Manufacturing method for optical substrate using film shaped mold, manufacturing device, and optical substrate obtained thereby

Patent metadata

Field	Value
Publication number	US-9511552-B2
Application number	US-201514674661-A
Country	US
Kind code	B2
Filing date	Mar 31, 2015
Priority date	Oct 5, 2012
Publication date	Dec 6, 2016
Grant date	Dec 6, 2016

Abstract

A method for producing an optical substrate includes: a step of preparing a long film-shaped mold having a concave-convex pattern surface having a concave-convex pattern; a step of forming a coating film made of a sol-gel material on the concave-convex pattern surface of the film-shaped mold; a step of adhering the coating film, which is formed on the concave-convex pattern surface of the film-shaped mold, to a substrate by arranging the concave-convex pattern surface of the film-shaped mold on which the coating film made of the sol-gel material is formed to face the substrate and by pressing a pressing roll against a surface of the film-shaped mold on a side opposite to the concave-convex pattern surface; a step of releasing the film-shaped mold from the coating film; and a step of curing the coating film adhered to the substrate.

First claim

What is claimed is:

1. A method for producing an optical substrate, the method comprising:
a step of preparing a film mold having a concave-convex pattern surface having a concave-convex pattern;
a step of forming a coating film made of a sol-gel material on the concave-convex pattern surface of the film mold;
a step of adhering the coating film, which is formed on the concave-convex pattern surface of the film mold, to a substrate by arranging the concave-convex pattern surface of the film mold on which the coating film made of the sol-gel material is formed to face the substrate and by pressing a pressing roll against a surface of the film mold on a side opposite to the concave-convex pattern surface;
a step of releasing the film mold from the coating film; and
a step of curing the coating film adhered to the substrate.

2. The method for producing the optical substrate according to claim 1 , wherein the step of preparing the film mold includes:
coating a film-base member with a concave-convex forming material;
performing a roll transfer of the concave-convex pattern to the concave-convex forming material by pressing a transfer roll having the concave-convex pattern against the concave-convex forming material with which the film-base member has been coated, while rotating the transfer roll; and
curing the concave-convex forming material, to which the concave-convex pattern has been transferred by the roll transfer, so as to obtain the film mold in a roll shape.

3. The method for producing the optical substrate according to claim 2 , wherein the film-base member having the cured concave-convex forming material is taken up by a film take-up roll to be wound around the film take-up roll.

4. The method for producing the optical substrate according to claim 2 , wherein the concave-convex pattern of the transfer roll is transferred while the film-base member is being transported by using a film feeding roll configured to feed the film-base member and a film take-up roll configured to take up the film-base member to wind the film-base member therearound.

5. The method for producing the optical substrate according to claim 3 , wherein the film mold in the roll shape wound around the film take-up roll is fed to and is moved toward the pressing roll.

6. The method for producing the optical substrate according to claim 5 , wherein the released film mold is taken up by a mold take-up roll to be wound around the mold take-up roll.

7. The method for producing the optical substrate according to claim 1 , wherein the pressing roll is pressed against the surface of the film mold on the side opposite to the concave-convex pattern surface while the coating film formed on the concave-convex pattern surface is being heated.

8. The method for producing the optical substrate according to claim 1 , wherein the coating film is heated between the step of adhering the coating film to the substrate and the step of releasing the film mold from the coating film, or in the step of releasing the film mold from the coating film.

9. The method for producing the optical substrate according to claim 1 , wherein the film mold is fed underneath the pressing roll while the film mold is being continuously coated with the sol-gel material, and a plurality of pieces of the substrate are transported to the pressing roll and the coating film formed on the concave-convex pattern surface of the film mold is pressed successively against the plurality of substrates with the pressing roll.

10. The method for producing the optical substrate according to claim 1 , wherein the concave-convex pattern of the film mold is an irregular concave-convex pattern;
an average pitch of concavities and convexities of the irregular concave-convex pattern is in a range of 100 nm to 1,500 nm; and
an average value of depth distribution of the concavities and convexities is in a range of 20 nm to 200 nm.

11. The method for producing the optical substrate according to claim 1 , wherein the substrate is a glass substrate.

12. The method for producing the optical substrate according to claim 1 , wherein the sol-gel material contains a silica precursor.

13. A method for producing an organic EL element, the method comprising:
producing a diffraction grating substrate, which has a concave-convex surface as an optical substrate, by using the method of producing the optical substrate as defined in claim 1 ; and
stacking a transparent electrode, an organic layer, and a metal electrode successively on the concave-convex surface of the diffraction grating substrate, so as to produce the organic EL element.

Assignees

• Jx Nippon Oil & Energy Corp

Inventors

• Toriyama Shigetaka
• Nishimura Suzushi
• Kozasa Naoto
• Takahashi Madoka

Classifications

• B29D11/00769

  Producing diffraction gratings · CPC title

• G02B5/0268

  characterized by the fabrication or manufacturing method · CPC title

• G02B1/12

  by surface treatment, e.g. by irradiation · CPC title

• B29D11/00798

  Producing diffusers · CPC title

• G02B5/021

  the diffusion taking place at the element's surface, e.g. by means of surface roughening or microprismatic structures · CPC title