Catalyst slurry preparation system and use thereof

Patent metadata

Field	Value
Publication number	US-9512245-B2
Application number	US-201614994812-A
Country	US
Kind code	B2
Filing date	Jan 13, 2016
Priority date	Jul 30, 2010
Publication date	Dec 6, 2016
Grant date	Dec 6, 2016

Abstract

A process includes preparing a diluted catalyst slurry in a catalyst slurry preparation system. The diluted catalyst slurry contains solid particulate catalyst and liquid hydrocarbon diluent. The catalyst slurry preparation system includes a mixing vessel with a top part, a bottom part and a rotatable impeller system which is actuated by a motor. The rotatable impeller system has a magnetic actuated agitator shaft which is positioned along a longitudinal axis of the mixing vessel and extends through the top part of the mixing vessel. At least two double-bladed hubs are fixed to the magnetic actuated agitator shaft.

First claim

The invention claimed is:

1. A process comprising:
preparing a diluted catalyst slurry in a catalyst slurry preparation system wherein the diluted catalyst slurry comprises a solid particulate catalyst and a liquid hydrocarbon diluent, wherein said catalyst slurry preparation system comprises:
a mixing vessel comprising a top part, a bottom part and a rotatable impeller system which is actuated by a motor,
wherein the rotatable impeller system comprises a magnetic actuated agitator shaft which is positioned along a longitudinal axis of said mixing vessel and extends through said top part of said mixing vessel and comprises at least two double-bladed hubs which are fixed to said magnetic actuated agitator shaft.

2. The process according to claim 1 , wherein said mixing vessel further comprises one or more baffles, wherein said one or more baffles are fixed longitudinally along an inner wall of said mixing vessel, whereby said one or more baffles extend radially inward.

3. The process according to claim 1 , wherein the blades of each double-bladed hub are symmetrically positioned about said double-bladed hub and have a pitch angle (α) between 65° and 75°.

4. The process according to claim 1 , wherein each blade of said double-bladed hub is an airfoil comprising a root portion attached to the double-bladed hub and a radially outwardly disposed tip portion with an upper side edge therebetween, wherein the upper side edge faces the top part of said mixing vessel, and wherein each blade comprises a lower side edge facing said bottom part of said mixing vessel.

5. The process according to claim 4 , wherein said tip portion inclines convexly toward said top part of said mixing vessel beyond said upper side edge, wherein said upper side edge extends laterally from said root portion to said tip portion and inclines concavely toward said tip portion, and wherein said lower side edge is concave.

6. The process according to claim 1 , wherein a first double-bladed hub is fixed to said magnetic actuated agitator shaft in a lower half of said mixing vessel.

7. The process according to claim 6 , wherein a second double-bladed hub is fixed to said magnetic actuated agitator shaft in a lower quarter of said mixing vessel.

8. The process according to claim 7 , wherein a distance between said first and said second double-bladed hub is between one half to one third of a length of said magnetic actuated agitator shaft.

9. The process according to claim 1 , wherein said one or more baffles extend radially inward over a distance of between 10% and 20% of a diameter of said mixing vessel.

10. The process according to claim 1 , wherein said double-bladed hub has a blade span of between 30% and 50% of a diameter of said mixing vessel.

11. The process according to claim 1 , further comprising one or more mud pots suitable for containing a concentrated catalyst slurry, wherein each mud pot is operably connected to said mixing vessel.

12. The process according to claim 11 , wherein the mixing vessel is connected to a polymerization reactor.

13. The process according to claim 1 , wherein said mixing vessel is a liquid full tank.

14. The process according to claim 1 , wherein the concentration of said solid particulate catalyst in said liquid hydrocarbon diluent is between 0.1% and 10% by weight.

15. The process according to claim 1 , wherein said solid particulate catalyst has an average diameter between 1 μm and 100 μm.

16. The process according to claim 1 , wherein said rotatable impeller system is rotatable at a speed of between 50 and 1000 rpm.

17. The process according to claim 1 , wherein said mixing vessel is cylindrical.

Assignees

• Total Res & Technology Feluy

Inventors

• Brusselle Alain
• Fouarge Louis

Classifications

• B01F13/0827

  Operations & Transport · mapped topic

• C08F4/65916

  supported on a carrier, e.g. silica, MgCl2, polymer · CPC title

• C08F10/00

  Homopolymers and copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond · CPC title

• B01F7/1675

  Operations & Transport · mapped topic

• B01F7/00633

  Operations & Transport · mapped topic