Method for producing a doped SiO2 slurry and use of the SiO2 slurry

Patent metadata

Field	Value
Publication number	US-9518218-B2
Application number	US-201314411332-A
Country	US
Kind code	B2
Filing date	Jun 25, 2013
Priority date	Jun 26, 2012
Publication date	Dec 13, 2016
Grant date	Dec 13, 2016

Abstract

The invention relates to a method for producing a doped SiO 2 slurry in which an SiO 2 suspension is brought into interaction with at least one doping solution, wherein the SiO 2 suspension and/or the doping solution act on one another in the form of an atomized spray, the average droplet diameter of which is in the range between 10 μm and 100 μm. The invention further relates to the use of an SiO 2 slurry doped by the atomized spray method for the production of doped quartz glass, particularly for the production of laser-active quartz glass.

First claim

The invention claimed is:

1. A method for producing a doped SiO 2 slurry, said method comprising:
providing at least one doping solution continually to a SiO 2 suspension that contains SiO 2 particles in an aqueous liquid so as to form the doped SiO 2 slurry,
wherein, while the doped SiO 2 slurry is being formed, an at least partially doped SiO 2 slurry is continuously kept in motion, and
wherein the SiO 2 suspension and the doping solution act on each other with the SiO 2 suspension and/or the doping solution being in the form of a spray mist having a mean drop diameter that is in a range between 10 μm and 100 μm.

2. The method according to claim 1 , wherein the mean drop diameter is in a range between 10 μm and 50 μm.

3. The method according to claim 1 , wherein the SiO 2 suspension and the at least one doping solution are in the form of spray mists and are intermixed in a mist phase thereof.

4. The method according to claim 1 , wherein the SiO 2 suspension or the doping solution are atomized into the spray mist using one or more spray nozzles.

5. The method according to claim 1 , wherein, the spray mist is generated at operating pressure in the range of 0.5 bar to 10 bar.

6. The method according to claim 1 , wherein, the spray mist is generated at flow rate in the range of 0.2 l/h to 4.0 l/h.

7. The method according to claim 1 , wherein the SiO 2 suspension or the doping solution or the at least partly doped SiO 2 slurry is kept in motion using one or more propeller stirrers.

8. The method according to claim 1 , wherein the SiO 2 suspension or the doping solution is filtered prior to the generation of the spray mist thereof.

9. The method according to claim 1 , wherein the SiO 2 suspension has a pH of more than 12.

10. The method according to claim 1 , wherein, the spray mist is generated at operating pressure of less than 5 bar.

11. The method according to claim 1 , wherein, the spray mist is generated at flow rate in the range of 0.2 l/h to 0.5 l/h.

Assignees

• Heraeus Quarzglas

Inventors

• Such Mario
• Schoetz Gerhard
• Langner Andreas

Classifications

• C03C2201/36

  containing rare earth metals and aluminium, e.g. Er-Al co-doped · CPC title

• C03C4/12

  for luminescent glass; for fluorescent glass · CPC title

• C03B2201/36

  doped with rare earth metals and aluminium, e.g. Er-Al co-doped · CPC title

• C09K11/025

  non-luminescent particle coatings or suspension media · CPC title

• C03C2201/3488

  Ytterbium · CPC title