Method for producing optical fiber preform

Patent metadata

Field	Value
Publication number	US-9517964-B2
Application number	US-201113229196-A
Country	US
Kind code	B2
Filing date	Sep 9, 2011
Priority date	Mar 12, 2009
Publication date	Dec 13, 2016
Grant date	Dec 13, 2016

Abstract

Provided is a method for producing an optical fiber preform including a dehydration step and a sintering step. In the dehydration step, a porous glass base material is provided to a furnace core tube of a dehydration-sintering furnace, and the porous glass base material is dehydrated using a dehydration agent added with an argon gas. In the sintering step, the porous glass base material dehydrated in the dehydration step is sintered. Further, in the dehydration step, a temperature of the porous glass base material begins to be increased in a condition such that a high heat conductivity gas, having a heat conductivity higher than a heat conductivity of the argon gas, is remaining inside the porous glass base material.

First claim

What is claimed is:

1. A method for producing an optical fiber preform, comprising:
providing a porous glass base material to a furnace core tube of a dehydration-sintering furnace, the furnace core tube being filled with air having a heat conductivity higher than a heat conductivity of argon gas;
beginning to replace the air in the furnace core tube with argon gas;
beginning to allow a temperature of the porous glass base material to increase when 30% to 90% of a volume of the air in the furnace core tube is replaced with argon gas so that 70% to 10% of a volume of the air remains in the furnace core tube in a case where a total volume of the air and the argon gas is defined as 100% by volume in the furnace core tube;
heating to dehydrate the porous glass base material using a dehydrating agent, the dehydrating agent being diluted by argon gas; and
sintering the dehydrated porous glass base material.

2. A method for producing an optical fiber preform, comprising:
providing a porous glass base material to a furnace core tube of a dehydration-sintering furnace, the furnace core tube being filled with air in the dehydration-sintering furnace;
preparing a high heat conductivity gas having a heat conductivity higher than a heat conductivity of argon gas, the high heat conductivity gas being different from air;
purging the high heat conductivity gas into the air filled furnace core tube and replacing 50% to 95% of a volume of the air presented in the furnace core tube with the high heat conductivity gas, the furnace core tube thus being filed with a mixture gas of the air and the high heat conductivity gas;
beginning to introduce argon gas into the furnace core tube;
beginning to allow a temperature of the porous glass base material to increase when 30% to 90% of a volume of the mixture gas in the furnace core tube is replaced with argon gas so that 70% to 10% of a volume of the mixture gas remains in the furnace core tube in a case where a total volume of the mixture gas and the argon gas is defined as 100% by volume in the furnace core tube;
heating to dehydrate the porous glass base material heated using a dehydrating agent, the dehydrating agent being diluted by argon gas; and
sintering the dehydrated porous glass base material.

3. The method for producing the optical fiber preform according to claim 2 , wherein the high heat conductivity gas is at least one type selected from the group consisting of a helium gas, nitrogen gas, and a neon gas.

4. The method for producing the optical fiber preform according to claim 2 , wherein the temperature of the porous glass base material begins to be increased when 40% to 80% of a volume of the mixture gas in the furnace core tube is replaced with argon gas.

Assignees

• Hamada Takahiro
• Fujikura Ltd

Inventors

• Hamada Takahiro

Classifications

• C03B37/01446 Primary

  Thermal after-treatment of preforms, e.g. dehydrating, consolidating, sintering (C03B37/01853 takes precedence) · CPC title