Method of making granular detergent compositions comprising surfactants

Patent metadata

Field	Value
Publication number	US-9528080-B2
Application number	US-201414446575-A
Country	US
Kind code	B2
Filing date	Jul 30, 2014
Priority date	Jul 30, 2013
Publication date	Dec 27, 2016
Grant date	Dec 27, 2016

Abstract

A process of making a granular detergent composition comprising the steps of:
a) forming an aqueous detergent slurry; b) spray drying the aqueous detergent slurry to form a plurality of spray-dried detergent particles; c) forming an emulsion comprising a surfactant; and d) adding the emulsion from step c) to at least a portion of the plurality of spray-dried detergent particles.

First claim

What is claimed is:

1. A process of making a granular detergent composition comprising the steps of:
a) forming an aqueous detergent slurry;
b) spray drying said aqueous detergent slurry to form a plurality of spray-dried detergent particles;
c) separately forming an emulsion comprising:
i. forming a first liquid comprising a graft copolymer of polyethylene oxide with vinyl acetate;
ii. forming a second liquid comprising a surfactant;
iii. passing the first and second liquids through a high shear mixer;
iv. mixing the first and second liquids to form the emulsion; and

d) adding the emulsion from step c) to at least a portion of said plurality of spray-dried detergent particles,
wherein an optical brightener is added to the first or second liquid, or an optical brightener is added to the emulsion once it is formed in step iv; wherein the weight ratio of the polyethylene oxide to vinyl acetate is from about 1:0.2 to about 1:10; and
wherein said aqueous detergent slurry comprises from about 0 wt % to about 5 wt % zeolite builder and from about 0 wt % to about 5 wt % of phosphate builder.

2. A process according to claim 1 , wherein the surfactant is selected from an anionic, cationic, zwitterionic or non-ionic surfactant.

3. A process according to claim 2 , wherein the surfactant is a non-ionic surfactant.

4. The process according to claim 1 , wherein the aqueous detergent slurry further comprises a detersive surfactant.

5. The process according to claim 1 , wherein the aqueous detergent slurry further comprises at least one additional detergent ingredient.

6. The process according to claim 1 , wherein the aqueous detergent slurry further comprises an alkalinity source.

7. The process according to claim 1 , wherein the emulsion is at a temperature of from about 30° C. to about 60° C., prior to it being added to the detergent particles.

Assignees

• Procter & Gamble

Inventors

• Tantawy Hossam Hassan
• Gault Sabrina Beatrice Danielle
• Patton Andrew Brian Greenaway
• Porter Adam
• Walker Stephen John
• Ahmadian Hossein

Classifications

• C11D11/02

  Preparation in the form of powder by spray drying · CPC title

• C11D3/3788 Primary

  Graft polymers · CPC title

• C11D17/0017 Primary

  Multi-phase liquid compositions · CPC title