Organotemplate-Free Solid-State Synthetic Method For Zeolite Molecular Sieves
US-2015298983-A1 · Oct 22, 2015 · US
US9527751B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-9527751-B2 |
| Application number | US-201213673661-A |
| Country | US |
| Kind code | B2 |
| Filing date | Nov 9, 2012 |
| Priority date | Nov 11, 2011 |
| Publication date | Dec 27, 2016 |
| Grant date | Dec 27, 2016 |
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The present invention relates to an organotemplate-free synthetic process for the production of a zeolitic material having a CHA-type framework structure comprising YO 2 , X 2 O 3 , and optionally comprising Z 2 O 5 , wherein said process comprises the steps of: (1) providing a mixture comprising one or more sources for YO 2 , one or more sources for X 2 O 3 , and seed crystals having a CHA framework structure, wherein the CHA framework structure of the seed crystals comprises YO 2 , X 2 O 3 , and optionally comprises Z 2 O 5 ; and (2) crystallizing the mixture obtained in step (1); wherein Y is a tetravalent element, X is a trivalent element, and Z is a pentavalent element, wherein optionally one or more sources for Z 2 O 5 are further provided in step (1), and wherein if the CHA framework of the seed crystals does not contain Z 2 O 5 , the seed crystals then have a YO 2 :X 2 O 3 molar ratio of 5 or greater than 5.
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What is claimed is: 1. An organotemplate-free synthetic process for the production of a zeolitic material having a CHA-type framework structure comprising YO 2 , X 2 O 3 , and optionally comprising Z 2 O 5 , wherein said process comprises the steps of: (1) providing a mixture comprising one or more sources for YO 2 , one or more sources for X 2 O 3 , and seed crystals having a CHA framework structure, wherein the CHA framework structure of the seed crystals comprises YO 2 , X 2 O…
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