Method for manufacturing aluminum-titanate-based ceramic honeycomb structure

Patent metadata

Field	Value
Publication number	US-9499442-B1
Application number	US-201313873379-A
Country	US
Kind code	B1
Filing date	Apr 30, 2013
Priority date	Mar 15, 2013
Publication date	Nov 22, 2016
Grant date	Nov 22, 2016

Abstract

A method for manufacturing a ceramic honeycomb structure includes kneading titania particles, alumina particles and binder ingredient such that raw material paste including the titania particles, alumina particles and binder ingredient is prepared, forming a body made of the paste and having a honeycomb structure such that the body has the honeycomb structure having through-holes extending in the longitudinal direction of the body and partitions formed between the through-holes, sintering the body made of the paste such that a ceramic body having the honeycomb structure is formed, applying sealant to either end of each through-hole of the ceramic body such that each through-hole of the ceramic body is sealed at one end, and heating the sealant sealing one end of each through-hole such that the ceramic body having cured sealant at one end of each through-hole in the honeycomb structure is formed.

First claim

What is claimed is:

1. A method for manufacturing a ceramic honeycomb structure, comprising:
kneading titania particles, alumina particles and a binder ingredient such that a raw material paste comprising the titania particles, the alumina particles and the binder ingredient is prepared;
forming a body comprising the raw material paste and having a honeycomb structure such that the body has the honeycomb structure having a plurality of through-holes extending in a longitudinal direction of the body and a plurality of partition portions formed between the through-holes;
sintering the body comprising the raw material paste and having the honeycomb structure at a temperature in a range of from 1350° C. to 1650° C. such that a ceramic body comprising aluminum titanate and having the honeycomb structure is formed;
applying a sealant comprising titania particles and alumina particles to one end of each of the through-holes of the ceramic body in the longitudinal direction such that each of the through-holes of the ceramic body is sealed at the one end; and
heating the sealant sealing the one end of each of the through-holes of the ceramic body at a temperature which is 1000° C. or higher and lower than the temperature of the sintering of the body such that the ceramic body having a cured sealant at the one end of each of the through-holes in the honeycomb structure is formed without sintering the cured sealant at the one end of each of the through-holes in the honeycomb structure,
wherein the heating of the sealant comprises heating both end surfaces of the ceramic body.

2. The method for manufacturing a ceramic honeycomb structure according to claim 1 , further comprising drying the body comprising the raw material paste and having the honeycomb structure.

3. The method for manufacturing a ceramic honeycomb structure according to claim 1 , further comprising degreasing the body comprising the raw material paste and having the honeycomb structure such that an organic ingredient in the raw material paste of the body is removed.

4. The method for manufacturing a ceramic honeycomb structure according to claim 1 , further comprising forming a precursor comprising particles comprising titania particles and alumina particles, wherein the kneading comprises kneading the binder ingredient and the particles of the precursor comprising the titania particles and the alumina particles.

5. The method for manufacturing a ceramic honeycomb structure according to claim 4 , wherein the forming of the precursor comprises spray-drying the alumina particles onto the titania particles.

6. The method for manufacturing a ceramic honeycomb structure according to claim 1 , wherein the heating of the sealant comprises heating the sealant at a temperature of 1100° C. or higher and lower than the temperature of the sintering of the body.

7. The method for manufacturing a ceramic honeycomb structure according to claim 3 , further comprising drying the body comprising the raw material paste and having the honeycomb structure.

8. The method for manufacturing a ceramic honeycomb structure according to claim 5 , further comprising degreasing the body comprising the raw material paste and having the honeycomb structure such that an organic ingredient in the raw material paste of the body is removed.

9. The method for manufacturing a ceramic honeycomb structure according to claim 7 , further comprising forming a precursor comprising particles comprising titania particles and alumina particles, wherein the kneading comprises kneading the binder ingredient and the particles of the precursor comprising the titania particles and the alumina particles.

10. The method for manufacturing a ceramic honeycomb structure according to claim 9 , wherein the forming of the precursor comprises spray-drying the alumina particles onto the titania particles.

11. The method for manufacturing a ceramic honeycomb structure according to claim 5 , wherein the heating of the sealant comprises heating the sealant at a temperature of 1100° C. or higher and lower than the temperature of the sintering of the body.

12. The method for manufacturing a ceramic honeycomb structure according to claim 4 , wherein the heating of the sealant comprises heating the sealant at a temperature of 1100° C. to or higher and lower than the temperature of the sintering of the body.

13. The method for manufacturing a ceramic honeycomb structure according to claim 4 , further comprising drying the body comprising the raw material paste and having the honeycomb structure.

14. The method for manufacturing a ceramic honeycomb structure according to claim 4 , further comprising degreasing the body comprising the raw material paste and having the honeycomb structure such that an organic ingredient in the raw material paste of the body is removed.

15. The method for manufacturing a ceramic honeycomb structure according to claim 9 , wherein the heating of the sealant comprises heating the sealant at a temperature of 1100° C. or higher and lower than the temperature of the sintering of the body.

16. The method for manufacturing a ceramic honeycomb structure according to claim 6 , further comprising drying the body comprising the raw material paste and having the honeycomb structure.

17. The method for manufacturing a ceramic honeycomb structure according to claim 6 , further comprising degreasing the body comprising the raw material paste and having the honeycomb structure such that an organic ingredient in the raw material paste of the body is removed.

18. The method for manufacturing a ceramic honeycomb structure according to claim 10 , wherein the heating of the sealant comprises heating the sealant at a temperature of 1100° C. or higher and lower than the temperature of the sintering of the body.

19. The method for manufacturing a ceramic honeycomb structure according to claim 13 , wherein the heating of the sealant comprises heating the sealant at a temperature of 1100° C. or higher and lower than the temperature of the sintering of the body.

20. The method for manufacturing a ceramic honeycomb structure according to claim 14 , wherein the heating of the sealant comprises heating the sealant at a temperature of 1100° C. or higher and lower than the temperature of the sintering of the body.

Assignees

• Ibiden Co Ltd

Inventors

• Yamayose Kazunori

Classifications

• C04B38/0006 Primary

  Honeycomb structures (from one or more corrugated sheets by winding or stacking C04B38/0083) · CPC title

• C04B35/62655

  Drying, e.g. freeze-drying, spray-drying, microwave or supercritical drying · CPC title

• C04B35/478

  based on aluminium titanates · CPC title

• C04B2235/6021

  Extrusion moulding · CPC title

• C04B35/62813

  Alumina or aluminates · CPC title