NMR probe head with variable RF resonant circuit capacitor which can be adjusted in steps via a piezo-electric actuator

Patent metadata

Field	Value
Publication number	US-9500726-B2
Application number	US-201414195919-A
Country	US
Kind code	B2
Filing date	Mar 4, 2014
Priority date	Mar 11, 2013
Publication date	Nov 22, 2016
Grant date	Nov 22, 2016

Abstract

An NMR probe head has a capacitor with a dielectric ( 5 ), which surrounds a cavity ( 15 ) in which a capacitor piston ( 7 ) is disposed. A sliding bush ( 9 ) has a through hole ( 16 ) in which a piston operating rod ( 8 ) extends. The piston operating rod ( 8 ) is connected to a piezo-electric actuator and to the capacitor piston ( 7 ) in such a way that it displaces the capacitor piston linearly when a sawtooth voltage is applied to the piezo-electric actuator. The sliding bush thereby applies braking friction to the piston operating rod during linear displacement of the capacitor piston and only allows the piston operating rod to slide through during the steep edges of the sawtooth voltage. This avoids the disadvantages of prior art, wherein the NMR probe head remains compact and the material cost and manufacturing complexity are reduced.

First claim

I claim:

1. An NMR probe head having an RF resonant circuit, the probe head comprising:
at least one capacitor that is part of the RF resonant circuit, said capacitor having a dielectric, which at least partially surrounds a cavity, said dielectric being connected to at least one electrode at which an electrical potential of said capacitor can be picked off, wherein a capacitor piston with an electrically conductive surface is disposed in said cavity within said dielectric;
a piezo-electric actuator disposed outside said cavity as an extension of an axis of said capacitor piston;
a piston operating rod mechanically connected to said piezo-electric actuator and cooperating with said capacitor piston to move said capacitor piston in said cavity; and
a sliding bush mechanically connected to said dielectric, said sliding bush having a through-hole through which said piston operating rod extends, wherein said piston operating rod moves said capacitor piston linearly in response to application of a sawtooth-waveform electric voltage to said piezo-electric actuator to tune said capacitor, said sliding bush thereby applying braking friction to said piston operating rod during linear displacement of said capacitor piston in such a fashion that said piston operating rod only slides through said through-hole during steep edges of said applied sawtooth voltage.

2. The NMR probe head of claim 1 , further comprising a mass element of mass m attached to a side of said piezo-electric actuator facing away from said piston operating rod, wherein, when said sawtooth-waveform electric voltage is applied to said piezo-electric actuator, said mass element moves with said actuator in a polarization direction thereof, said mass m thereby producing additional inertial forces.

3. The NMR probe head of claim 2 , further comprising a hollow mechanical body having a cavity in which said piezo-electric actuator is received, wherein said hollow mechanical body mechanically stresses said piezo-electric actuator in a polarization direction thereof.

4. The NMR probe head of claim 3 , wherein a mechanical stress exerted by said hollow mechanical body on said piezo-electric actuator is chosen to be sufficiently large that said piezo-electric actuator is always compressed during operation.

5. The NMR probe head of claim 3 , wherein said hollow mechanical body is integral with said mass element.

6. The NMR probe head of claim 2 , wherein at least one of moving parts of said capacitor, said capacitor piston, said piston operating rod, said piezo-electric actuator and said mass element, can be secured against rotation about said axis of said capacitor piston by a choice of cross-sectional shape or of a triangular cross-section, at least of said piston operating rod and of said through-hole of said sliding bush.

7. The NMR probe head of claim 1 , wherein at least outer surfaces of said capacitor piston and said piston operating rod are constructed from electrically conductive material on which an electrical connection of said capacitor is mounted, wherein a second electrical potential of the capacitor can be picked off at said electrical connection.

8. The NMR probe head of claim 7 , wherein at least outer surfaces of said sliding bush are also constructed from electrically conductive material and form an electrical contact with said piston operating rod so that said second electrical potential of said capacitor can be picked off at said sliding bush.

9. The NMR probe head of claim 1 , wherein said capacitor is mechanically rigidly fastened to the NMR probe head via said sliding bush.

10. The NMR probe head of claim 1 , wherein said sliding bush has a mechanically rigid part and an elastic part.

11. The NMR probe head of claim 10 , wherein said elastic part of said sliding bush is constituted in a shape of a collet, said collet clamping said piston operating rod to produce mechanical friction.

12. The NMR probe head of claim 11 , wherein said collet provides an electrically conductive contact between said sliding bush and said piston operating rod.

13. The NMR probe head of claim 10 , wherein said mechanically rigid part is integral with said elastic part of said sliding bush.

Assignees

• Bruker Biospin Ag

Inventors

• Baumann Daniel Guy

Classifications

• G01R33/36

  Electrical details, e.g. matching or coupling of the coil to the receiver · CPC title

• G01R33/34 Primary

  Constructional details, e.g. resonators {, specially adapted to MR} · CPC title

• G01R33/3628 Primary

  Tuning/matching of the transmit/receive coil · CPC title

• G01R33/30 Primary

  Sample handling arrangements, e.g. sample cells, spinning mechanisms · CPC title

• G01R33/34092

  RF coils specially adapted for NMR spectrometers · CPC title