of the carrier bodies, while the carrier bodies are vertically aligned.

7. The method according to claim 1 , wherein the third quantity of coating suspension is distributed over the length of the carrier bodies by sucking or blowing.

8. A method for coating an open-pored body with at least one coating suspension for producing a coated body having a predetermined catalytic activity, comprising
a) performing a raw coating process comprising introducing to the body a first quantity of the coating suspension that is greater than a target coating quantity and removing from the body a second quantity of the coating suspension that is designed to yield on the body a raw coating of the coating suspension that is made to be below the target coating quantity, the target coating quantity being the minimum quantity of coating suspension that is required, in the wet state, for achieving the predetermined catalytic activity;
b) determining the quantity of raw coating produced on the body; and
c) correcting the raw coating by introducing a third quantity of coating suspension to the raw coating while the raw coating is still wet, so that a final coating quantity is made to be equal to or greater than the target coating quantity,
wherein the raw coating process of step a) has a predetermined fluctuation range that defines a minimum quantity of raw coating that the process is predetermined to apply to a body and a maximum quantity of raw coating that the process is predetermined to apply to a body,
wherein any difference between the target coating quantity and the final coating quantity applied in step c) is less than half the difference between the predetermined minimum and maximum quantities of raw coating defined by the fluctuation range of the raw coating process of step a), and
wherein, in step c) the quantity of raw coating is brought closer to the target coating quantity by introducing the third quantity of coating suspension to an upper end face of the carrier body, and then distributing the third quantity of coating suspension over the length of the carrier body by sucking or blowing.

9. A method for coating an open-pored body with at least one coating suspension for producing a coated body having a predetermined catalytic activity, comprising
a) performing a raw coating process comprising introducing to the body a first quantity of the coating suspension that is greater than a target coating quantity and removing from the body a second quantity of the coating suspension that is designed to yield on the body a raw coating of the coating suspension that is made to be below the target coating quantity, the target coating quantity being the minimum quantity of coating suspension that is required, in the wet state, for achieving the predetermined catalytic activity;
b) determining the quantity of raw coating produced on the body; and
c) correcting the raw coating by introducing a third quantity of coating suspension to the raw coating while still wet, so that a final coating quantity is made to be equal to or greater than the target coating quantity,
wherein the raw coating process of step a) has a predetermined fluctuation range that defines a minimum quantity of raw coating that the process is predetermined to apply to a body and a maximum quantity of raw coating that the process is predetermined to apply to a body,
wherein any difference between the target coating quantity and the final coating quantity applied in step c) is less than half the difference between the predetermined minimum and maximum quantities of raw coating defined by the fluctuation range of the raw coating process of step a), and
wherein the additional coating suspension is distributed over the entire length of the raw coating produced in step a).

Assignees

• Fehnle Oliver
• Detterbeck Dieter
• Wienand Axel
• Mergner Bernd
• Umicore Ag & Co Kg

Inventors

• Fehnle Oliver
• Detterbeck Dieter
• Wienand Axel
• Mergner Bernd

Classifications

• F01N2510/06

  for exhaust purification, e.g. catalytic reaction · CPC title

• B01J37/0215

  Coating · CPC title

• B05D7/22

  to internal surfaces, e.g. of tubes · CPC title

• B01J35/04

  Operations & Transport · mapped topic

• F01N3/2803 Primary

  characterised by structure, by material or by manufacturing of catalyst support · CPC title