Systems and methods for forming and processing alloy ingots

Patent metadata

Field	Value
Publication number	US-9533346-B2
Application number	US-201414278134-A
Country	US
Kind code	B2
Filing date	May 15, 2014
Priority date	Feb 5, 2010
Publication date	Jan 3, 2017
Grant date	Jan 3, 2017

Abstract

Processes and methods related to producing, processing, and hot working alloy ingots are disclosed. An alloy ingot is formed including an inner ingot core and an outer layer metallurgically bonded to the inner ingot core. The processes and methods are characterized by a reduction in the incidence of surface cracking of the alloy ingot during hot working.

First claim

What is claimed is:

1. A process for forming an alloy ingot comprising:
vacuum induction melting a nickel-base alloy to form a first alloy electrode;
electroslag refining the first alloy electrode to form a second, refined alloy electrode; and
vacuum arc remelting the second, refined alloy electrode into an alloy liner positioned in a crucible of a vacuum arc remelting apparatus, thereby forming an alloy ingot comprising an outer layer metallurgically bonded to an inner ingot core;
wherein the vacuum arc remelting apparatus comprises a head that mates with the crucible to form a sealed furnace chamber surrounding the alloy liner and the second, refined alloy electrode, and wherein a vacuum is drawn within the sealed furnace chamber during the vacuum arc remelting.

2. The process of claim 1 , wherein the outer layer comprises a nickel-base alloy that is more ductile than the nickel-base alloy comprising the inner ingot core.

3. The process of claim 1 , wherein the nickel-base alloy comprises, in weight percent, 0 to 0.08 carbon, 0 to 0.35 manganese, 0 to 0.35 silicon, 0 to 0.015 sulfur, 0 to 0.015 phosphorus, 17.0 to 21.0 chromium, 50.0 to 55.0 nickel, 0 to 1.0 cobalt, 2.8 to 3.3 molybdenum, 0.65 to 1.15 titanium, 0.20 to 0.80 aluminum, 0 to 0.006 boron, 5.0 to 5.5 niobium and/or tantalum, balance iron and incidental impurities.

4. The process of claim 1 , wherein the alloy liner comprises an alloy comprising, in weight percent, 0 to 0.10 carbon, 0 to 0.50 manganese, 0 to 0.50 silicon, 0 to 0.015 sulfur, 0 to 0.015 phosphorus, 20.0 to 22.0 chromium, 0 to 1.0 cobalt, 0 to 5.0 iron, 8.0 to 10.0 molybdenum, 0 to 0.40 titanium, 0 to 0.40 aluminum, 3.15 to 4.15 niobium and/or tantalum, balance nickel and incidental impurities.

5. The process of claim 1 , further comprising:
hot working the alloy ingot, wherein the hot working comprises applying force onto the outer layer, and wherein the force plastically deforms the alloy ingot.

6. The process of claim 5 , wherein hot working the alloy ingot comprises upset-and-draw forging the alloy ingot.

7. The process of claim 5 , further comprising removing at least a portion of the outer layer from the alloy ingot after hot working the alloy ingot.

8. The process of claim 1 , wherein a metallurgical bond between the outer layer and the inner ingot core comprises an alloy gradient region in which the composition of the ingot transitions along a gradient from an electrode alloy composition to a liner alloy composition.

9. The process of claim 1 , wherein the alloy liner has a wall thickness in the range of 0.25 inches to 0.5 inches.

10. The process of claim 1 , further comprising metallurgically bonding an end layer on to at least one end of the alloy ingot comprising an outer layer metallurgically bonded to an inner ingot core.

11. The process of claim 1 , further comprising metallurgically bonding end layers on to opposed ends of the alloy ingot comprising an outer layer metallurgically bonded to an inner ingot core, wherein the inner ingot core is enclosed within an outer circumferential layer and two end layers.

12. The process of claim 1 , wherein the vacuum arc remelting comprises:
forming an arc in an electrode arc gap between a free end of the refined alloy electrode and a base plate in the crucible or a closed end of the alloy liner;
dripping molten alloy from the free end of the refined alloy electrode, through the electrode arc gap, and into the alloy liner; and
moving the refined alloy electrode to maintain the electrode arc gap as molten alloy drips from the free end of the refined alloy electrode, through the electrode arc gap, and into the alloy liner.

13. The process of claim 1 , wherein the vacuum arc remelting comprises:
positioning the refined alloy electrode in the vacuum arc remelting apparatus connected to a ram;
sealing the refined alloy electrode and alloy liner inside a furnace chamber formed by the crucible and a mating head, wherein the ram is movably positioned through a sealed opening in the head;
drawing a vacuum within the furnace chamber;
forming an arc in an electrode arc gap between a free end of the refined alloy electrode and a base plate in the crucible or a closed end of the alloy liner;
dripping molten alloy from the free end of the refined alloy electrode, through the electrode arc gap, and into the alloy liner; and
moving the refined alloy electrode with the ram to maintain the electrode arc gap as molten alloy drips from the free end of the alloy electrode, through the electrode arc gap, and into the alloy liner.

Assignees

• Ati Properties Inc
• Ati Properties Llc

Inventors

• Minisandram Ramesh S

Classifications

• B22D7/02

  Casting compound ingots of two or more different metals in the molten state, i.e. integrally cast · CPC title

• Y10T428/12493

  Composite; i.e., plural, adjacent, spatially distinct metal components [e.g., layers, joint, etc.] · CPC title

• F27B2014/045

  Vacuum · CPC title

• C22B9/20 Primary

  Arc remelting · CPC title

• B21J5/00

  Methods for forging, hammering, or pressing (for working sheet-metal or metal tubes, rods, or profiles B21D; for working wire B21F); Special equipment or accessories therefor · CPC title